Quantitative description and local structures of trivalent metal ions Eu(III) and Cm(III) complexed with polyacrylic acid

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(1)Quantitative description and local structures of trivalent metal ions Eu(III) and Cm(III) complexed with polyacrylic acid Gilles Montavon, M. Bouby, Sandrine Huclier-Markai, Bernd Grambow, H. Geckeis, T. Rabung, I. Pashalidis, B. Amekraz, C. Moulin. To cite this version: Gilles Montavon, M. Bouby, Sandrine Huclier-Markai, Bernd Grambow, H. Geckeis, et al.. Quantitative description and local structures of trivalent metal ions Eu(III) and Cm(III) complexed with polyacrylic acid. Journal of Colloid and Interface Science, Elsevier, 2008, 327, pp.324-332. �10.1016/j.jcis.2008.08.037�. �in2p3-00339580�. HAL Id: in2p3-00339580 http://hal.in2p3.fr/in2p3-00339580 Submitted on 2 Dec 2008. HAL is a multi-disciplinary open access archive for the deposit and dissemination of scientific research documents, whether they are published or not. The documents may come from teaching and research institutions in France or abroad, or from public or private research centers.. L’archive ouverte pluridisciplinaire HAL, est destinée au dépôt et à la diffusion de documents scientifiques de niveau recherche, publiés ou non, émanant des établissements d’enseignement et de recherche français ou étrangers, des laboratoires publics ou privés..

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(214) TPn u7l& a0U55l n,h~TPU(Pj VjkT5Uy wv0l n lgV

(215) 5lg3 S ]/D o |¢h&T0Hu im$l #Ýj-y|y Ti ab0iml7W&U5U(T(V.u7T5n ltV

(216) (W&UÝTPU(l u7lYVW&iJjkTU j-y.jU*W'X0l n W'0l|h&Tu im$l #[l&H 0l'Rn 0T5i c0u*l'n.h&(W@jkU[R 4j VgV

(217) 5j-y.$W 5n T0W&h' j R 0TKyy j b[imltimWYVl n W&ijkU;Vl n W&hYV

(218) jkT5Uy b0l)V-w7l&l&U*h&T5Hu 0iz$l #[l&8u*lYVW&ij TPUyjUvV

(219) (lgu7T05l@imizjkU5NW&U(< /jkKj 8W 0TKyy j b0imlvl ! !/l~hYV.T !Lu7lYVW&ijkT0U8ikT0W&5jU5 T5UtV

(220) (lg y 0l&h&jmWYVjkTPU h&W&Ugb0l|$l #0h&iÁa[5l&R {L5l8jkU;Vl'nW&hYVjkTPUNw W;yvy]V-a[5jkl& !

(221) T5n|Wvw7jk5l nW@U0lN=T ! 3 R Ýuv!R ? @kZ BN(!R ? @kZ AW&U5>u*lYVW&iLjkTU h&T5U5h&l&UV

(222) n W¿V

(223) j TPUy !R @FE B @âr 9S )RJ{L52l J;a[W@UV/Ij !

(224) jmh&WYVjzT5U T ! 3 S ]/ 3Pjmy]V

(225) n jÁba5V

(226) jkT5UEbPlYV-w7l~l'UV

(227) 5lNba[ip y T5i a5VjkT5U7W&U5gV

(228) 5l 0TiÁc(u8l Rn (W(ylÀw7Wy.5TPU(lÀw7j V7{} ?RM.eva!y jkU58#u¢W/y !

(229) i a[T5n l;yh&l&U;VJu7lYVW&i0jkTU[R{L5l u*lYV

(230) 5T0 (W;yLV

(231) 5l3W&X0W&U;VW'0l,V

(232) Tvb0l3W ~5jnl&hYV 7 y 0l&h&jmWYV

(233) jmTPU7u*lYV

(234) (T*W;yh&TPu 0W'n l&vV

(235) T8T;V

(236) (l'/n 5n/T0h&l&;a0n ly 5l;yh'n j b[l~ jkU V

(237) 5l ikj Vl'nWYV-a0n l&Êws5l'nl V

(238) 5l u7lYVW&iDj-T5U y 0l&h&jmWYV

(239) jkT5U j-y 5l nöjÁX[l& jkU55jkn l&hYViÁc[R {15l h'(W'n W&hYVl nöj WYVjkTPU =T !V

