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Analysis of temporal and spatial contact voltage fluctuation during fretting in automotive connectors

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HAL Id: hal-01104786

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Submitted on 19 Jan 2015

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Analysis of temporal and spatial contact voltage fluctuation during fretting in automotive connectors

Sofiane El Mossouess, N Benjemâa, E Carvou, Rochdi El Abdi, H Obame, L Doublet, T Rodari

To cite this version:

Sofiane El Mossouess, N Benjemâa, E Carvou, Rochdi El Abdi, H Obame, et al.. Analysis of temporal and spatial contact voltage fluctuation during fretting in automotive connectors. IEEE. The 27th International Conference on Electrical Contacts, Jun 2014, Dresden, Germany. IEEE, 2014. �hal- 01104786�

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Analysis of temporal and spatial contact voltage fluctuation during fretting in automotive connectors

S. El Mossouess1, 2, E. Carvou1, R. El Abdi1, N. Benjemâa3, H. Obame1, L. Doublet2 and T. Rodari2

1Institut de Physique de Rennes, Université de Rennes1, Campus de Beaulieu, 35042 Rennes Cedex – France

2Entreprise Valeo, Etudes Electroniques- Créteil, Europarc. 94000 Créteil –France

3Entreprise Contelec- 8 rue de la Motte Baril, 35000 Rennes- France

Abstract

Our study is focused on contact voltage fluctuations during fretting with small amplitudes of a few tens microns which generate damage of the contact of connectors. A contact composed by a pin and a curve female part are submitted to vibration cyclic of 25µm at 100Hz and supplied with current ramp from 0.1mA to 3A in two directions. With the help of fast devices, the voltage and position data acquisition are conjointly made with the common DC contact voltage dur- ing fretting. Some unexpected results state that voltage fluctuation occurs in the different stage of fretting and start at the beginning of test in the insertion direction and located at half of track. These small voltage fluctuations around few mV increased to few hundred millivolts and may reach few volt at ultimate phase of degradation with random distribu- tion along the track. When the motion is stopped the ohmic conduction of such fretting interface is ensured only when the subsequent voltage stay below a sutured value depending on the degradation and current level. It is found that the common three phases of degradation have a different saturation voltage which appears at higher and higher current and induce voltage breakdown. Regarding that symmetric characterises is obtained in two the directions current ramp the semiconducting behaviour effect of oxide layers on debris particle is negligible. As voltage-current experimental data was well fitted to similar equation of granular material conduction we have deduced the fitting parameters (Vl and I0) of interface.

Keywords: fretting-corrosion, fritting, contact resistance, contact voltage, intermittence.

1 Introduction

Due to repetitive micro sliding, fretting phenomena has been defined as a subsequent electrical and mechanical degradation of the contact interface in telecommunication and more recently in automotive connectors. Electrical degradation is currently quantified by contact resistance increases [1,2,3]. Also intermittence and contact voltage fluctuation have been investigated and reported in the lit- erature [4,5,6]. In order to explain voltage fluctuations mentioned in the literature [7] as shown in the figure 1 the authors have focused their on the three regions.

Tension et résistance en fonction du nombre d'opération FCI demi-tulipe étamée, 100Hz, 50 µm P-P

Operations

100 1000 10000 100000 1000000

Contact Voltage(V)

0.0001 0.001 0.01 0.1 1

Contact Resistance (m)

Voltage Col 7 vs Rc

Phase 1

Phase 2

Phase 3

5 50 500 5000

0.5

Figure 1 Evolution of contact voltage and resistance dur- ing fretting at 200 mA. Dashed area indicates the three phases of fretting.

Some considerations on electrical break down by fritting voltage phenomena [8] and non-linearity conduction [9]

in the corroded interface or granular materials [10] are suggested to explain the origin of large low fluctuation.

Using the latest sensitive voltage analysis in real time we focus our interest on contact voltage fluctuations. As shown in Figure1 typical example the low level and near the constriction voltage (Phase1) are analysed [11]. In the second level corresponding to fretting appearance and fi- nally at the saturated voltage [12]. This analysis is made fluctuation during cycle time and position in the track. To disclose the non-linearity between voltage and current we explore and plot voltage current characteristics in wide range current 100µA to 3A. This work is done on com- mercials tin coated connectors (Female part shape with plane lamella) and medium frequency 100Hz with ampli- tude 50µm P-P. The objective of this work is to extend the knowledge of contact voltage and its validity to define the contact resistance verses time and displacement inside the cycle. By this approach we aim to define the dynamic contact resistance and his dependency to the current flow level.

