• Aucun résultat trouvé

Td corrigé Complete Publications List pdf

N/A
N/A
Protected

Academic year: 2022

Partager "Td corrigé Complete Publications List pdf"

Copied!
54
0
0

Texte intégral

(1)

Publications

1973

1. M. Novotny, M.L. Lee, "Detection of Marijuana Smoke in the Atmosphere of a Room,"

Experientia 29, 1038-1039 (1973).

1974

2. M. Novotny, M.L. McConnell, M.L. Lee, "Some Aspects of High-Resolution Gas Chromatographic Analysis of Complex Volatile Samples," J. Agr. Food Chem. 22, 765- 770 (1974).

3. M. Novotny, M.L. Lee, K.D. Bartle, "Some Analytical Aspects of the Chromatographic Headspace Concentration Method Using a Porous Polymer," Chromatographia 7, 333- 338 (1974).

4. M. Novotny, M.L. Lee, K.D. Bartle, "The Methods for Fractionation, Analytical Separation and Identification of Polynuclear Aromatic Hydrocarbons in Complex Mixtures," J. Chromatogr. Sci. 12, 606-612 (1974).

5. K.D. Bartle, M.L. Lee, M. Novotny, "High-Resolution GLC Profiles of Urban Air Pollutant Polynuclear Aromatic Hydrocarbons," Intern. J. Environ. Anal. Chem. 3, 349- 356 (1974).

6. M. Novotny, M.L. McConnell, M.L. Lee, R. Farlow, "High-Resolution Gas

Chromatographic Analysis of the Volatile Constituents of Body Fluids with Use of Glass Capillary Columns," Clin. Chem. 20, 1105-1110 (1974).

7. M.J. Hartigan, J.E. Purcell, M. Novotny, M.L. McConnell, M.L. Lee, "Analytical

Performance of a Novel Nitrogen-Sensitive Detector and Its Applications with Glass Open Tubular Columns," J. Chromatogr. 99, 339 (1974).

1975

8. M.L. Lee, K.D. Bartle, M. Novotny, "Profiles of the Polynuclear Aromatic Fraction from Engine Oils Obtained by Capillary Column GLC and Nitrogen-Selective Detection," Anal.

Chem. 47, 540-543 (1975).

1976

9. M. Novotny, M.L. Lee, C.E. Low, A. Raymond, "Analysis of Marijuana Samples from Different Origins by High-Resolution Gas-Liquid Chromatography for Forensic

Application," Anal. Chem. 48, 24-29 (1976).

10. M.L. Lee, M. Novotny, K.D. Bartle, "Gas Chromatography/Mass Spectrometric and Nuclear Magnetic Resonance Spectrometric Studies of Carcinogenic Polynuclear Aromatic

(2)

Hydrocarbons in Tobacco and Marijuana Smoke Condensates," Anal. Chem. 48, 405-416 (1976).

11. M. Novotny, M.L. Lee, "A Possible Chemical Basis for the Higher Mutagenicity of Marijuana Smoke as Compared to Tobacco Smoke," Experientia 32, 280-282 (1976).

12. M. Novotny, M.L. Lee, C.E. Low, M.P. Maskarinec, "High-Resolution Gas Chromatogra- phy/Mass Spectrometric Analysis of Tobacco and Marijuana Sterols," Steroids 27, 665- 673 (1976).

13. F.I. Onuska, A.W. Wolkoff, M.E. Comba, R.H. Larose, M. Novotny, M.L. Lee, "Gas Chromatographic Analysis of Polynuclear Aromatic Hydrocarbons in Shellfish on Short, Wall-Coated Glass Capillary Columns," Anal. Letters 9, 451-460 (1976).

14. M.L. Lee, M. Novotny, K.D. Bartle, "Gas Chromatography/Mass Spectrometric and Nuclear Magnetic Resonance Determination of Polynuclear Aromatic Hydrocarbons in Airborne Particulates," Anal. Chem. 48, 1566-1572 (1976).

15. M.L. Lee, R.A. Hites, "Characterization of Sulfur-Containing Polycyclic Aromatic Compounds in Carbon Blacks," Anal. Chem. 48, 1890-1893 (1976).

16. K.D. Bartle, M.L. Lee, M. Novotny, "An Integrated Approach to the Analysis of Air- Pollutant Polynuclear Aromatic Hydrocarbons," Proc. Analyt. Div. Chem. Soc. 13, 304- 307 (1976).

1977

17. G.P. Prado, M.L. Lee, R.A. Hites, D.P. Hoult, J.B. Howard, "Soot and Hydrocarbon Formation in a Turbulent Diffusion Flame," Proc. 16th Intl. Symp. Combust., 649-661 (1977).

18. M.L. Lee, R.A. Hites, "Mixed Charge Exchange-Chemical Ionization Mass Spectrometry of Polycyclic Aromatic Hydrocarbons," J. Am. Chem. Soc. 99, 2008 (1977).

19. M.L. Lee, G.P. Prado, J.B. Howard, R.A. Hites, "Source Identification of Urban Airborne Polycyclic Aromatic Hydrocarbons by Gas Chromatographic Mass Spectrometry and High-Resolution Mass Spectrometry," Biomed. Mass Spectrom. 4, 182-186 (1977).

20. K.D. Bartle, M.L. Lee, M. Novotny, "Identification of Environmental Polynuclear Aromatic Hydrocarbons by Pulse Fourier-Transform 1H Nuclear Magnetic Resonance Spectroscopy," Analyst 102, 731-738 (1977).

1979

21. M.L. Lee, D.L. Smith, L.R. Freeman, "High-Resolution Gas Chromatographic Profiles of Volatile Organic Compounds Produced by Microorganisms at Refrigerated Temperatures,"

Appl. Environ. Microbiol. 37, 85-90 (1979).

(3)

22. M.L. Lee, D.L. Vassilaros, W.S. Pipkin, W.L. Sorenson, "Combined-Column Gas

Chromatography and Mixed Charge Exchange Chemical Ionization Mass Spectrometry of Isomeric Polycyclic Aromatic Hydrocarbons," Trace Organic Analysis: A New Frontier in Analytical Chemistry, NBS Special Publication 519, 1979, p. 731-738.

23. B.W. Wright, M.L. Lee, G.M. Booth, "Determination of Triphenyltin Hydroxide Derivatives by Capillary GC and Tin-Selective FPD," J. High Resolut.

Chromatogr./Chromatogr. Commun. 2, 189-190 (1979).

24. C.M. White, A.G. Sharkey, Jr., M.L. Lee, D.L. Vassilaros, "Some Analytical Aspects of the Quantitative Determination of Polycyclic Aromatic Hydrocarbons in Fugitive

Emissions from Coal Liquefaction Processes," Polynuclear Aromatic Hydrocarbons, P.W.

Jones and P. Leber, Eds. (Ann Arbor Science, Ann Arbor, MI, 1979), p. 261-275.

25. M.L. Lee, D.L. Vassilaros, C.M. White, M. Novotny, "Retention Indices for Programmed- Temperature Capillary Column Gas Chromatography of Polycyclic Aromatic

Hydrocarbons," Anal. Chem. 51, 768-774 (1979).

26. M.L. Lee, D.L. Vassilaros, L.V. Phillips, D.M. Hercules, H. Azumaya, J.W. Jorgenson, M.P. Maskarinec, M. Novotny, "Surface Deactivation in Glass Capillary Columns and Its Investigation by Auger Electron Spectroscopy," Anal. Letters 12, 191-203 (1979).

1980

27. M.L. Lee, C. Willey, R.N. Castle, C.M. White, "Separation and Identification of Sulfur Heterocycles in Coal-Derived Products," Polynuclear Aromatic Hydrocarbons: Chemistry and Biological Effects, A. Bjorseth and A.J. Dennis, Eds. (Battelle Press, Columbus, OH, 1980), p. 59.

28. C.M. White, M.L. Lee, "Identification and Geochemical Significance of Some Aromatic Components of Coal," Geochim. Cosmochim. Acta 44, 1825-1832 (1980).

29. M.L. Lee, B.W. Wright, "Capillary Column Gas Chromatography of Polycyclic Aromatic Compounds: A Review," J. Chromatogr. Sci. 18, 345-358 (1980).

30. M.L. Lee, B.W. Wright, "The Preparation of Glass Capillary Columns in Gas Chromatography," J. Chromatogr. 184, 235-312 (1980).

31. M. Iwao, M.L. Lee, R.N. Castle, "Synthesis of Phenanthro[b]thiophenes," J. Heterocyclic Chem. 17, 1259-1264 (1980).

32. M.L. Lee, D.M. Later, D.K. Rollins, L.D. Hansen, D.J. Eatough, "Dimethyl and

Monomethyl Sulfates: Presence in Coal Fly Ash and Airborne Particulates," Science 207, 186-188 (1980).

33. L.D. Hansen, L.R. Phillips, N.F. Mangelson, M.L. Lee, "Analytical Study of the Effluents from a High Temperature Entrained Flow Gasifier," Fuel 59, 323-330 (1980).

(4)

34. B.W. Wright, M.L. Lee, S.W. Graham, L.V. Phillips, D.M. Hercules, "Glass Surface Analytical Studies in the Preparation of Open Tubular Columns for Gas Chromatography,"

J. Chromatogr. 199, 355-369 (1980).

35. A.E. Purcell, D.W. Later, M.L. Lee, "Analysis of the Volatile Constituents of Baked, 'Jewel' Sweet Potatoes," J. Agr. Food Chem. 28, 939-941 (1980).

36. B.W. Wright, M.L. Lee, "Rapid Analysis Using Short Capillary Columns for Gas Chromatography," J. High Resolut. Chromatogr./Chromatogr. Commun. 3, 352-354 (1980).

37. F. Merli, M. Novotny, M.L. Lee, "Fractionation and Gas-Chromatographic Analysis of Aza-Arenes in Complex Mixtures," J. Chromatogr. 199, 371-378 (1980).

38. P.A. Peaden, M.L. Lee, Y. Hirata, M. Novotny, "High Performance Liquid

Chromatographic Separation of High-Molecular-Weight Polycyclic Aromatic Compounds in Carbon Black," Anal. Chem. 52, 2268-2271 (1980).

1981

39. M. Novotny, S.R. Springston, P.A. Peaden, J.C. Fjeldsted, M.L. Lee, "Capillary Supercritical Fluid Chromatography," Anal. Chem. 53, 407A-412 (1981).

40. M.L. Lee, P.A. Peaden, B.W. Wright, D.W. Later, J.C. Fjeldsted, "The Extension of Capillary Column Gas Chromatography to the Analysis of Compounds of Low Volatility,"

Proc. 4th Intl Symp. on Capillary Chromatography, R.E. Kaiser, Ed. (Hüthig, West Germany, 1981), p. 229-237.

41. R. Pratap, Y. Tominaga, M.L. Lee, R.N. Castle, "Synthesis of Pyreno[b]thiophenes," J.

Heterocyclic Chem. 18, 973-975 (1981).

42. K.D. Bartle, B.W. Wright, M.L. Lee, "Characterization of Glass, Quartz, and Fused Silica Capillary Column Surfaces from Contact Angle Measurements," Chromatographia 14, 387-396 (1981).