(240) 5l|jkU;Vl'nW&hYV

(241) jkT5U7WYVV

(242) (ltu Tikl&hYa[imW'n y h~W@imlÀw W;y y

(243) V-a[Pjkl~ b5c3V-w7T*$W nTW~h'5l;y V

(244) 5lgy

(245) V

(246) T5jkh&5jkTu*lYV

(247) n/c =T !V

(248) 5l3h&T5Hu 0iz$l #P^j-R lR&V

(249) 5l|U;a[u b[l n.=T ! g h&5W&jkUy1jkUVl'n W&hYVjkUvw7j V 5.aNj-y W'U(W@ikcyl&8b5<c 5 iklhYV

(250) n/T y 5nWYcNjkT0U5jWYV

(251) j TPUNu*Wy y|y 0l&hYV

(252) n Tu*lYV

(253) n/Gc 5AePoS4e #W'U( b5cÝvy/c0u8u*lYV

(254) n jkh MJikTw MJjml&iz1 MJikTL w M!n W&hYVjkT5U5WYVjkT5U*h&T(a 0ikl& w j V

(255) Nl&j V5l'n. oS4Ge ]v y MJi MNMNMJo] oS_-e !

(256) TPRn 51a 5lYVl&h V

(257) jkT5U .T5 n vi V

(258) n W&oX0jkT0iklYV5l¿Vl~hYV

(259) jkT5U5^ ]vDy MJ:i MNMOM o

(260) !

(261) T5n g?5lYVl~hYV

(262) jkT5U )R {L5lNU;a[u b[l n3W@U(¯U5WYV-a0nlN=T !¤h&Tu im$l #[l&y 0l&h&jml;y ^1j

(263) R l8V

(264) 5lNU;a[u b[l n3T !¤h;W n]b0T #5c0imWYVl85n Ta y b0Ta0U5 8$h ^ V

(265) (l¢u7T5l =T !Db0jkU55jU5 ]b0jm5l&U;VWYVl~û7TU(T5l'UVWYV$l 4W U5 V

(266) 5l U;a[u b[l n4=T ! c0nWYV/j TPUgw WYVl'nLu TPiml&hYa[iml;yLb0Ta0U5 Jw l'n l|W;yy l;yy lgb5c7{"} ?MeR 6§Gv6 0 : 6 v. M ., 6*=.8: . .

(267)

(268) . #TPu7u*l'n h&jmW&izikc4W'X0W&jmizW'b0imlyT5j a[u 0l'n h&5ikT5n WYVl u7TPU0T5c(n WYVl+ MJi a0p0W&^ a0n]a[uH ^Q5.a0n/T 5j a[u T#0jml nTPikW'bPT^" } 5 #{ 3} ^ y T0Pj au W~h;l)VW¿Vl ]3h nT5ikW'b0T ^ 5T5iÁc0Wh'n/c5imjmh W&h&jm g8 WYV S¯w 4R(7W@U( SOHw 4N W ]gimn jmh& ^7#i& ^5_eW~h@i W~cP^ 5.a0n j-y T8{.T ^ 8W ^0A5 e0W&h&ikW'c0=^ 5.a0n j-y TN{LT W'U( d >R ^ 5?e0W&h&ikW'c[^=5.a0n/jzyTN{1T w l'n l,a!y l~8W;y.n l&hl&jÁX[l&R d/ Àu y]VTh py T5i a5V

(269) jkT5Uvw*W;yTbVW&jkU5l& b5c*5j-y)y Ti a5V/jkT5U*W&U5Øy$l [W'n WYV

(270) jkT5<U !-nTu¢W c0l~W'n yTPi NQ !