2 Experimental device and procedure

2.1 Vibration characteristics

The samples are extracted from a commercial automotive connector which is made in copper alloys coated with Nickel 2µm under layer and tin 2µm external coat. To

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simulate real working conditions a particular vibration characteristics are imposed directly to the contact. As is shown in figure 2, one side (half side of the female part) is fixed firmly on force sensor and attached on the ground while the male part (the lamella) is attached to the shaker, working at frequency 100 Hz with amplitude of 2a=50µm (peak to peak) of sinus oscillations. This movement is controlled and measured by displacement sensor (by laser 0.1µm of resolution) focused.

Figure 2 Fretting device and Voltage and displacement measurements

on the female and male parts. The contact force of 2N is applied by micro sliding and indentation of female part on lamella. The average fretting contact voltage is measured by a micro voltmeter (0.1 µV resolution averaged over 1 Power line cycle of 20ms i.e. 2 periods of oscillations of fretting 10ms) under 200mA delivered by current source with 10V Voltage compliance. Also, this current source was used in range 100µA to 3A to plot current Voltage characteristic at different phases of fretting. For faster fluctuation during the cycle as show in figure 3 a digital oscilloscope was used to acquire contact voltage fluctua- tions and displacement during one cycle (sampling period 20µs) at different stages of fretting. So we can made analysis of the voltage on the two distinct direction of sliding: the insertion –a to +a and the extraction +a to –a of the lamella.

The samples are extracted from a commercial connector which is made in copper alloys coated with Nickel 2µm under layer and tin 2µm external coat.

Time (ms)

3 4 5 6 7 8 9 10 11 12

Contact Voltage (V)

0.000 0.005 0.010 0.015 0.020 0.025 0.030

Contact Displacement m)

-30 -20 -10 0 10 20 30

Voltage Displacement

+a

Figure 3 Contact voltage and contact displacement during one vibration cycle at 100Hz and 50µm p-p.

3 Results

The main results deal with voltage analyses during sliding in the two directions of motion and its non-linearity in wide range of current versus aging phases as are shown in figure 1.

3.1 Voltage fluctuations during fretting

Contact voltage are plotted for 2 successive cycles after each 1000 cycles during different stages of aging corre- sponding to the previous three phases described in the figure 1. Theses curves are shown in figures (4,5,6).

As we can see in figure 4a at earlier first phase of fretting corresponding to low voltage (0 to 10 mV) a mayor part of fluctuations take place at half period of duty cycles.

However this low voltage remains constant during the second part of duty cycle. In addition we have examined the voltage fluctuation during displacement (figure 4b) in the twice directions i.e. from (-a) to (+a) directions of the displacement (insertion) and from the (+a) to the (-a) di- rection (extraction). Let’s note that in the insertion direc- tion a maximum voltage is observed at the left part of the track (comprised between 0 and –a, approximately 17µm). Surprisingly this maximum voltage wasn’t ob- served when the displacement is in the reversed direction (extraction). Subsequently contact voltage remains con- stant and keep contact resistance at its construction value.

This behaviour is currently observed during the first phase of fretting approximately 10 000 cycles. One can assume that this behaviour is due to the unsymmetrical surface damage.

2D Graph 1

Time(ms)

2.5 5.0 7.5 10.0 12.5 15.0 17.5 20.0 22.5

Contact Voltage (mV)

0 2 4 6 8 10

Contact Displacement (µm)

-40 -20 0 20 40 1 K Cy.

2 K Cy.

3 K Cy.

4 K Cy.

5 K Cy.

6 K Cy.

7 K Cy.

8 K Cy.

9 K Cy.

10 K Cy.

Displacement

1 to 10000 operations

a

Force Sensor

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2D Graph 5

Contact track(µm)

-30 -20 -10 0 10 20 30

Contact Voltage (mV)

0.0 0.5 1.0 1.5 2.0

Contact Resistance (m)

0.0 2.5 5.0 7.5 10.0 Positive direction Negative direction

- a + a

b

Figure 4 Voltage fluctuation during the first phase of fret- ting: a) fluctuation during time of two periods after differ- ent number of cycles, b) fluctuation during displacement after 1K cycle.