43. C. Willey, M. Iwao, R.N. Castle, M.L. Lee, "Determination of Sulfur Heterocycles in Coal Liquids and Shale Oils," Anal. Chem. 53, 400-407 (1981).

44. D.W. Later, B.W. Wright, M.L. Lee, "Construction of an Efficient Fused Silica Capillary Column Effluent Splitter for Gas Chromatography," J. High Resolut.

Chromatogr./Chromatogr. Commun. 4, 406-408 (1981).

45. Y. Tominaga, M.L. Lee, R.N. Castle, "Synthesis of Anthra[b]thiophenes and Benzo[b]naphtho[d]-thiophenes," J. Heterocyclic Chem. 18, 967-972 (1981).

46. B.W. Wright, K.D. Bartle, M.L. Lee, "Surface Characterization of Fused Silica, Quartz, and Glass Capillary Columns from Contact Angle Measurements," Proc. 4th Intl Symp. on Capillary Chromatography, R.E. Kaiser, Ed. (Hüthig, West Germany, 1981), p. 505-522.

(5)

47. D.W. Later, M.L. Lee, K.D. Bartle, R.C. Kong, D.L. Vassilaros, "Chemical Class

Separation and Characterization of Organic Compounds in Synthetic Fuels," Anal. Chem.

53, 1612-1620 (1981).

48. D.J. Eatough, M.L. Lee, D.W. Later, B.E. Richter, N.L. Eatough, L.D. Hansen, "Dimethyl Sulfate in Particulate Matter from Coal- and Oil-Fired Power Plants," Environ. Sci.

Technol. 15, 1502-1506 (1981).

49. Y. Tominaga, M.L. Lee, R.N. Castle, "Synthesis of Phenaleno[1,9-bc]thiophene," J.

Heterocyclic Chem. 18, 977-979 (1981).

50. K.D. Bartle, M.L. Lee, S.A. Wise, "Factors Affecting the Retention of Polycyclic Aromatic Hydrocarbons in Gas Chromatography," Chromatographia 14, 69-72 (1981).

51. R.D. Thompson, M. Iwao, M.L. Lee, R.N. Castle, "Synthesis of

Benzo[3,2]phenanthro[4,5-bcd]thiophene and Chryseno[4,5-bcd]thiophene," J.

Heterocyclic Chem. 18, 981-984 (1981).

52. Y. Hirata, M. Novotny, P.A. Peaden, M.L. Lee, "A Comparison of Capillary

Chromatographic Techniques for the Separation of Very Large Polycyclic Aromatic Molecules," Anal. Chim. Acta 127, 55-61 (1981).

53. R. Pratap, M.L. Lee, R.N. Castle, "Synthesis of Triphenyleno[b]thiophenes," J.

Heterocyclic Chem. 18, 1457-1459 (1981).

54. F. Merli, D. Wiesler, M.P. Maskarinec, M. Novotny, D.L. Vassilaros, M.L. Lee,

"Characterization of the Basic Fraction of Marijuana Smoke by Capillary Gas Chromatography/Mass Spectrometry," Anal. Chem. 53, 1929-1935 (1981).

55. M.L. Lee, K.D. Bartle, "The Chemical Analysis of Particulate Carbon," Proc. Symp.

Particulate Carbon: Formation During Combustion, D.C. Siegla and G.W. Smith, Eds.

(Plenum Press, New York, 1981), p. 91-106.

56. K.D. Bartle, M.L. Lee, S.A. Wise, "Modern Analytical Methods for Environmental Polycyclic Aromatic Compounds," Chem. Soc. Rev. 10, 113-158 (1981).

1982

57. D.W. Later, M.L. Lee, B.W. Wilson, "Selective Detection of Amino Polycyclic Aromatic Hydrocarbons in Solvent Refined Coal," Anal. Chem. 54, 117-123 (1982).

58. R. Pratap, M.L. Lee, R.N. Castle, "Synthesis of Benzo[b]phenanthro[d]thiophenes," J.

Heterocyclic Chem. 19, 219-220 (1982).

59. B.T. Pittard, L.R. Freeman, D.W. Later, M.L. Lee, "Identification of Volatile Organic Compounds Produced by Fluorescent Psuedomonads on Chicken Breast Muscle," Appl.

Environ. Microbiol. 43, 1504-1506 (1982).

(6)

60. P.A. Peaden, B.W. Wright, M.L. Lee, "The Preparation of Non-Extractable Methyl- phenylpolysiloxane Stationary Phases for Capillary Column Gas Chromatography,"

Chromatographia 15, 335-340 (1982).

61. P.A. Peaden, M.L. Lee, "Supercritical Fluid Chromatography: Methods and Principles," J.

Liquid Chromatogr. 5, 179-221 (1982).

62. D.L. Vassilaros, P.W. Stoker, G.M. Booth, M.L. Lee, "Capillary Gas Chromatographic Determination of Polycyclic Aromatic Compounds in Vertebrate Fish Tissue," Anal.

Chem. 54, 106-112 (1982).

63. D.W. Later, M.L. Lee, R.A. Pelroy, B.W. Wilson, "Identification and Mutagenicity of Nitrogen-Containing Polycyclic Aromatic Compounds in Synthetic Fuels," in Polynuclear Aromatic Hydrocarbons: Physical and Biological Chemistry, M. Cooke, A.J. Dennis, and G.L. Fisher, Eds. (Battelle Press, Columbus, OH, 1982), p. 427-438.

64. R. Pratap, R.N. Castle, and M.L. Lee, "Synthesis of Benzo[1,2]phenaleno[bc]thiophenes,"

J. Heterocyclic Chem. 19, 439-441 (1982).

65. B.W. Wright, P.A. Peaden, M.L. Lee, T.J. Stark, "Free Radical Crosslinking in the Preparation of Non-Extractable Stationary Phases for Capillary Gas Chromatography," J.

Chromatogr. 248, 17-34 (1982).

66. P.A. Peaden, J.C. Fjeldsted, M.L. Lee, S.R. Springston, M. Novotny, "Instrumental Aspects of Capillary Supercritical Fluid Chromatography," Anal. Chem. 54, 1090-1093 (1982).

67. D.L. Vassilaros, D.A. Eastmond, W.R. West, G.M. Booth, M.L. Lee, "Determination and Bioconcentration of Polycyclic Aromatic Sulfur Heterocycles in Aquatic Biota," in Polynuclear Aromatic Hydrocarbons: Physical and Biological Chemistry, M. Cooke, A.J.

Dennis, and G.L. Fisher, Eds. (Battelle Press, Columbus, OH, 1982), p. 845-857.

68. B.W. Wilson, C. Willey, D.W. Later, M.L. Lee, "Effects of Process Distillation on the Distribution of Amino Polycyclic Aromatic Hydrocarbons in Refined Coal Derived Liquids," Fuel 61, 473-477 (1982).

69. Y. Tominaga, R. Pratap, R.N. Castle, M.L. Lee, "The Synthesis of the Monomethyl Isomers of Benzo[b]naphtho[2,1-d]thiophene," J. Heterocyclic Chem. 19, 859-863 (1982).

70. B.W. Wright, P.A. Peaden, G.M. Booth, M.L. Lee, "Determination of Surface Hydroxyl Concentration on Glass and Fused Silica Capillary Columns," Chromatographia 15, 584- 586 (1982).

71. R.D. Smith, W.D. Felix, J.C. Fjeldsted, M.L. Lee, "Capillary Column Supercritical Fluid Chromatography-Mass Spectrometry," Anal. Chem. 54, 1883-1885 (1982).

(7)

72. M.L. Lee, D.L. Vassilaros, D.W. Later, "Capillary Column Gas Chromatography of Environmental Polycyclic Aromatic Compounds," Intern. J. Environ. Anal. Chem. 11, 251-262 (1982).

73. R.C. Kong, M.L. Lee, Y. Tominaga, R. Pratap, M. Iwao, R.N. Castle, S.A. Wise,

"Capillary Column Gas Chromatographic Resolution of Isomeric Polycyclic Aromatic Sulfur Heterocycles in a Coal Liquid," J. Chromatogr. Sci. 20, 502-510 (1982).

74. R. Pratap, Y. Tominaga, R.N. Castle, M.L. Lee, "The Synthesis of the Monomethyl Derivatives of Benzo[b]naphtho[2,3-d]thiophene," J. Heterocyclic Chem. 19, 865869 (1982).

75. B.W. Wright, P.A. Peaden, M.L. Lee, "Effect of Viscosity on Stationary Phase Stability in Capillary Column Gas Chromatography," J. High Resolut. Chromatogr./Chromatogr.

Commun. 5, 413-416 (1982).

76. R.D. Smith, J.C. Fjeldsted, M.L. Lee, "A Direct Fluid Injection Interface for Capillary Supercritical Fluid Chromatography-Mass Spectrometry," J. Chromatogr. 247, 231-243 (1982).

77. R.C. Kong, M.L. Lee, Y. Tominaga, R. Pratap, M. Iwao, R.N. Castle, "Mesogenic Polysiloxane Stationary Phase for High Resolution Gas Chromatography of Isomeric Polycyclic Aromatic Compounds," Anal. Chem. 54, 1802-1866 (1982).

78. Y. Tominaga, R. Pratap, R.N. Castle, M.L. Lee, "Synthesis of All of the Monomethyl Isomers of Benzo[b]naphtho[1,2-d]thiophene," J. Heterocyclic Chem. 19, 871-877 (1982).

79. D.L. Vassilaros, R.C. Kong, D.W. Later, M.L. Lee, "Linear Retention Index System for Polycyclic Aromatic Compounds: Critical Evaluation and Additional Indices," J.

Chromatogr. 252, 1 -20 (1982).

80. Y. Tominaga, R.N. Castle, M.L. Lee, "Synthesis of Benzo[4,5]phenaleno[1,9-

bc]thiophene and Benzo[4,5]phenaleno[9,1-bc]thiophene," J. Heterocyclic Chem. 19, 1125-1130 (1982).

81. D.L. Vassilaros, P.W. Stoker, G.M. Booth, M.L. Lee, "Capillary Gas Chromatographic Determination of Polycyclic Aromatic Compounds in Vertebrate Fish," Anal. Chem. 54, 106-112 (1982).

1983

82. R.D. Smith, J.C. Fjeldsted, M.L. Lee, "Supercritical Fluid Chromatography-Mass Spectrometry," Intern. J. Mass Spectrom. Ion Physics 46, 217-220 (1983).

83. B.E. Richter, J.C. Kuei, J.I. Shelton, L.W. Castle, J.S. Bradshaw, M.L. Lee, "Polysiloxane Stationary Phases Containing Tolyl and Cyanopropyl Groups: Oxidation During

Crosslinking," J. Chromatogr. 279, 21-30 (1983).

(8)

84. D.W. Later, R.A. Pelroy, D.D. Mahlum, C.W. Wright, M.L. Lee, W.C. Weimer, B.W.

Wilson, "Identification and Comparative Genotoxicity of Polycyclic Aromatic

Hydrocarbons and Related Nitrogen-Containing Heteroatomic Species in Products from Coal Liquefaction Processes," in Polynuclear Aromatic Hydrocarbons: Formation, Metabolism and Measurement, M. Cooke, A.J. Dennis, Eds. (Battelle Press, Columbus, OH, 1983), p. 771-784.