(271) Do &%NU(lYa5V

(272) n/T5U y Ta0n h&lR "!#$%

(273) &(') (%#')+*,+- &+,% & /.012. 3 iziV

(274) (lØyTi a5VjkTPU0y w7l n l1 5n l 0W'n l&8w7j V8ai V

(275) n W$ a0n lgw W~Vl n,W U5ÝW@iki!V

(276) 0l W&U(W@ikcyl;y#w l'n l75TPU(l7WYV nT5TPu Vl'uH 0l n WYV-a0n lR | w j V/ W8u7Timl&h)aimW'n#w7l&jkV#T! W w W;yÀa!yl&ØVT 5n l$ 0W n lgV

(277) 5lØyW&uH imly8!

(278) T5n {Q} ?RMe>u8l~W(y

(279) a0n l&u*l@UV y,jkU d 7=R MJT5n¤W'ikiLTV

(280) 5l'n¤l # 0l'n/jzu*l&U;V y^ ( 7W 3 w W;y aJy l&R5`|Wy l&ÝTU izj Vl'n WYV-a0n l 5W¿VW o ^ j V3j-y W;y)y]a[u*l&EV

(281) 5WYV | w7j V/ 4S 34N 7W W@U( ( 7W>(W~XPlEy jzu*jzimW'n h&T5Hu 0iz$l #PWYV/j TPHU 5n=T 0l'n-V

(282) jkl;/y !

(283) T5n 51aJR 55ÈJú#¥z!ú )zú 5[z+© 5 3 S

(284) // D6 | W&U( 3 S

(285) // D6ù3h yW&Hu imlyLw7l n l 5n$l 0W'n l&vb5c*u :j #[jkU5NW&izj J;a[TV y.=T ! S W'U( 33^s-h /W&h&l)VW¿V$l vy-VTh'pDyTPi a5V

(286) j TPUy¿R{L5<l f X0W&iÁa[l w7W;y¤V

(287) 5l&U W& /a!y]Vl&w7j V

(288) §W@imj J;a[T(V yA=T ! f HÀi#T5n *W H]fxR MJT5ngV

(289) 5lEyW&1u 0iml;y 5n $l 0W n l&DjU d 3^#l # 0l'n jzu*l&U;V y3w7l'n7l l n !

(290) T5n/u*l&DjkU"W 0ikT(XPl§bPT # !]iÁa!y 0l&¯w7j V

(291) d n l'ikW)V/jÁX0l ;a[u8jm5jV-(c )R MTPn73h&^¤W'U5 g h&T5U5hl&U;V

(292) n W V

(293) jkT5U7y 6 u7!R ? @kZ ^V

(294) 5l V

(295) jku8lÀVTvn l~W&h'7l J;a[jkizjÁb0n jÁau w Wy y 5TwvU3V

(296) T bPl,n $W 5jk5^0j-R lR@bPl&ikT(L w !

(297) jÁX[ltu*jkUa5Vl;y)R MJT5n g WYV h'T5U5h~l@UV

(298) n W V

(299) jkTPU7y 8 u7!R ? @kZ ^,h&T5U;VW~hYV|V

(300) jku8ly X[W'n/c(jzU !-n Tu W&U5 H5W'c[y w l'n l U5l&hl;yyW'n/3 c !

(301) TPn l J;a[jkizjÁb5nWYV

(302) jkT5UR 51a[^JÀu W@U( g3^3h*h&T5U5h&l&U;V

(303) nWYV

(304) jkT5Uy w7l'nl h&(l;h p0l&xa!y jkU5 W : 9 o 5#Ph&l&i oS_e

(305) sQgo 5 ikl&u*l&U;VW&:i ^Lb5cDizj J;a[jmHy h&jkU;VjzikimWYV/j TPUh&T(a0UV

(306) jkU W&h'p0W'n ; &(¯{"} 6-,` ? j J;a[jmHe0h&jUV/jkimizW)V/jkT5U W'U(W@ikc5l' n _W'U5 b5c {1T;VW'i tn/0W&U5jmh¢#W'n/b0T5U { 3 "u7lW;y]a0nl@u*l&U;V y e55jku8W~'a { 3 (P W'U(W@ikc5l' n ^Pn l y 0l&h V

(307) jÁX[l@iÁcKR. .