However, for further operations corresponding at the sec- ond phase (figure 1) this maximum voltage in the left side is remained and additional maximum appears in the sec- ond part of duty cycle as shown in figure 5a. This is con- firmed by plotting the voltage during displacement in figure 5b. Also, we remark that the position in the fretting track and amplitude of this voltage fluctuation are changed during this second phase.

Time (ms)

2.5 5.0 7.5 10.0 12.5 15.0 17.5 20.0 22.5

Contact Voltage (mV)

0 10 20 30 40 50

Contact Displacement (µm)

-40 -20 0 20 40 11 K Cy.

12 K Cy.

13 K Cy.

14 K Cy.

15 K Cy.

16 K Cy.

17 K Cy.

18 K Cy.

19 K Cy.

20 K Cy.

30 K Cy.

Displacement

11000 to 30000 operations

a

Contact Track (µm)

-30 -20 -10 0 10 20 30

Contact Voltage (V)

0.00 0.02 0.04 0.06 0.08 0.10 0.12

Contact Resistance ()

0.0 0.1 0.2 0.3 0.4 0.5 0.6 Positive direction

Negative direction

- a + a

b

Figure 5 Voltage fluctuation during the second phase of fretting: a) fluctuation during time of two periods after different number of cycles, b) fluctuation during dis- placement after 20K cycle.

Finally, at the last phase of fretting the contact voltage become random but some stable voltage can be observed during a fraction of the duty cycle approximately during a quarter of cycle 2.5ms (figure 6a.b). In addition, this volt-

age can fall down to the low value close to the second phase value. Also, this random behaviour of contact volt- age fluctuation and its limited value can be attributed to the breakdown of films by fritting phenomena reported by Holm [8]. This random behaviour at this advanced stage of fretting can be related to the sever degradation by wear and accumulation of debris and their sudden ejection.

2D Graph 1

Time (ms)

2.5 5.0 7.5 10.0 12.5 15.0 17.5 20.0 22.5

Contact Voltage (V)

0 1 2 3 4 5

Contact Displacement (µm)

-40 -20 0 20 40 160 K Cy.

161 K Cy.

162 K Cy.

163 K Cy.

164 K Cy.

165 K Cy.

166 K Cy.

167 K Cy.

168K Cy.

169 K Cy.

Displacement

160000 to 169000 operations

a

2D Graph 5

Track (µm)

-30 -20 -10 0 10 20 30

Contact Voltage (V)

0.0 0.5 1.0 1.5 2.0 2.5 3.0

Contact Resistance ()

0.0 2.5 5.0 7.5 10.0 12.5 15.0 Positive direction Negative direction

- a + a

b

Figure 6 Voltage fluctuation during the third phase of fretting: a) fluctuation during time of two periods after different number of cycles, b) fluctuation during dis- placement after 168K cycle.

In fact, the origin of theses fluctuations was assumed to the debris coming from the wear of the coating [10,11]

and their oxidation [13]. However, the observed fluctua- tions of the first phase are mainly due to mechanical abra- sion of the coating localised in the same position of the track while their appearances in the insertion motion can be attributed to the uniformity wear zone.

Lastly and principally in the second and third phases the production of the wear debris is accentuated and their oxidation is activated so the maximum voltage fluctuation is observed and each side of the centre of motion.

3.2 Contact voltage analysis after fretting

As reported in the literature the oxidation of contact sur- faces induce poor conduction and non-linearity of current flow in the contact. As an example in the literature re- ported in literature for tarnished films [9], we believed that the similar phenomena can take place in this corroded debris in various phases of fretting. For this aim, we ap- plied urrent ramp from 0.10mA to 1A at contact simple stopped at different phases of figure 1.In the first phase this result given in figure 7, we can remark that the con-

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tact voltage is proportional to the current. So the linearity is ensured and contact résistance remain constant Rc=Vc/Ic and close to the construction value. Its value is close to construction value of few mΩ witch we can cal- culate by the slope of the curve V-I. At the second and the third phases the contact voltage follow linear evolution and remain proportional to the current where the slope is the contact résistance Rc=Vc\Ic. However, when this voltage reach certain value generally > 100mV break down appears and contact voltage fluctuate around con- stant value. From this voltage level contact resistance is variable and could decrease with current enhancement as is shown in figure 8. This phenomena is accentuated and take place at lowest current of few tens mA and higher breaking voltage>500mV namely in the phase 3.