85. E.V. Bowman, L.R. Freeman, D.W. Later, M.L. Lee, "Comparison of Volatiles Produced by Selected Pseudomonads on Chicken Skin," J. Food Sci. 48, 1358-1359 (1983).

86. Y. Tominaga, M.L. Tedjamulia, R.N. Castle, M.L. Lee, "Synthesis of All of the

Monomethyl Isomers of Naphtho[2,1-b]thiophene," J. Heterocyclic Chem. 20, 487-490 (1983).

87. R.A. Pelroy, D.L. Stewart, Y. Tominaga, M. Iwao, R.N. Castle, M.L. Lee, "Microbial Mutagenicity of Three- and Four-Ring Polycyclic Aromatic Sulfur Heterocycles,"

Mutation Res. 117, 31-40 (1983).

88. J.C. Fjeldsted, W.P. Jackson, P.A. Peaden, M.L. Lee, "Density Programming in Capillary Supercritical Fluid Chromatography," J. Chromatogr. Sci. 21, 222-225 (1983).

89. B.E. Richter, J.C. Kuei, N.J. Park, S.J. Crowley, J.S. Bradshaw, M.L. Lee, "Azo Compounds for Free Radical Crosslinking of Polysiloxane Stationary Phases," J. High Resolut. Chromatogr./Chromatogr. Commun. 6, 371-374 (1983).

90. D.W. Later, T.G. Andros, M.L. Lee, "Isolation and Identification of Amino Polycyclic Aromatic Hydrocarbons from Coal Derived Products," Anal. Chem. 55, 2126-2132 (1983).

91. M.L. Tedjamulia, Y. Tominaga, R.N. Castle, M.L. Lee, "Synthesis of Benzo-

[b]phenanthro[d]thiophenes and Anthra[b]benzo[d]thiophenes," J. Heterocyclic Chem. 20, 861-866 (1983).

92. S.A. Wise, R.M. Campbell, W.E. May, M.L. Lee, R.N. Castle, "Normal and Reversed- Phase Liquid Chromatographic Separations of Polycyclic Aromatic Sulfur Heterocycles,"

in Polynuclear Aromatic Hydrocarbons: Formation, Metabolism and Measurement, M.

Cooke and A.J. Dennis, Eds. (Battelle Press, Columbus, OH, 1983), p. 1247-1266.

93. P.A. Peaden, M.L. Lee, "Theoretical Treatment of Resolving Power in Open Tubular Supercritical Fluid Chromatography," J. Chromatogr. 259, 1-16 (1983).

94. R.C. Kong, M.L. Lee, "Static Coating of Small Diameter Capillary Columns at Elevated Temperatures," J. High Resolut. Chromatogr./Chromatogr. Commun. 6, 319-322 (1983).

95. D.W. Later, M.L. Lee, "Chromatographic Methods for the Chemical and Biological Characterization of Polycyclic Aromatic Compounds in Synfuel Materials," Advanced Techniques in Synthetic Fuels Analysis, C.W. Wright, W.C. Weimer, and W.D. Felix, Eds.

(U.S. DOE Technical Information Center, Washington, DC, 1983), p. 44-73.

(9)

96. M.L. Tedjamulia, Y. Tominaga, R.N. Castle, M.L. Lee, "The Synthesis of Dinaphthothiophenes," J. Heterocyclic Chem. 20, 1143-1148 (1983).

97. D.A. Eastmond, C.M. Muehle, R.L. Price, C.A. Hutchens, G.M. Booth, M.L. Lee, "Acute Toxicity, Bioconcentration, and Elimination of a Coal Liquid in Freshwater Organisms,"

Polynuclear Aromatic Hydrocarbons: Formation, Metabolism and Measurement, M.

Cooke and A.J. Dennis, Eds. (Battelle Press, Columbus, OH, 1983), p. 451-469.

98. J.C. Fjeldsted, B.E. Richter, W.P. Jackson, M.L. Lee, "Scanning Fluorescence Detection in Capillary Supercritical Fluid Chromatography," J. Chromatogr. 269, 423-430 (1983).

99. R.C. Kong, M.L. Lee, "Static Coating of Capillary Columns Using Mixed Solvents,"

Chromatographia 17, 451-454 (1983).

100. M.L. Tedjamulia, Y. Tominaga, R.N. Castle, M.L. Lee, "The Synthesis of Phenanthro[4,5- bcd]thiophene and the Four Monomethylphenanthro[4,5-bcd]thiophenes," J. Heterocyclic Chem. 20, 1149-1152 (1983).

101. M.L. Lee, "High Resolution Supercritical Fluid Chromatography," Physics Bull. 34, 370- 371 (1983).

102. B.E. Richter, J.C. Kuei, L.W. Castle, B.A. Jones, J.S. Bradshaw, M.L. Lee,

"Nonextractable Cyanopropyl Polysiloxane Stationary Phases for Capillary Chromatography," Chromatographia 17, 570-573 (1983).

103. R.N. Castle, M. Iwao, Y. Tominaga, R. Pratap, R.D. Thompson, M.L. Lee, "The Synthesis of Potentially Mutagenic Polycyclic Aromatic Thiophenes and Their Methyl Derivatives via the Wadsworth-Emmons Reaction Followed by Photocyclization," Polynuclear Aromatic Hydrocarbons: Formation, Metabolism and Measurement, M. Cooke and A.J.

Dennis, Eds. (Battelle Press, Columbus, OH, 1983), p. 269-281.

104. J.C. Fjeldsted, R.C. Kong, M.L. Lee, "Capillary Supercritical Fluid Chromatography with Conventional Flame Detectors," J. Chromatogr. 279, 449-455 (1983).

105. M. Tedjamulia, Y. Tominaga, M.L. Lee, R.N. Castle, "The Synthesis of Potentially Mutagenic Polycyclic Aromatic Amines," in Polynuclear Aromatic Hydrocarbons:

Formation, Metabolism and Measurement, M. Cooke and A.J. Dennis, Eds. (Battelle Press, Columbus, OH, 1983), p. 1161-1172.

106. M.L. Tedjamulia, Y. Tominaga, R.N. Castle, M.L. Lee, "The Synthesis of All of the Dimethyldibenzothiophenes and Monoethyldibenzothiophenes," J. Heterocyclic Chem. 20, 1485-1495 (1983).

107. G.E. Martin, S.L. Smith, W.J. Layton, M.R. Willcott, III, M. Iwao, M.L. Lee, R.N. Castle,

"Assignment of the 1H and 13C-NMR Spectra of Phenanthro[1,2-b]thiophene Through the Concerted Application of Two-Dimensional NMR Spectroscopic Techniques," J.

Heterocyclic Chem. 20, 1367-1381 (1983).

(10)

108. M. Sugiura, M.L. Tedjamulia, Y. Tominaga, R.N. Castle, M.L. Lee, "The Synthesis of the Monomethylbenzo[2,3]phenanthro[4,5-bcd]thiophenes," J. Heterocyclic Chem. 20, 1453- 1459 (1983).

109. M.J. Musmar, M.R. Willcott, III, G.E. Martin, R.T. Gampe, Jr., M. Iwao, M.L. Lee, R.E.

Hurd, L.F. Johnson, R.N. Castle, "Auto-correlated 13C13C Double Quantum Coherence Two-Dimensional NMR Spectroscopy: Utilization of a Modified Version of the Technique as an Adjunct in the Total Assignment of the 1H and 13C NMR Spectra of the Mutagen Phenanthro[3,4-b]thiophene," J. Heterocyclic Chem. 20, 1661-1669 (1983).

1984

110. R.C. Kong, M.L. Lee, M. Iwao, Y. Tominaga, R. Pratap, R.D. Thompson, R.N. Castle,

"Determination of Sulfur Heterocycles in Selected Synfuels," Fuel 63, 702-708 (1984).

111. D.A. Eastmond, G.M. Booth, M.L. Lee, "Toxicity, Accumulation, and Elimination of Polycyclic Aromatic Sulfur Heterocycles in Daphnia Magna," Arch. Environ. Contam.

Toxicol. 13, 105-111 (1984).

112. M.L. Lee, R.C. Kong, C.L. Woolley, J.S. Bradshaw, "Fused Silica Capillary Column Technology for Gas Chromatography," J. Chromatogr. Sci. 22, 136-142 (1984).

113. J.C. Fjeldsted, M.L. Lee, "Capillary Supercritical Fluid Chromatography," Anal. Chem.

56, 619A-624 (1984).

114. R.M. Campbell, M.L. Lee, "Capillary Column Gas Chromatographic Determination of Nitro Polycyclic Aromatic Compounds in Particulate Extracts," Anal. Chem. 56, 1026- 1030 (1984).

115. J.C. Kuei, J.I. Shelton, L.W. Castle, R.C. Kong, J.S. Bradshaw, M.L. Lee, "Polarizable Biphenyl Polysiloxane Stationary Phase for Capillary Column Gas Chromatography," J.

High Resolut. Chromatogr./Chromatogr. Commun. 7, 13-18 (1984).

116. S.M. Fields, R.C. Kong, J.C. Fjeldsted, M.L. Lee, P.A. Peaden, "Effect of Column Diameter on Efficiency in Capillary Supercritical Fluid Chromatography," J. High Resolut. Chromatogr./Chromatogr. Commun. 7, 312-318 (1984).

117. H. Kudo, M.L. Tedjamulia, R.N. Castle, M.L. Lee, "Angular Polycyclic Thiophenes Containing Two Thiophene Rings. I.," J. Heterocyclic Chem. 21, 185-192 (1984).

118. G.M. Booth, J.R. Larsen, M.L. Lee, "The Environmental Effects of Fossil Fuels: A Global Perspective," Proc. Intl Conf. Environ. Contam. (London, July 1984), p. 606-610.

119. R.C. Kong, S.M. Fields, W.P. Jackson, M.L. Lee, "Preparation of Small Diameter

Capillary Columns for Gas and Supercritical Fluid Chromatography," J. Chromatogr. 289, 105-116 (1984).

(11)

120. J.S. Bradshaw, S.J. Crowley, C.W. Harper, M.L. Lee, "Autocrosslinkable Methyl-2- phenylethylpolysiloxane Stationary Phase for Capillary Column Gas Chromatography," J.

High Resolut. Chromatogr./Chromatogr. Commun. 7, 89-92 (1984).

121. S.M. Fields, R.C. Kong, M.L. Lee, P.A. Peaden, "Effect of Stationary Phase Film Thickness on Efficiency in Capillary Supercritical Fluid Chromatography," J. High Resolut. Chromatogr./Chromatogr. Commun. 7, 423-428 (1984).

122. M.J. Musmar, R.T. Gampe, Jr., G.E. Martin, W.J. Layton, S.L. Smith, R.D. Thompson, M. Iwao, M.L. Lee, R.N. Castle, "Combined Application of Auto-Correlated (COSY) and Homonuclear J-Resolved Two-Dimensional NMR Spectra for the Assignment of

Congested, Non-First Order Spectra of Polycyclic Aromatic Systems: Assignment of the

1H-1H Spin-Coupling Constants," J. Heterocyclic Chem. 21, 225-233 (1984).

123. M.J. Musmar, G.E. Martin, M.L. Tedjamulia, H. Kudo, R.N. Castle, M.L. Lee, "Two- Dimensional Relayed Coherence Transfer Experiments as a Means of Subgrouping Protonated Carbon Resonances of Complex Polynuclear Heteroaromatics on the Basis of Vicinal Proton-Proton Connectivities," J. Heterocyclic Chem. 21, 929-933 (1984).