(308) 55ÈJú#¥z ¦0 ¨)£'¿ ú¤m©+5 W'n W&u7l)Vl'n y !

(309) TPn"V

(310) 5l¢S3]/ 6-3h y/c[y]Vl&u W n l fH4 ^ -#u 4 @ S%^ K5.a 4 @âr S

(311) .W&hlYVWYVlÝh TPU(h&l'U;V

(312) nWYV

(313) jkT5U§w W;y3X0W'n jml& !-n Tu R @âr V

(314) T(R S4RNMJTn,V

(315) 5l8S3]/ D6 | y/cy

(316) Vl&u7^PV

(317) 5l8 f w W(y.X0W'n jml&<!-n T0u vVT70R @^(V

(318) (l g h~TPU(h&l&U;V

(319) n W V

(320) jkT5U<!

(321) n Tu ( !R ? @kZ VT-R suv!R ? @kZ W'U(xV

(322) (l u*lYVW&ijkT5UÝh&T5U5h&l&UV

(323) n WYV

(324) jkT5U7!-nTu @âr V

(325) T-!R @FE S4RU V

(326) 5j-y|y]V-a[c(^l # 0l'n jzu*l&U;VW&iJh&TPU(Pj V/jkT5Uy w l'n l7h'5Ty l&U>yTxV

(327) (WYV j UÝW~XPl'n W'0l7U5TV.u7T5n lgV

(328) 5W'UÝT5U5l7u8l)VW@iJjkT5Uj-y¤h&Tu iml$#0l&- 0l'n" 0T5i c0u*l'n¤h'(W&jU /h&T5Uy j 5l'n jU5 V

(329) 5WYV T5U5iÁc T5U5l 3 h&(W@jkU h&W&U jzUVl'n W&h)V wsj V

(330) 9 S )R¯ ikj-y]V =T !4V

(331) 5l y W&u iml h'(W'n W&hYVl nöjmy]Vjkhy1j-yL0jÁX0l&U7jkUgV

(332) 5lgy

(333) a iml&u*l@UVW'n/c7jkU !

(334) TPn u*WYVjkT5Uy)R {L5l|$l # 0l'n jku*l&U;VW&i5W)VW !

(335) T5nV

(336) (lÀ3 S ]/ D6 | y/cy

(337) Vl&u W'n l|5jÁX0jz5l~ jkU;VTvV-wsTØy l n/jkl;y¿R MJT5nV

(338) 58l !

(339) jny]VTPU(l öyl'n jkl;y. ê5 ^h TPU(Pj VjkT5UyLw l'n l3h@(TKyl'U8jkU*T5n 5l'nV

(340) T8(WYX0l T !V

(341) 5l|u*lYVW&ijkT5U*h&TH u 0iml #Pl&R5{L5l 0T0W'iPw WyLVTNWYX0T5jk V

(342) (l 5nl(yl&U5h&l3T !R!-nl&l,S W&U5vV

(343) TNW'U(W@ikcylvy l&imlhYV/j X[l@ikc7V

(344) 5l,3 S ]/ o | h~THu 0iz$l #KR 3h&h&T5n 5jkUNVT V

(345) 5l u lYV

(346) 5T0xa!yl&ÝW@U(xV

(347) (l7h&TPU(Pj V/jkT5Uy|y]V-a[j l&5^l&j V5l' n 5.;a {"} ?RM.e0^v y MJ:i MNMNMJP^ 5Ae5 o S4e ATPnAÀu {"} ?/M.e Àw l'n l aJy l~>Wy 5n Tb0ly)&R MJTPn#V-(ly l&h&T5U5¯yl'n jzly öy l nöjml;yA/ ^ e5/ ^3 S ]/D AW'U5 S3

(348) // o | y [l&h&jml;y7h&T0l #0j-y]VsjkUHyTi a5VjkTPU[R.{(l;yl>5WYVWØw l'n lNa!y l& !

(349) T5ntV

(350) (l>5lYVl'nu jkU0WYV

(351) j TPUT !,V

(352) 5l. 0W'n W&u7l)Vl'n y.h'(W'n W&h)Vl'n jÁjU5vS ]// 6 | jkU;Vl n W&hYV

(353) jkT5UR |U5ic*#u w*W;ya!yl&1 !