2D Graph 1

Contact current (A)

0.0 0.2 0.4 0.6 0.8 1.0

Contact Voltage (V)

0.0 0.1 0.2 0.3 0.4 0.5 0.6

I source vs 0 I source vs 3 I source vs 4 I source vs 5 I source vs 6 I source vs 7 I source vs 8 I source vs 9 I source vs 10 I source vs 11 I source vs 12 I source vs 13 I source vs 14 I source vs 15 I source vs 16 I source vs 17 I source vs 18 I source vs 19 I source vs Puissance0.015 PasLog vs a1 PasLog vs a9 PasLog vs a2 PasLog vs a3

Phase 1Phase 2Phase 3

Figure 7 Current voltage characteristics at stopped mo- tion at different stage of fretting. Dashed curves are power curves 5 and 25 mW.

Also, the breaking and the non-linearity domain can be limited by the maximum of power dissipation which can be supported by contact interface without damage. Two power curves corresponding 5mW and 25mW can limit this domain. Theses curves are marked by dashed line in figure 7. Also, beyond the maximum power of 25mW supported by the contact it is found that power of 0.15W breakdown and non-linearity appears all the time. In this work we have confronted the breaking voltage value of such interface resulting from the fretting to the previous theory of HOLM [8]. It is clearly that breaking voltage is comprised in the range of 170mV to 700mV; this is corre- sponding to fritting A and B.

2D Graph 3

Contact Voltage (V)

0.001 0.01 0.1 1

Contact Resistance (

0.01 0.1 1 10

Fritting Voltage

Figure 8 Contact resistance verses contact voltage from different stage of fretting.

3.3 Contact voltage analysis after fretting

In order to examine the semi-conducting and non-linearity phenomena we apply the current ramp in the two direc- tions: from –1A to 1A alternatively (I+∆I) and (I-∆I) with logarithmic step ∆I. The corresponding plots are given in figure 9 corresponding to contact degradation stopped at different phases of fretting. As the main remarks that the curves are symmetric and no-rectifying effect coming to semi-conducting of oxide layers on tin and copper and nickel debris.

2D Graph 1

Contact current (A)

-3 -2 -1 0 1 2 3

Contact Voltage (V)

-0.8 -0.6 -0.4 -0.2 0.0 0.2 0.4 0.6 0.8 1.0

Col 4 vs Col 5 Col 4 vs Col 10 Col 4 vs Col 12 Col 4 vs Col 14 Col 4 vs Col 14 Col 4 vs Col 16 Col 4 vs Col 18 Col 4 vs Col 20 Col 4 vs Col 22 Col 4 vs Col 22 Col 1 vs Col 2

Figure 9 Contact voltage versus contact current for posi- tive and negative current at stopped motion for different stage of fretting.

In addition, some attempt by fitting experimental result (figure10) data (I-V) to the well-known equation of con- tact voltage Vc versus current Ic in granular materials [10]:

) 1

(

) 1 (1

0 c

e V Vc l

Where Vl=0.371 mV is voltage satu- ration (breaking voltage) and I0=1.633A is relate the cur- rent slop. A similar fitted curve is obtained for negative ramp Vl =0.278 and Il =1.344A. Furthermore, by deriva- tion of the upper equation we deduce the dynamic contact resistance Rd law versus current Ic: 0 I0

I

d

C

e R R

Where

R0 is Vl/I0. This mean that contact resistance decrease ex- ponentially whit the applied current I2D Graph 1 c.

Contact Current (A)

-3 -2 -1 0 1 2 3

Contact Voltage (V)

-0.4 -0.3 -0.2 -0.1 0.0 0.1 0.2 0.3 0.4

Fited curve to Vl(1-exp(-I/I0)) Fited curve to Vl(1-exp(-I/I0))

Vl

-Vl

Figure 10 Contact voltages versus contact current: Solid lines are the fitted curves to experimental data.