124. R.N. Castle, M.L. Tedjamulia, Y. Tominaga, R. Pratap, M. Sugiura, H. Kudo, M.L. Lee, M. Iwao, R.D. Thompson, G.E. Martin, R.T. Gampe, Jr., M.J. Musmar, S.L. Smith, W.J.

Layton, R.E. Hurd, L.F. Johnson, "The Synthesis and Properties of Polycyclic Aromatic Thiophenes and Related Heterocycles Occurring in Coal-derived Products," Lectures in Heterocyclic Chemistry 7, 1-52 (1984).

125. T. McFall, G.M. Booth, M.L. Lee, Y. Tominaga, R. Pratap, M. Tedjamulia, R.N. Castle,

"Mutagenic Activity of Methyl-Substituted Tri- and Tetracyclic Aromatic Sulfur Heterocycles," Mutation Res. 135, 97-103 (1984).

126. R.C. Kong, C.L. Woolley, S.M. Fields, M.L. Lee, "Deactivation of Small Diameter Fused Silica Capillary Columns for Gas and Supercritical Fluid Chromatography,"

Chromatographia 18, 362-366 (1984).

127. C.L. Woolley, R.C. Kong, B.E. Richter, M.L. Lee, "Deactivation of Fused Silica Capillary Columns with Polymethylhydrosiloxanes," J. High Resolut. Chromatogr./Chromatogr.

Commun. 7, 329-332 (1984).

128. W.P. Jackson, B.E. Richter, J.C. Fjeldsted, R.C. Kong, M.L. Lee, "High Resolution Supercritical Fluid Chromatography," Ultrahigh Resolution Chromatography, ACS Symposium Series 250, S. Ahuja, Ed. (American Chemical Society, Washington, DC, 1984), p. 121-133.

129. M.L. Tedjamulia, H. Kudo, R.N. Castle, M.L. Lee, "Angular Polycyclic Thiophenes Containing Two Thiophene Rings. Part II," J. Heterocyclic Chem. 21, 321-325 (1984).

130. M.L. Tedjamulia, J.G. Stuart, Y. Tominaga, R.N. Castle, M.L. Lee, "The Synthesis of Naphtho[1,2-b]thiophene and All of the Eight Isomers of Monomethylnaphtho[1,2-b]

thiophene," J. Heterocyclic Chem. 21, 1215-1219 (1984).

(12)

131. D.W. Later, T. McFall, G.M. Booth, M.L. Lee, M. Tedjamulia, R.N. Castle,

"Mutagenicity of Isomeric Two-, Three-, and Four-Ring Amino Polycyclic Aromatic Hydrocarbons," Environ. Mutagenesis 6, 497-515 (1984).

132. B.A. Jones, J.C. Kuei, J.S. Bradshaw, M.L. Lee, "Cyanopropyl Polysiloxane Stationary Phases for Gas Chromatography: Characterization and Evaluation," J. Chromatogr. 298, 389-397 (1984).

133. H. Kudo, M.L. Tedjamulia, R.N. Castle, M.L. Lee, "The Synthesis of Phenanthrodibenzo- thiophenes," J. Heterocyclic Chem. 21, 1833-1839 (1984).

134. M.L. Lee, J.C. Kuei, N.W. Adams, B.J. Tarbet, M. Nishioka, B.A. Jones, J.S. Bradshaw,

"Polarizable Polysiloxane Stationary Phases for Capillary Column Gas Chromatography,"

J. Chromatogr. 302, 303-318 (1984).

135. L. Baldwin, M.L. Tedjamulia, J.C. Stuart, R.N. Castle, M.L. Lee, "The Synthesis of Polycyclic Thiophenes Derived from Phenanthrene Intermediates," J. Heterocyclic Chem.

21, 1775-1779 (1984).

136. B.A. Jones, J.S. Bradshaw, M. Nishioka, M.L. Lee, "The Synthesis of Smectic Liquid- Crystalline Polysiloxanes from Biphenylcarboxylate Esters and Their Use as Stationary Phases for High Resolution Gas Chromatography," J. Org. Chem. 49, 4947-4951 (1984).

137. H. Kudo, R.N. Castle, M.L. Lee, "Synthesis of Monomethyl Isomers of

Naphtho[1,2:4,5]thieno[2,3-c]quinoline," J. Heterocyclic Chem. 21, 1761-1764 (1984).

1985

138. M. Nishioka, J.S. Bradshaw, M.L. Lee, Y. Tominaga, M. Tedjamulia, R.N. Castle,

"Capillary Column Gas Chromatography of Sulfur Heterocycles in Heavy Oils and Tars Using a Biphenylpolysiloxane Stationary Phase," Anal. Chem. 57, 309-312 (1985).

139. W.P. Jackson, R.C. Kong, M.L. Lee, "Capillary Supercritical Fluid Chromatography of Polynuclear Aromatic Compounds," Polynuclear Aromatic Hydrocarbons: Mechanisms, Methods, and Metabolism, M. Cooke and A.J. Dennis, Eds. (Battelle Press, Columbus, OH, 1985), p. 609-625.

140. P.W. Stoker, M.R. Plasterer, R.L. McDowell, R. Campbell, S. Fields, R. Price, C. Muehle, W.R. West, G.M. Booth, J.R. Larsen, M.L. Lee, "Effects of Coal-Derived Tars on

Selected Aquatic and Mammalian Organisms," Polynuclear Aromatic Hydrocarbons:

Mechanisms, Methods, and Metabolism, M. Cooke and A.J. Dennis, Eds. (Battelle Press, Columbus, OH, 1985), p. 1239-1257.

141. M.J. Musmar, G.E. Martin, R.T. Gampe, Jr., M.L. Lee, R.E. Hurd, M.L. Tedjamulia, H.

Kudo, R.N. Castle, "Assignment of the 13C-NMR Spectrum of Phenanthro[4,3-

a]dibenzothiophene Through the Utilization of Two Dimensional Relayed Coherence

(13)

Transfer and Double Quantum Coherence Spectroscopy," J. Heterocyclic Chem. 22, 219- 223 (1985).

142. J.C. Kuei, B.J. Tarbet, W.P. Jackson, J.S. Bradshaw, K.E. Markides, M.L. Lee, "n- Octylmethylpolysiloxane Stationary Phase for Capillary Column Gas and Supercritical Fluid Chromatography," Chromatographia 20, 25-30 (1985).

143. M. Nishioka, M.L. Lee, H. Kudo, D.R. Muchiri, L.J. Baldwin, S. Pakray, J.G. Stuart, R.N.

Castle, "Determination of Hydroxylated Thiophenic Compounds in a Coal Liquid," Anal.

Chem. 57, 1327-1330 (1985).

144. S.M. Fields, M.L. Lee, "Effects of Density and Temperature on Efficiency in Capillary Supercritical Fluid Chromatography," J. Chromatogr. 349, 305-316 (1985).

145. W.R. West, P.A. Smith, P.W. Stoker, G.M. Booth, T. Smith-Oliver, B.E. Butterworth, M.L. Lee, "Analysis and Genotoxicity of a PAC-Polluted River Sediment," in Polynuclear Aromatic Hydrocarbons: Mechanisms, Methods, and Metabolism, M. Cooke, A.J. Dennis, Eds. (Battelle Press, Columbus, OH, 1985), p. 1395-1411.

146. H. Kudo, R.N. Castle, M.L. Lee, "Synthesis of Monoamino and Monohydroxy- dibenzothiophenes," J. Heterocyclic Chem. 22, 215-218 (1985).

147. K.E. Markides, M. Nishioka, B.J. Tarbet, J.S. Bradshaw, M.L. Lee, "Smectic

Biphenylcarboxylate Ester Liquid-Crystalline Polysiloxane Stationary Phase for Capillary Gas Chromatography," Anal. Chem. 57, 1296-1299 (1985).

148. M. Nishioka, R.M. Campbell, W.R. West, P.A. Smith, G.M. Booth, M.L. Lee, H. Kudo, R.N. Castle, "Determination of Aminodibenzothiophenes in a Coal Liquid," Anal. Chem.

57, 1868-1871 (1985).

149. P.W. Stoker, J.R. Larsen, G.M. Booth, M.L. Lee, "Pathology of Gill and Liver Tissues from Two Genera of Fishes Exposed to Two Coal-Derived Materials," J. Fish Biol. 27, 31-46 (1985).

150. H. Kudo, R.N. Castle, and M.L. Lee, "Synthesis of the Isomeric Monomethyl Derivatives of the Novel Naphtho[2,1:4,5]thieno[2,3-c]quinoline Ring System," J. Heterocyclic Chem. 22, 211-214 (1985).

151. J.S. Bradshaw, N.W. Adams, R.S. Johnson, B.J. Tarbet, C.M. Schregenberger, M.A.

Pulsipher, M.B. Andrus, K.E. Markides, M.L. Lee, "Preparation of Polysiloxane

Stationary Phases for Capillary Column Chromatography: A New Methoxyphenyl Phase,"

J. High Resolut. Chromatogr./Chromatogr. Commun. 8, 678-683 (1985).

152. M. Nishioka, R.M. Campbell, M.L. Lee, D.R. Muchiri, J.G. Stuart, R.N. Castle, "Isolation and Determination of Hydroxylated Nitrogen Heterocycles in a Coal Liquid," Anal. Chem.

57, 2211-2215 (1985).

(14)

153. M.J. Musmar, G.E. Martin, R.T. Gampe, Jr., V.M. Lynch, S.H. Simonsen, M.L. Lee, M.L.

Tedjamulia, R.N. Castle, "1-Methylphenanthro[3,4-b]thiophene: Determination of the Tertiary Structure in the Solution and Crystalline States by NMR Spectroscopy and X-Ray Diffraction," J. Heterocyclic Chem. 22, 545-553 (1985).

154. K.E. Markides, B.J. Tarbet, C.L. Woolley, C.M. Schregenberger, J.S. Bradshaw, M.L.

Lee, K.D. Bartle, "Deactivation of Fused Silica Capillary Columns with

Phenylhydrosiloxanes," J. High Resolut. Chromatogr./Chromatogr. Commun. 8, 378-384 (1985).

155. D.W. Later, B.W. Wilson, M.L. Lee, "Standardization of Alumina and Silica Adsorbents Used for Chemical Class Separation of Polycyclic Aromatic Compounds," Anal. Chem.

57, 2979-2984 (1985).

156. M.J. Quast, E.L. Ezell, G.E. Martin, M.L. Lee, M.L. Tedjamulia, J.G. Stuart, R.N. Castle,

"Long Range Optimized Two-Dimensional Proton-Carbon Chemical Shift Correlation.

Application in the Total Assignment of the 1H- and 13C-NMR Spectra of 9-

Methylphenanthro[4,3-a]dibenzothiophene," J. Heterocyclic Chem. 22, 1453-1459 (1985).

157. K.E. Markides, H-C.K. Chang, C.M. Schregenberger, B.J. Tarbet, J.S. Bradshaw, M.L.

Lee, "Evaluation of Smectic Biphenylcarboxylate Ester Liquid-Crystalline Polysiloxane Stationary Phases for Capillary Column Chromatography," J. High Resolut.