(354) T5nV

(355) 5j-y yl'n jkly)R ]V!j-y.Wy)y]a[u8l~sV

(356) (WYNV 51a W'U57Àu 0W'X0lgy jmu8jzimW'n.jkU;Vl'nW&hYV

(357) jmTPU 5n/T 0l'n-V

(358) jkly !

(359) T5n g3^ws5jzh&7j-yLn l&Wy T5U0W~b0iml b0Wyl&7TPU7W,u3ai Vj V-a[5l|T !Ly]V-a[5jklyLn $l 0T5nVl~gjkUgV

(360) 5l|ikj Vl'nWYV-a0n lR . . . {}Q?RMe ú#&£Á)¨¿£&/ú#z£|k©

(361) ¼5 È3[z©+5 u7j-y)y jkTUN5l~h&W'c8nWYVl;y#T! / uH W@U( 5.a1ikl'XPl@i-y¿R{L5lv5l&h~W~c*n W)Vlvh&T5Uy]VW U;V y ^p ^ W'U(V

(362) (l>h&T5n/n l;y 0TPU(PjkU%izj !/l)V/jku*l;y ^ τ4!p @kZù^ÀW n l¯y l&Uy j Vj XPlVTEV

(363) 5lUauvb[l'n7T!vh&T5T5n jkU5W)Vl&Ew7W)Vl'n u7Timl&h)aimly ^ J5^PjkUgV

(364) (l !]jkn y

(365) Vh&T5Tn jkU0WYV

(366) jkT5U8y 05l n l $5o R 6 5. . . .

(367) . . . . &l u7jyy jkTU y [l&hYV

(368) n W%T=!Ý#uNR3{0l3 0l&W'p> 0Ty j V

(369) jkT5U T=!8V

(370) (l"l&u j-y)y jkT0U y 0l~hYV

(371) n W"jzy p5U5TwsUgV

(372) Tvb0lgy l Uy j V/jÁX[lÀVTtV

(373) 5l8!]j nYy

(374) Vh'T5T5n jkU5WYVjkT5U8y 05l&n l|W n/Ta0U57Àu 5 R. 6. ". . →. !. . .

(375) l #Ph&j VWYVjkTPU>y 0l&hYV

(376) n W7T! 5.aJR{L5lgVùn W'Uy j V/jkT5UÝjyAl&U;V

(377) jÁnl&iÁc>U(TPU(o/5l'0l&U5l n WYVl&R[{(l'n l!

(378) TPnl&^ V

(379) 5l W$ 0l&W'nW@U(h&l T! uvai V/j: 0iml bPW&U5y jkU0Pjmh&WYVl~ V

(380) 5l 5n l;y l&U(h&l T=! 5jI! !/l n l&U;V y 0l&h&jzly¿R4{0l 5l&h&T5U;XPTi a5VjkT5U T !>V

(381) 5l $l #0h&j VWYVjkT5U y 0lhYV

(382) n W w W;y9 0l&n !

(383) T5n u7l& h&T5Uy jm5l'n jU V

(384) (WYV+ 0l&W'pöy%l #05jÁbj V ?T5n l'U;V

(385) ~jzW&U7W U57QgW)a!y)y jzW&U8y ($W 0 l l # 5n l;y)yl&gb5c 6 . →. . . . − −

(386) = . − + . . ws5l'n l,^(w W'U5 ?W'n l V

(387) 5l|jUVl'Uy j V]c(^ 0l&W'p 0TKy j V/jkT5U5^0W'U( ikjkU0lÀw7jm;V

(388) 5^5n l;y 0l~hYV

(389) jÁX0l&icKR /U h~TPU(h@iÁaJy jkTU(^l&W~h@ h&TuH 0iml #Pl& y 0lh@jml;yOw*W;y h&0W'n W&hYVl n/jÁl&¢b5c j V y%imjC!lYV/jku*l W&U5 V

(390) 0l 0 l&W'p 0Ty/j VjkT5Uy*T ! l&u7j-y)y jkTU3/#u1*W&U5 → 51a*l #Ph&j VWYVjkTPU4y 0l~hYV

(391) n WR{(l;y l → jkU !