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4 Conclusion

The present study aims to expand our knowledge about the phenomena of fretting carrying an interest of fluctuat- ing voltages of contacts in conjunction with mean voltag- es widely used as a control of degradation of electrical conduction of contacts.

Indeed, the voltage fluctuations appear from the begin- ning of vibration only in a part of the track and preferen- tially in the direction of insertion. By consequence these fluctuations generate in these parts of the track contacts resistances higher resistance value compared to the value of the constriction resistance. This result demonstrates the existence of localized mechanical degradation of the track of a non-uniform manner. It is only in the next phases of fretting that these fluctuations reinforce and change place of occurrence in the track to become random and very important along a portion of the track friction : it is the effect of wear and debris accumulated in the conduction and ejected periodically that can explain this behavior.

These voltage fluctuations disappear at each stop of the vibration, giving way to a stable voltage with different values depending on the state of chemical and mechanical interface degradation. The linearity of the conduction is kept to a certain current level from which a phenomena of electrical breakdown appears and is accompanied accom- panied by voltage limitation as described by Holm "Frit- ting voltage". This phenomenon of saturation and non- linearity is similar to that of the conduction in the granular material of which the texture is similar to that of the wear debris in the interface [10]. In conclusion the study of fluctuations and saturation voltage as the current increases and the state of degradation gets worse, constitute a useful and appropriate tool for characterizing the conduction contacts during fretting.

ACKNOWLEDGMENTS

The authors wish to thank Professor Brian Mitchell for reviewing the manuscript. They also acknowledge the French Agence Nationale de la Recherche et de la Tech- nologie (ANRT) for financial support.

5 References

[1] M. Antler "Survey of contact fretting in Electrical connectors» IEEE Trans.on components, Hybrids and Manufacturing 1985 vol.8 pp 87-104

[2] J.L. Queffelec, N. Ben jemaa and D. Travers, " Mate- rials and contact shape studies for automobile connectors development " IEEE Trans., Comp., Hybrids., and Ma- nuf., Technol., March 1990 Vol.14 NO. 1, pp. 90-94, [3] M Braunovic "Effect of fretting on the contact resis- tance of aluminium with different contact materials" Pro- ceeding of the 9th ICEC Chicago 1978, pp 173-179 [4] B Abott "Time distribution of intermittent versus con- tact resistance for Tin-Tin connectors interfaces during low motion"

[5] C. Maul, J. W. McBride, J. Swingler

“On the Nature of Intermittence in Electrical Contacts”

Proc. Int. Conf. Electrical Contacts Stockholm 2000, pp312-319

[6] E. Carvou, N. Ben Jemaa "Time and Level Analysis of Contact Voltage Intermittences Induced by Fretting in Power Connector" Proceeding of Holm conf 2007. pp- 211-215

[7] E. Carvou, N. Ben Jemaa "Electrical contact beha- viour of power connector during fretting vibration" Pro- ceeding of Holm conf. pp-211-215 2007

[8] R.Holm Electrical Contact “Fourth edition” pp 87 [9] n. ben jemaa, j.l. queffelec, d. travers" electrical con- duction through cuas corrosion films on copper contacts"

Proceeding of the holm conference Chicago 1989.pp 147- 153

[10] E. Falcona, B. Castaing, and M. Creyssels

“Nonlinear electrical conductivity in a 1D granular me- dium” Eur. Phys. J. B 38 (2004), 475–483

[11] S. Fouvry , P. Jedrzejczyk, O. Perrinet, O. Alquier, P. Chalandon, Introduction of a “modified Archard wear law” topredict the electrical contact endurance of thin plated silver coatings subjected to fretting wear Proceed- ing of ICEC 2012 China pp 191-203

[12] N. Ben jemaa J. Swingler Correlation between Wear and electrical behavior of contact interfaces during Fret- ting vibration ICEC 2006 Sendai Japon

[13] S. Noël*, D. Alamarguy, L. Baraton “Influence of Contact Interface Composition on the Electrical and Tri- bological Properties of Nickel Electrodeposits during Fretting Tests” Proceeding of ICEC 2012 China pp-221- 227

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