Chromatogr./Chromatogr. Commun. 8, 516-520 (1985).

158. L.J. Baldwin, S. Pakray, R.N. Castle, M.L. Lee, "The Synthesis of Hydroxyphenyl- thiophenes," J. Heterocyclic Chem. 22, 1667-1167 (1985).

159. K.E. Markides, B.J. Tarbet, C.M. Schregenberger, J.S. Bradshaw, K.D. Bartle, M.L. Lee,

"Deactivation of Fused Silica Capillary Columns with Cyanopropylhydrosiloxanes," J.

High Resolut. Chromatogr./Chromatogr. Commun. 8, 741-747 (1985).

1986

160. J.G. Stuart, M.J. Quast, G.E. Martin, V.M. Lynch, S.H. Simonsen, M.L. Lee, R.N. Castle, J.L. Dallas, B.K. John, L.F. Johnson, "Benzannelated Analogs of Phenanthro[1,2-b]- and [2,1-b]thiophene: Synthesis and Structural Characterization by Two-Dimensional Nmr and X-Ray Techniques," J. Heterocyclic Chem. 23, 1215-1234 (1986).

161. M. Nishioka, R.M. Campbell, M.L. Lee, R.N. Castle, "Isolation of Sulfur Heterocycles from Petroleum and Coal-Derived Materials by Ligand Exchange Chromatography," Fuel 65, 270-273 (1986).

162. M.L. Lee, S.R. Goates, K.E. Markides, S.A. Wise, "Frontiers in Analytical Techniques for PAH," in Polynuclear Aromatic Hydrocarbons: Chemistry, Characterization, and

Carcinogenesis, M. Cooke, A.J. Dennis, Eds. (Battelle Press, Columbus, OH, 1986), p. 13- 37.

(15)

163. K.E. Markides, E.D. Lee, R. Bolick, M.L. Lee, "Capillary Supercritical Fluid

Chromatography with Dual-Flame Photometric Detection," Anal. Chem. 58, 740-743 (1986).

164. G.M. Booth, D. Alder, M.L. Lee, M.W. Carter, R.C. Whitmore, R.E. Seegmiller,

"Environmental Fate and Properties of 1-(4-chlorophenyl)3-(2,6-difluorobenzoyl)urea (Diflubenzuron, Dimilin),"Benzoylphenylureas, J.E. Wright, Ed. (Plenum Press, New York, 1986), p. 141-204.

165. J.S. Bradshaw, R.S. Johnson, N.W. Adams, M.A. Pulsipher, K.E. Markides, M.L. Lee,

"New Polar-Substituted Phenyl Siloxane Monomers and Polymers for Capillary Gas Chromatography," J. Chromatogr. 357, 69-78 (1986).

166. M.J. Quast, G.E. Martin, V.M. Lynch, S.H. Simonsen, J.G. Stuart, M.L. Tedjamulia, R.N.

Castle, M.L. Lee, "The Crystal and Molecular Structure of 9-Methylphenanthro[4,3- a]dibenzothiophene," J. Heterocyclic Chem. 23, 1115-1118 (1986).

167. M. Nishioka, M.L. Lee, "Sulfur Heterocycles in Coal-Derived Products: Relation Between Structure and Abundance," Fuel 65, 390-396 (1986).

168. S.A. Wise, R.M. Campbell, W.R. West, M.L. Lee, K.D. Bartle, "Characterization of Polycyclic Aromatic Hydrocarbon Minerals Curtisite, Idrialite, and Pendletonite Using High-Performance Liquid Chromatography, Gas Chromatography, Mass Spectrometry, and Nuclear Magnetic Resonance Spectroscopy," Chem. Geology 54, 339-357 (1986).

169. W.P. Jackson, K.E. Markides, M.L. Lee, "Supercritical Fluid Injection of High-Molecular- Weight Polycyclic Aromatic Compounds in Capillary Supercritical Fluid

Chromatography," J. High Resolut. Chromatogr./Chromatogr. Commun. 9, 213-217 (1986).

170. M. Nishioka, B.J. Jones, B.J. Tarbet, J.S. Bradshaw, M.L. Lee, "Gas Chromatographic Retention Behavior of Polycyclic Aromatic Compounds on Smectic Liquid-Crystalline Polysiloxane Stationary Phases," J. Chromatogr. 357, 79-91 (1986).

171. M. Nishioka, P.A. Smith, G.M. Booth, M.L. Lee, H. Kudo, D.R. Muchiri, R.N. Castle, L.H. Klemm, "Determination and Mutagenic Activity of Nitrogen-Containing Thiophenic Compounds in Coal-Derived Products," Fuel 65, 711-714 (1986).

172. W.R. West, S.A. Wise, R.M. Campbell, K.D. Bartle, M.L. Lee, "The Analysis of

Polycyclic Aromatic Hydrocarbon Minerals Curtisite and Idrialite by High Resolution Gas and Liquid Chromatographic Techniques," Polynuclear Aromatic Hydrocarbons:

Chemistry, Characterization, and Carcinogenesis, M. Cooke and A.J. Dennis, Eds.

(Battelle Press, Columbus, OH, 1986), p. 995-1009.

173. R.M. Campbell, M.L. Lee, "Supercritical Fluid Fractionation of Petroleum and Coal Derived Mixtures," Anal. Chem. 58, 2247-2251 (1986).

(16)

174. J.S. Bradshaw, C. Schregenberger, H-C.K. Chang, K.E. Markides, M.L. Lee, "Synthesis and Chromatographic Properties of Polysiloxane Stationary Phases Containing

Biphenylcarboxylate Ester Liquid Crystalline Side Groups," J. Chromatogr. 358, 95-106 (1986).

175. M. Nishioka, H-C.K. Chang, M.L. Lee, "Structural Characteristics of Polycyclic Aromatic Hydrocarbon Isomers in Coal-Tars and Combustion Products," Environ. Sci. Technol. 20, 1023-1027 (1986).

176. W.R. West, P.A. Smith, G.M. Booth, M.L. Lee, "Determination and Genotoxicity of Nitrogen Heterocycles in a Sediment from the Black River," Environ. Toxicol. Chem. 5, 511-519 (1986).

177. W.R. West, M.L. Lee, "Evaluation of a Thermionic Detector for Capillary Supercritical Fluid Chromatography of Nitrated Polycyclic Aromatic Compounds," J. High Resolut.

Chromatogr./Chromatogr. Commun. 9, 161-167 (1986).

178. B.A. Jones, K.E. Markides, J.S. Bradshaw, M.L. Lee, "Contemporary Capillary Column Technology for Chromatography," Chromatogr. Forum 1, 38-44 (1986).

179. W.R. West, P.A. Smith, G.M. Booth, S.A. Wise, M.L. Lee, "Determination of Genotoxic Polycyclic Aromatic Hydrocarbons in a Sediment from the Black River," Arch. Environ.

Contam. Toxicol. 15, 241-249 (1986).

180. M. Nishioka, D.G. Whiting, R.M. Campbell, M.L. Lee, "Supercritical Fluid Fractionation and Detailed Characterization of the Sulfur Heterocycles in a Petroleum Vacuum

Residue," Anal. Chem. 58, 2251-2255 (1986).

181. C.L. Woolley, K.E. Markides, M.L. Lee, "Deactivation of Fused Silica Capillary Columns with Polymethylhydrosiloxanes: Optimization of Reaction Conditions," J. Chromatogr.

367, 9-22 (1986).

182. K.E. Markides, S.M. Fields, M.L. Lee, "Capillary Supercritical Fluid Chromatography of Labile Carboxylic Acids," J. Chromatogr. Sci. 24, 254-257 (1986).

183. C.L. Woolley, K.E. Markides, M.L. Lee, "Deactivation of Fused Silica Capillary Columns with Polymethylhydrosiloxanes: Characterization of the Deactivated Surface," J.

Chromatogr. 367, 23-34 (1986).

184. K.E. Markides, M.L. Lee, "Recent Advances in Capillary Supercritical Fluid

Chromatography," Advances in Capillary Chromatography, J.G. Nikelly, Ed. (Dr. Alfred Huthig Verlag, Heidelberg, 1986), p. 19-34.

185. M.A. Pulsipher, K.E. Markides, R.S. Johnson, J.S. Bradshaw, M.L. Lee, "Methoxyphenyl Polysiloxane Stationary Phases for Capillary Column Gas Chromatography," J.

Chromatogr. Sci. 24, 383-391 (1986).

(17)

186. M.L. Lee, K.E. Markides, "Current Technological Challenges in Capillary Supercritical Fluid Chromatography," J. High Resolut. Chromatogr./Chromatogr. Commun. 9, 652-656 (1986).

1987

187. J.M. Bayona, B.J. Tarbet, H-C.K. Chang, C.M. Schregenberger, M. Nishioka, K.E.

Markides, J.S. Bradshaw, M.L. Lee, "Selective Gas Chromatographic Stationary Phases for Nitrogen-Containing Polycyclic Aromatic Compounds," Intern. J. Environ. Anal.

Chem. 28, 263-278 (1987).

188. J.C. Kuei, K.E. Markides, M.L. Lee, "Supercritical Ammonia as Mobile Phase in Capillary Chromatography," J. High Resolut. Chromatogr./Chromatogr. Commun. 19, 257-262 (1987).

189. M.R. Plasterer, G.M. Booth, M.L. Lee, W.R. West, P. Smith, M.L. Tedjamulia, Y.

Tominaga, R.N. Castle, "Comparative Mutagenicity of Analogous Amino- and Nitropolycyclic Aromatic Hydrocarbons," Twenty-fourth Hanford Life Sciences

Symposium: Health & Environmental Research on Complex Organic Mixtures, R.H. Gray, E.K. Chess, P.J. Mellinger, R.G. Riley, and D.L. Springer, Eds. (Richland, WA, 1987), p.

251-257.

190. K. Takahasi, R.N. Castle, M.L. Lee, "Syntheses of 1-,2-,3-, and 4-Acridinecarbaldehydes,"

J. Heterocyclic Chem. 24, 977-979 (1987).

191. M. Zander, J. Jacob, M.L. Lee, "Empirical Quantitative Relationship Between Molecular Structure and Phosphorescence Transition Energy of Polycyclic Aromatic Thiophenes," Z.

Naturforsch. 42a, 735-738 (1987).

192. C.L. Woolley, K.D. Bartle, K.E. Markides, M.L. Lee, "Deactivation of Small Diameter Fused Silica Capillary Columns with Organosilicon Hydrides," J. High Resolut.

Chromatogr./Chromatogr. Commun. 9, 506-514 (1987).

193. M.L. Lee, K.E. Markides, "Chromatography with Supercritical Fluids," Science 235, 1342-1347 (1987).

194. H. Kudo, K. Takahasi, R.N. Castle, M.L. Lee, "Synthesis of

[1]Benzothienonaphthyridines," J. Heterocyclic Chem. 24, 1009-1011 (1987).

195. D.J. Eatough, C.L. Benner, J.M. Bayona, F.M. Caka, H. Tong, L. Lewis, J.D. Lamb, M.L.

Lee, E.A. Lewis, L.D. Hansen, "Sampling for Gas Phase Nicotine in Environmental Tobacco Smoke with a Diffusion Denuder and Passive Sampler," Proceedings of the 1987 EPA/APCA Symposium on Measurement of Toxic and Related Pollutants (APCA,

Pittsburgh, PA, 1987), p. 132-139.