(392) T5n u7WYVjkT5UØw WyÀa!yl&ØVT W;y yl;y y#V

(393) 5l8i ThW&i.l&UX0jÁn T5U5u8l&UV¤T=!.S a!y jkU5V

(394) (l S3]/ D6-3hNy/cy

(395) Vl@u W;y3W n $l !l'n l&U(h&l R. ". . !. . !w75l n lgu7T5n l,V

(396) 5W&UvV-w7Ty 0l&h&jkl;y#W n l 5nl;y l&U;VW'U58j !V

(397) 5l&jÁnh&0l@u7jmhW;i l #Ph@0W&U0l n WYVly|W'nl8ikT(w l'n V

(398) 5W&UNV

(399) 5l8i a[u8jkU0ly h~l@U(hl85l&h&W'c T !.V

(400) 5l V-w T¯ y 0l&h&jkly ^Lij !/l)V/jku*l X0W&iÁa[ly|T ! V

(401) 5l V-w7T8y 0l&h&jkl;y.W'nl|T(bVW'jkU0l&7h&TPU0y jm5l'n jUvV

(402) 5lgy jzu 0ikCj !/jml&7l J;a[WYV

(403) j TPPU . !"$#%'&()&+*-,.0/#213/04(256708. D. : : 9 τ <>−="; ? = : @ τ − ;. w7j V

(404) τ @kZb[l@jkU5vV

(405) 5l|Tb!y l nXPl& iÁa[u8jkU0l;yh;l&U(h&l|l~h&W'c8nWYVl'^ τA V

(406) (ltikj !/lYVjku*l|T !Ll #[h&j Vl~xy l~h@jml;yjk^0W@U0 A j V y u7Ti l !-n WhYV

(407) jkT5U8jI!V5l8!/iÁa[T5n l;y h~l@U(h&l,c0jzl&imy!

(408) T5n.W&iziy 0l&h&jml(yW'n lgjk0l&U;V

(409) jmh&W&i R A j-yh&W&izh)aimWYVl& . a!y jkUvV

(410) 5l|l J;ajkizjÁb0n jÁau h~TPUy

(411) VW'U;V yws5jziml D C− B W'n l !

(412) j V-VjU 0W'n W&u7lYVl'ny)R EF#G7!4(2HIJ768 lYVW'jki-y4h&T5U5h~l'n U5jU5 V

(413) 5l¢y 0lhYV

(414) nTKyh&T 5jkh 5l'X0jmhl Wyw l&izi Wy 5lYVW&jki-y"T5U (T(w y 0l~hYV

(415) n/Ty h~=T 5jkhs5WYVWtw l'n lvTbVW&jkU5l&Ýh&W&U8b0lH!

(416) TaU(Nl&iy¿lYws5l'nl ^ RP!LU5TV#y]VW Vl&8T;V

(417) (l'n]w7j-y l~^5.a W'U(NÀu y l&h&jml;y.w7l'nlgl$#0h&j Vl~NWYVV

(418) (l. LM K . . U5u W@U(1M; R U5u iml~X[l&i-y ^0n l;y 0l~hYV/jÁXPl@ikc!RMJT5n .

(419) 5l&h&W'cOh)a0nXPlØu*lW;y

(420) a0n l&u8l&UV y ^!

(421) iÁa[TPn ly h&l&U5h~ll&u7j-y)y jkTU [l&W'pysWYVAWYbPT(a5V U5u L M → K 3W&U5 !

(422) T5n 5.a[^W'U( 8U5u

(423) !

(424) T5n#Àu w l'n lvjkU;Vl 5n WYVl&0R ?.jI!lYVju*l 7U5u L M →. →. *u l&Wy]a0n l&u*l&U;V yw l'n lgy

(425) VW'n]Vl&H!-n T0u V

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(521) l'n l&U5h&ly7jkU¯V

(522) 0l¯y [l&hYV

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