196. N.W. Adams, J.S. Bradshaw, J.M. Bayona, K.E. Markides, M.L. Lee, "Synthesis and Chromatographic Properties of Liquid Crystalline Polycyloxanes Containing Steroid Substituents," Mol. Cryst. Liquid Cryst. 147, 43-60 (1987).

(18)

197. S.M. Fields, K.E. Markides, M.L. Lee, "Retention in Capillary Supercritical Fluid Chromatography with Carbon Dioxide Mobile Phases Containing Polar Modifiers," J.

Chromatogr. 406, 223-235 (1987).

198. D.J. Eatough, C.L. Benner, J.M. Bayona, F.M. Caka, R.L. Mooney, J.D. Lamb, M.L. Lee, E.A. Lewis, L.D. Hansen, "Identification of Conservative Tracers of Environmental Tobacco Smoke," Indoor Air '87: Proceedings of the 4th International Conference on Indoor Air Quality and Climate, Vol. 2 (Berlin [West], August 17-21, 1987).

199. K.D. Bartle, C.L. Woolley, K.E. Markides, M.L. Lee, R.S. Hansen, "The Rayleigh Instability of Stationary Phase Films in Capillary Column Chromatography," J. High Resolut. Chromatogr./Chromatogr. Commun. 10, 129-136 (1987).

200. M.L. Lee, K.E. Markides, "Supercritical Fluid Chromatography," Nature 327, 441-442 (1987).

201. B.W. Wright, B.E. Richter, M.L. Lee, "Surface Chemistry and Preparation of Siliceous Capillary Columns for Gas Chromatography," Modern Methods of Capillary Separation Methods, M. Novotny, Ed. (Wiley-Interscience, New York).

202. S.K. Aggarwal, J.S. Bradshaw, M. Eguchi, S. Parry, B.E. Rossiter, K.E. Markides, M.L.

Lee, "New Chiral Polysiloxanes Prepared from Derivatives of (+)- or (-)-2-Phenyl-3- Butenoic Acid, (R)-1-Hepten-3-ol and (R)-1-Cyclohexyl-2-Propen-1-ol," Tetrahedron 43, 451-462 (1987).

203. J.S. Bradshaw, S.K. Aggarwal, C.A. Rouse, B.J. Tarbet, K.E. Markides, M.L. Lee,

"Polysiloxanes Containing Thermally Stable Chiral Amide Side Chains for Capillary Gas and Supercritical Fluid Chromatography," J. Chromatogr. 405, 169-177 (1987).

204. M. Zander, J. Jacob, M.L. Lee, “Empirical Quantitative Relationship between Molecular Structure and Phosphorescence Transition Energy of Polycyclic Aromatic Thiophenes,” Z.

Naturforsch 42a, 735-738 (1987).

1988

204. H-C.K. Chang, M. Nishioka, K.D. Bartle, S.A. Wise, J.M. Bayona, K.E. Markides, M.L.

Lee, "Identification and Comparison of Low-Molecular-Weight Neutral Constituents in Two Different Coal Extracts," Fuel 67, 45-57 (1988).

205. R.J. Skelton, Jr., K.E. Markides, P.B. Farnsworth, M.L. Lee, F.J. Yang, "Multi-Element Selective Radio Frequency Plasma Detector for Capillary Gas Chromatography," J. High Resolut. Chromatogr./Chromatogr. Commun. 11, 75-81 (1988).

206. S.L. Castle, J-K. Lou, H. Kudo, R.N. Castle, M.L. Lee, "The Synthesis of Novel Heterocyclic Ring Systems via Photocyclization. 1. Thieno[3,2:4,5]thieno[2,3- c]quinoline and Thieno[2,3:4,5]- thieno[2,3-c]quinoline," J. Heterocyclic Chem. 25, 1363-1365 (1988).

(19)

207. W.R. West, P.A. Smith, G.M. Booth, M.L. Lee, "Isolation and Detection of Genotoxic Components in a Black River Sediment," Environ. Sci. Technol. 22, 224-228 (1988).

208. M. Nishioka, M.L. Lee, "Preferred Annellated Structures of Polycyclic Aromatic Compounds in Coal-Derived Materials," ACS Symp. Ser. 14, 235-253 (1988).

209. C.L. Woolley, B.J. Tarbet, K.D. Bartle, K.E. Markides, J.S. Bradshaw, M.L. Lee, "Static Coating of Phenyl and Biphenyl Polysiloxane Stationary Phases on Small-Diameter Capillary Columns," J. High Resolut. Chromatogr./Chromatogr. Commun. 11, 113-118 (1988).

210. H. Tang, C.L. Benner, G.H. Richards, M.L. Lee, E.A. Lewis, L.D. Hansen, D.T. Eatough,

"Monitoring of Environmental Tobacco Smoke Nicotine with a Sorbent Bed-Capillary Gas Chromatograph System," Intern. J. Environ. Anal. Chem. 33, 197-208 (1988).

211. S.M. Fields, K.E. Markides, M.L. Lee, "Ultraviolet-absorption Detector for Capillary Supercritical Fluid Chromatography with Compressible Mobile Phases," Anal. Chem. 60, 802-806 (1988).

212. S.M. Fields, K.E. Markides, M.L. Lee, "Practical Aspects of Mixed Mobile Phases in Capillary Supercritical Fluid Chromatography," J. High Resolut.

Chromatogr./Chromatogr. Commun. 11, 25-29 (1988).

213. J.M. Bayona, K.E. Markides, M.L. Lee, "Characterization of Polar Polycyclic Aromatic Compounds in a Heavy Duty Diesel Exhaust Particulate by Capillary Column Gas Chromatography and High Resolution Mass Spectrometry," Environ. Sci. Technol. 22, 1440-1447 (1988).

214. C.A. Rouse, A.C. Finlinson, B.J. Tarbet, J.C. Pixton, N.M. Djordjevic, K.E. Markides, J.S.

Bradshaw, M.L. Lee, "Comparison of Oligoethylene Oxide-Substituted Polysiloxanes with Carbowax as Stationary Phases for Capillary Chromatography," Anal. Chem. 60, 901-905 (1988).

215. R.M. Campbell, N.M. Djordjevic, K.E. Markides, M.L. Lee, "Supercritical Fluid Chromatographic Determination of Hydrocarbon Groups in Gasolines and Middle Distillate Fuels," Anal. Chem. 60, 357-362 (1988).

216. E.C. Huang, B.J. Jackson, K.E. Markides, M.L. Lee, "Direct Coupling of Capillary Supercritical Fluid Chromatography to High Resolution Mass Spectrometry with Minimum Modification," Chromatographia 25, 51-54 (1988).

217. S.A. Wise, L.C. Sander, H-C.K. Chang, K.E. Markides, M.L. Lee, "Shape Selectivity in Liquid and Gas Chromatography: Polymeric Octadecylsilane (C18) and Liquid Crystalline Stationary Phases," Chromatographia 25, 473-479 (1988).

(20)

218. H. Tang, G. Richards, K. Gunther, J. Crawford, M.L. Lee, E.A. Lewis, D.J. Eatough,

"Determination of Gas Phase Nicotine and 3-Ethenylpyridine, and Particulate Phase Nicotine in Environmental Tobacco Smoke with a Collection Bed-Capillary Gas

Chromatography System," J. High Resolut. Chromatogr./Chromatogr. Commun. 11, 775- 782 (1988).

219. E.C. Huang, B.J. Jackson, K.E. Markides, M.L. Lee, "Direct Heated Interface Probe for Capillary Supercritical Fluid Chromatography/Double Focusing Mass Spectrometry,"

Anal. Chem. 60, 2715-2719 (1988).

220. B.J. Tarbet, J.S. Bradshaw, K.E. Markides, B.A. Jones, M.L. Lee, "The Chemistry of Capillary Column Technology," LC/GC 6, 233-248 (1988).

221. H-C.K. Chang, K.E. Markides, J.S. Bradshaw, M.L. Lee, "Selectivity Enhancement for Petroleum Hydrocarbons Using a Smectic Liquid Crystalline Stationary Phase in Supercritical Fluid Chromatography," J. Chromatogr. Sci. 26, 280-289 (1988).

1989

222. J-K. Lou, R.N. Castle, M.L. Lee, "The Synthesis of Isomeric Naphthylethylcarbazole Derivatives as Potential Reference Compounds in Coal-Derived Products," J. Heterocyclic Chem. 26, 1213-1219 (1989).

223. K.E. Markides, M.L. Lee, D.W. Later, "Capillary Supercritical Fluid Chromatography:

Practical Aspects," in Microbore Column Chromatography, A Unified Approach to Chromatography, Frank Yang, Ed. (Marcel Dekker, NY, 1989), p. 239-264.

224. D.J. Eatough, C.L. Benner, J.M. Bayona, G. Richards, J.D. Lamb, M.L. Lee, E.A. Lewis, L.D. Hansen, "Chemical Composition of Environmental Tobacco Smoke. 1. Gas-Phase Acids and Bases," Environ. Sci. Technol. 23, 679-687 (1989).

225. M.L. Lee, B. Xu, E.C. Huang, N.M. Djordjevic, H-C.K. Chang, K.E. Markides, "Liquid Sample Introduction Methods in Capillary Column Supercritical Fluid Chromatography,"

J. Microcol. Sep. 1, 7-13 (1989).

226. B.J. Tarbet, J.S. Bradshaw, D.F. Johnson, A.C. Finlinson, C.A. Rouse, K. Jones, S.R.

Sumpter, E.C. Huang, K.E. Markides, M.L. Lee, "Synthesis and Structural Considerations of Oligoethylene Oxide-containing Polysiloxane Stationary Phases in Capillary Gas and Supercritical Fluid Chromatography," J. Chromatogr. 473, 103-113 (1989).

227. J.K. Lou, K. Takahaski, J.D. McKenney, Jr., R.N. Castle, "Synthesis of Bridged

Heteroaromatic Compounds as Reference Standards for Coal Degradation Products," J.

Heterocyclic Chem. 26, 1845-1848 (1989).

228. C.L. Benner, J.M. Bayona, F.M. Caka, H. Tang, L.J. Lewis, J. Crawford, J.D. Lamb, M.L.

Lee, E.A. Lewis, L.D. Hansen, D.J. Eatough, "Chemical Composition of Environmental Tobacco Smoke. 2. Particulate Phase Compounds," Environ. Sci. Technol. 23, 688-698 (1989).

(21)

229. D.E. Raynie, S.M. Fields, N.M. Djordevic, K.E. Markides, M.L. Lee, "A Method for the Preparation of Binary Mobile Phase Mixtures for Capillary Supercritical Fluid

Chromatography," J. High Resolut. Chromatogr. 12, 51-52 (1989).

230. R.J. Skelton, Jr., P.B. Farnsworth, K.E. Markides, M.L. Lee, "Element Selective Detection After Supercritical Fluid Chromatography Using a Radio Frequency Plasma Detector,"

Anal. Chem. 61, 1815-1821 (1989).

231. I.L. Davies, B. Xu, K.E. Markides, K.D. Bartle, M.L. Lee, "Multidimensional Open Tubular Column Supercritical Fluid Chromatography Using a Flow-Switching Interface,"

J. Microcol. Sep. 2, 71-84 (1989).

232. H-C.K. Chang, K.E. Markides, J.S. Bradshaw, M.L. Lee, "Separation of Steroid Isomers Using a Liquid Crystalline Polysiloxane Stationary Phase in Capillary Supercritical Fluid Chromatography," J. Microcol. Sep. 1, 131-135 (1989).

233. D.E. Raynie, K.E. Markides, M.L. Lee, S.R. Goates, "Back-Pressure Regulated Restrictor for Flow Control in Capillary Supercritical Fluid Chromatography," Anal. Chem. 61, 1178-1181 (1989).

234. Q.L. Xie, K.E. Markides, M.L. Lee, "Supercritical Fluid Extraction-Supercritical Fluid Chromatography with Fraction Collection for Sensitive Analytes," J. Chromatogr. Sci. 27, 365-370 (1989).

235. K.M. Payne, I.L. Davies, K.D. Bartle, K.E. Markides, M.L. Lee, "Multidimensional Packed Capillary Column Supercritical Fluid Chromatography Using a Flow Switching Interface," J. Chromatogr. 477, 161-168 (1989).

236. J.K. Simons, C.H. N.A. Zabriskie, S.M. Fields, M.L. Lee, S.R. Goates, "Supercritical Fluid Chromatography/Supersonic Jet Spectroscopy: I. Microcolumns and Direct Expansions," J. Microcol. Sep. 1, 200-206 (1989).

237. S.R. Goates, C.H. Sin, J.K. Simons, K.E. Markides, M.L. Lee, "Supercritical Fluid Chromatography/Supersonic Jet Spectroscopy: II. Capillary Column SFC with a Sheath- Flow Nozzle," J. Microcol. Sep. 1, 207-211 (1989).

238. I.L. Davies, K.E. Markides, M.L. Lee, "Applications of Coupled LC-GC: A Review," J.

High Resolut. Chromatogr. 12, 193-207 (1989).

239. R.J. Skelton, Jr., H-C.K. Chang, P.B. Farnsworth, K.E. Markides, M.L. Lee, "Radio Frequency Plasma Detector for Sulfur Selective Capillary Gas Chromatographic Analysis of Fossil Fuels," Anal. Chem. 61, 2292-2298 (1989).

240. Z. Juvancz, M.A. Pulsipher, M.M. Schirmer, R.S. Johnson, K.E. Markides, J.S. Bradshaw, M.L. Lee, "New Cyanophenyl-containing Polysiloxane Stationary Phases for Capillary Column Gas Chromatography," J. Microcol. Sep. 1, 142-149 (1989).

(22)

241. Z. Juvancz, M.A. Pulsipher, M.M. Schirmer, R.S. Johnson, K.E. Markides, J.S. Bradshaw, M.L. Lee, "New Nitrophenyl- and Nitromethoxyphenyl-substituted Methylpolysiloxane Stationary Phases for Capillary Column Gas Chromatography," J. Microcol. Sep. 1, 309- 319 (1989).

1990

242. I.L. Davies, K.E. Markides, K.D. Bartle, M.L. Lee, "Multidimensional Supercritical Fluid Chromatography," in Multidimensional Chromatography, H.J. Cortes, Ed. (Marcel

Dekker, NY, 1990), p. 301-330.

243. E.C. Huang, B.J. Jackson, K.E. Markides, M.L. Lee, "Application of Capillary

Supercritical Fluid Chromatography/Double Focusing Mass Spectrometry Under Negative Ion Chemical Ionization Conditions," J. Microcol. Sep. 2, 88-96 (1990).

244. K.M. Payne, B.J. Tarbet, J.S. Bradshaw, K.E. Markides, M.L. Lee, "Simultaneous Deactivation and Coating of Porous Silica Particles for Microcolumn Supercritical Fluid Chromatography," Anal. Chem. 62, 1379-1384 (1990).

245. H. Tang, G. Richards, C.L. Benner, J.P. Tuominen, M.L. Lee, E.A. Lewis, L.D. Hansen, D.J. Eatough, "Solanesol: A Tracer for Environmental Tobacco Smoke," Environ. Sci.

Technol. 24, 848-852 (1990).

246. H-C.K. Chang, R.J. Skelton, Jr., K.E. Markides, M.L. Lee, "Determination of Sulfur- Containing Polycyclic Aromatic Compounds in Coal Extracts Using Capillary Gas Chromatography with Radio Frequency Plasma Detection," Polycycl. Aromat. Comp. 1, 251-264 (1990).

247. Z. Juvancz, K.M. Payne, K.E. Markides, M.L. Lee, "Multidimensional Packed Capillary to Open Tubular Column SFC/SFC Using a Valve-Switching Interface," Anal. Chem. 62, 1384-1388 (1990).

248. R.J. Skelton, Jr., K.E. Markides, M.L. Lee, P.B. Farnsworth, "Characterization of Near- Infrared Atomic Emission from a Radio Frequency Plasma as a Basis for Selective Detection After Capillary Gas Chromatography," Appl. Spectros. 44, 853-857 (1990).

249. M.W. Raynor, K.D. Bartle, A.A. Clifford, J.M. Chalmers, T. Katase, C.A. Rouse, K.E.

Markides, M.L. Lee, "Analysis of Aliphatic and Phenolic Carboxylic Acids by Capillary Supercritical Fluid Chromatography-Fourier-Transform Infrared Microspectrometry," J.

Chromatogr. 505, 179-190 (1990).

250. D.E. Raynie, M.L. Lee, D.R. Nelson, K.T. Harper, E.W. Mead, F.R. Stermitz, "Alkaloids of Arctomecon Species (Papaveraceae). 12-Methoxyallocryptopine, A New Protopine- type Alkaloid," Biochem. Syst. Ecol. 18, 45-48 (1990).

251. S.R. Sumpter, C.L. Woolley, E.C. Huang, K.E. Markides, M.L. Lee, "Static Coating of 5 to 50-μm i.d. Capillary Columns for Open Tubular Column Chromatography," J.

Chromatogr. 517, 503-519 (1990).

(23)

1991

252. S.R. Sumpter, M.L. Lee, "Enhanced Radial Dispersion in Open Tubular Column Chromatography," J. Microcol. Sep. 3, 91-113 (1991).

253. H-C.K. Chang, K.D. Bartle, K.E. Markides, M.L. Lee, "Structural Comparison of Low- Molecular-Weight Extractable Compounds in Different Rank Coals Using Capillary Column Gas Chromatography," in Advances in Coal Spectroscopy, H. Meuzelaar, Ed.

(Plenum Press, NY, 1991), p. 141-164.

254. J.S. Bradshaw, M.M. Schirmer, Z. Juvancz, K.E. Markides, M.L. Lee, "New Polar Polysiloxane Stationary Phases Containing Cyano, Nitrophenyl and 8-Quinolinyl Units Attached to Diethylene Oxide Side Groups," J. Chromatogr. 540, 279-291 (1991).

255. M. Huang, K.E. Markides, M.L. Lee, "Evaluation of an Ion Mobility Detector for Supercritical Fluid Chromatography with Solvent-modified Carbon Dioxide Mobile Phases," Chromatographia 31, 163-167 (1991).

256. L.Q. Xie, Z. Juvancz, K.E. Markides, M.L. Lee, "On-Line Multidimensional Open

Tubular Column Supercritical Fluid Chromatography Using a Valve-Switching Interface,"

Chromatographia 31, 233-238 (1991).

257. I.J. Koski, B.A. Jansson, K.E. Markides, M.L. Lee, "Analysis of Prostaglandins in Aqueous Solutions by Supercritical Fluid Extraction and Chromatography," J. Pharm. &

Biomed. Anal. 9, 281-290 (1991).

258. J.P. Tuominen, K.E. Markides, M.L. Lee, "Optimization of Internal Valve Injection in Open Tubular Column Supercritical Fluid Chromatography," J. Microcol. Sep. 3, 229-239 (1991).

259. B.E. Rossiter, P. Petersson, D.F. Johnson, M. Eguchi, J.S. Bradshaw, K.E. Markides, M.L.

Lee, "Rational Design of Chiral Stationary Phases for Capillary Supercritical Fluid Chromatography," Tetrahedron Let. 32, 3609-3612 (1991).

260. S.H. Page, S.R. Goates, M.L. Lee, "Methanol/CO2 Phase Behavior in Supercritical Fluid Chromatography and Extraction," J. Supercrit. Fluids 4, 109-117 (1991).

261. Z. Juvancz, M.M. Schirmer, D.F. Johnson, K.E. Markides, J.S. Bradshaw, M.L. Lee, "4- (Methylsulfonyl)phenyl-containing Polysiloxane Stationary Phase for Capillary Column Gas Chromatography," J. Microcol. Sep. 3, 349-353 (1991).

262. S.H. Page, D.E. Raynie, S.R. Goates, D.J. Dixon, K.P. Johnston, M.L. Lee, "Predictability and Effect of Phase Behavior of CO2/Propylene Carbonate in Supercritical Fluid

Chromatography," J. Microcol. Sep. 3, 355-369 (1991).

(24)

263. K. Rasmussen, G.M. Booth, M.L. Lee, "Mutagenicities of Hydroxy-Substituted

Carbazoles and Dibenzothiophenes Using the CHO/HGPRT Assay," Environ. Toxicol. 10, 1133-1137 (1991).

264. H. Budzinski, P. Garrigues, J. Connan, M.L. Lee, J. Andersson, J. Bellocq, "Determination of Maturity Indicators in Alkylated Aromatic Series by Gas Chromatography-Mass

Spectrometry (GC-MS)," Organic Geochemistry: Advances and Applications in the Natural Environment, D.A.C. Manning, Ed. (Manchester University Press, New York, 1991), p. 619-623.

265. D.E. Raynie, K.E. Markides, M.L. Lee, "Boiling Range Distribution of Petroleum and Coal-Derived Heavy Ends by Supercritical Fluid Chromatography," J. Microcol. Sep. 3, 423-433 (1991).

266. Z. Liu, P.B. Farnsworth, M.L. Lee, "Sample Introduction in Capillary Supercritical Fluid Chromatography Using Sequential Density Gradient Focusing and Solvent Venting," J.

Microcol. Sep. 3, 435-442 (1991).

267. H.G. Lee, E.D. Lee, M.L. Lee, "Atmospheric Pressure Ionization Time-of-Flight Mass Spectrometer for Real-Time Explosives Vapor Detection," Proceedings of the First International Symposium on Explosive Detection Technology, Siraj M. Khan, Ed. (FAA Technical Center, Atlantic City International Airport, 1992), p. 619-636.

268. I.J. Koski, M.L. Lee, "Solute Focusing in Supercritical Fluid Chromatography," J.

Microcol. Sep. 3, 481-490 (1991).

269. I.J. Koski, K.E. Markides, M.L. Lee, "Preservation of Column Efficiency When Using Solvent Vent Injection in Open Tubular Column Supercritical Fluid Chromatography," J.

Microcol. Sep. 3, 521-529 (1991).

270. C.H. Sin, E.D. Lee, M.L. Lee, "Atmospheric Pressure Ionization Time-of-Flight Mass Spectrometry with a Supersonic Ion Beam," Anal. Chem. 63, 2897-2900 (1991).

271. R.N. Castle, H. Kudo, M.L. Lee, "The Synthesis of Some Monomethylanthracenamines,"

Collect. Czech. Chem. Commun. 56, 2269-2277 (1991).

1992

272. R.E. Carlson, S. Critchfield, W.P. Vorkink, J-Z. Dong, R.J. Pugmire, M.L. Lee, Y. Zhang, J. Shabtai, K.D. Bartle, "High Resolution Chromatographic Characterization of

Depolymerized Coals of Different Rank: Aliphatic and Aromatic Hydrocarbons," Fuel 71, 19-29 (1992).

273. L.Q. Xie, K.E. Markides, M.L. Lee, "Biomedical Applications of Analytical Supercritical Fluid Separation Techniques," Anal. Biochem. 200, 7-19 (1992).

(25)

274. S.H. Page, S.R. Sumpter, M.L. Lee, "Fluid Phase Equilibria in Supercritical Fluid

Chromatography with CO2-Based Mixed Mobile Phases: A Review," J. Microcol. Sep. 4, 91-122 (1992).

275. M. Huang, W.P. Vorkink, M.L. Lee, "Evaluation of Surface-bonded Polyethylene Glycol and Polyethylene Imine in Capillary Electrophoresis," J. Microcol. Sep. 4, 135-143 (1992).

276. P. Petersson, K.E. Markides, D.F. Johnson, B.E. Rossiter, J.S. Bradshaw, M.L. Lee,

"Chromatographic Evaluation of Chiral (1R-trans)-N,N-1,2-Cyclohexylenebisbenzamide- oligodimethylsiloxane Copolymeric Stationary Phases for Capillary Supercritical Fluid Chromatography," J. Microcol. Sep. 4, 155-162 (1992).

277. Z. Liu, P.B. Farnsworth, M.L. Lee, "High-Speed, Thermally Modulated SFE/GC for the Analysis of Volatile Organic Compounds in Solid Matrices," J. Microcol. Sep. 4, 199-208 (1992).

278. M. Huang, W.P. Vorkink, M.L. Lee, "High Efficiency Cross-linked Polyacrylamide Coating for Capillary Electrophoresis of Proteins," J. Microcol. Sep. 4, 233-238 (1992).

279. D.F. Johnson, J.S. Bradshaw, M. Eguchi, B.E. Rossiter, M.L. Lee, P. Petersson, K.E.

Markides, "Synthesis of (1R-trans)-N,N-1,2-

cyclohexylenebisbenzamideoligodimethylsiloxane Copolymers for Use as Chiral

Stationary Phases for Capillary Supercritical Fluid Chromatography," J. Chromatogr. 594, 283-290 (1992).

280. M. Wu, M.L. Lee, P.B. Farnsworth, "Nitrogen-selective Detection for Gas

Chromatography With a Helium Radiofrequency Plasma Detector," J. Anal. Atomic Spectrom. 7, 197-200 (1992).

281. W.F. Sye, Z.X. Zhao, M.L. Lee, "Comparative Application of Sulfur Chemiluminescence Detection in Gas and Supercritical Fluid Chromatography," Chromatographia 33, 507-513 (1992).

282. I.J. Koski, K.E. Markides, B.E. Richter, M.L. Lee, "Microliter Sample Introduction for Open Tubular Column Supercritical Fluid Chromatography Using a Packed Capillary for Solute Focusing," Anal. Chem. 64, 1669-1675 (1992).

283. Z. Zhao, A. Malik, M.L. Lee, "Separations of Proteins and Proteolytic Digests of Proteins by Capillary Electrophoresis on Superox-coated Open Tubular Columns," J. Microcol.

Sep. 4, 411-417 (1992).

284. M. Huang, M.L. Lee, "Hydrogel Polymer Coatings for Capillary Electrophoretic Separation of Proteins," J. Microcol. Sep. 4, 491-496 (1992).

285. B.E. Rossiter, S.L. Reese, S. Morgan, A. Malik, J.S. Bradshaw, M.L. Lee, "Syntheses of Isomeric Cyanobiphenyl-Substituted Polysiloxanes for Stationary Phases in Gas

Chromatography," J. Microcol. Sep. 4, 521-527 (1992).

(26)

286. A. Malik, I. Ostrovsky, S.R. Sumpter, S.L. Reese, S. Morgan, B.E. Rossiter, J.S.

Bradshaw, M.L. Lee, "Novel Cyanobiphenylpolysiloxane Stationary Phases for Gas and Supercritical Fluid Chromatography," J. Microcol. Sep. 4, 529-540 (1992).

287. M. Huang, S. Liu, B.K. Murray, M.L. Lee, "High Resolution Separation and Quantitation of Ribonucleotides Using Capillary Electrophoresis," Anal. Biochem. 207, 231-235 (1992).

288. T.D. Parrish, E.S. Francis, G.M. Booth, D.J. Eatough, M.L. Lee, "Supercritical Fluid Chromatography Coupled with the Salmonella Microsuspension Mutagenicity Assay,"

Fres. J. Anal. Chem. 344, 442-446 (1992).

289. D.J. Eatough, T.D. Parrish, E.S. Francis, G.M. Booth, M.L. Lee, E.A. Lewis, "Combined Supercritical Fluid Chromatography/Microsuspension Mutagenicity Assay of

Environmental Tobacco Smoke," Measurement of Toxic and Related Air Pollutants, Proc.

of the 1992 U.S. EPA/A&WMA Internat. Symp. (Air & Waste Management Association, Pittsburgh, PA, 1992), p. 433-444.

290. C.H. Sin, S.R. Goates, M.L. Lee, D.M. Lubman, "Analysis with Supercritical Fluids:

Extraction and Chromatography," in Supersonic Jet Spectroscopy with Supercritical Fluids, Chapter 11 (1992), p. 190-202.

291. C.H. Sin, E.D. Lee, M. Wu, P.B. Farnsworth, M.L. Lee, "Design of a Versatile Time-of- flight Mass Spectrometer with an Atmospheric Pressure Ion Source," Proc. First

International Conference on Instrumentation for Time-of-flight Mass Spectrometry (LeCroy Corporation, Chestnut Ridge, New York, 1992), p. 213-223.

1993

292. Y. Tominaga, R.N. Castle, M.L. Lee, "Synthesis of Aminochrysenes by the Oxidative Photocyclization of Acetylaminostilbenes," Chem. Pharm. Bull. 41, 1853-1855 (1993).

293. J.S. Bradshaw, G. Yi, B.E. Rossiter, S.L. Reese, P. Petersson, K.E. Markides, M.L. Lee,

"Novel Cyclodextrin-Oligosiloxane Copolymers and Their Use as Stationary Phases for Separating Enantiomers in Open Tubular Column Supercritical Fluid Chromatography,"

Tetrahedron Let. 34, 79-82 (1993).

294. J-Z. Dong, W.P. Vorkink, M.L. Lee, "Origin of Long-Chain Alkylcyclohexanes and Alkylbenzenes in a Coal-Bed Wax," Geochim. Cosmochim. Acta 57, 837-849 (1993).

295. A. Malik, Z. Zhao, M.L. Lee, "Simple Method for the Preparation of Highly Efficient Polymer-coated Capillary Electrophoresis Columns," J. Microcol. Sep. 5, 119-125 (1993).

296. L.Q. Xie, K.E. Markides, M.L. Lee, N.K. Hollenberg, G.H. Williams, S.W. Graves,

"Bioanalytical Application of Multidimensional Open Tubular Column Supercritical Fluid Chromatography," Chromatographia 35, 363-371 (1993).

(27)

297. G. Yi, J.S. Bradshaw, B.E. Rossiter, S.L. Reese, P. Petersson, K.E. Markides, M.L. Lee,

"Novel Cyclodextrin-Oligosiloxane Copolymers for Use as Stationary Phases to Separate Enantiomers in Open Tubular Column Supercritical Fluid Chromatography," J. Org.

Chem. 58, 2561-2565 (1993).

298. I.J. Koski, E.D. Lee, I. Ostrovsky, M.L. Lee, "Solid-phase Injector for Open Tubular Column Supercritical Fluid Chromatography," Anal. Chem. 65, 1125-1129 (1993).

299. S.H. Page, H. Yun, M.L. Lee, S.R. Goates, "Rapid Method for the Determination of Phase Behavior of Fluid Mixtures Employed in Supercritical Fluid Experiments," Anal. Chem.

65, 1493-1495 (1993).

300. D.E. Raynie, K.M. Payne, K.E. Markides, M.L. Lee, "Evaluation of Microbore and Packed Capillary Column Chromatography with an Ethylvinylbenzene-Divinylbenzene Polymeric Packing Material and Supercritical Ammonia as the Mobile Phase," J.

Chromatogr. 638, 75-83 (1993).

301. M. Huang, G. Yi, J.S. Bradshaw, M.L. Lee, "Charged Surface Coatings for Capillary Electrophoresis," J. Microcol. Sep. 5, 199-205 (1993).

302. P.Z. Liu, A. Malik, M.C.J. Kuchar, W.P. Vorkink, M.L. Lee, "Polymeric Hollow Fibers for Capillary Electrophoresis," J. Microcol. Sep. 5, 245-253 (1993).

303. Z. Liu, I. Ostrovsky, P.B. Farnsworth, M.L. Lee, "Instrumentation for Comprehensive Two-Dimensional Capillary Supercritical Fluid-Gas Chromatography," Chromatographia 35, 567-573 (1993).

304. S.H. Page, S.R. Sumpter, S.R. Goates, D.J. Dixon, K.P. Johnston, M.L. Lee "Tri-n-butyl- phosphate/CO2 and Acetone/CO2 Phase Behaviors and Utilities in Capillary Supercritical Fluid Chromatography," J. Supercrit. Fluids 6, 95-101 (1993).

305. A. Malik, W. Li, M.L. Lee, "Preparation of Long Packed Capillary Columns Using Carbon Dioxide Slurries," J. Microcol. Sep. 5, 361-369 (1993).

306. S.H. Page, A. Malik, S.R. Sumpter, M.L. Lee, "Demonstration of a Linear Composition Gradient During Water Saturation of CO2 in Supercritical Fluid Chromatography,"

Chromatographia 37, 93-97 (1993).

307. M. Wu, Z. Liu, P.B. Farnsworth, M.L. Lee, "Comprehensive Supercritical Fluid

Extraction/Gas Chromatographic Analysis of Organic Compounds in Soil Matrices with an Element-Selective Radiofrequency Plasma Detector," Anal. Chem. 65, 2185-2188 (1993).

308. G. Yi, J.S. Bradshaw, B.E. Rossiter, A. Malik, W. Li, M.L. Lee, "New Permethyl- Substituted β-Cyclodextrin Polysiloxanes for Use as Chiral Stationary Phases in Open Tubular Column Chromatography," J. Org. Chem. 58, 4844-4850 (1993).

Références

Documents relatifs

[r]

O debate sobre a nova economia diz respeito principalmente aos Estados Unidos, na medida em que o crescimento europeu se explica muito bem pelos argumentos tradicionais, sem falar

[r]

[r]

[r]

The study focuses on phonological, orthographical, lexical, syntactical, semantic, pragmatic and tex- tual aspects and reveals the overwhelming influence of French, English and

[r]

[r]