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Microwave-based microsensor printed on film for the monitoring of environmental or health-related chemical compounds

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HAL Id: hal-01831510

https://hal.archives-ouvertes.fr/hal-01831510

Submitted on 5 Jul 2018

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Microwave-based microsensor printed on film for the monitoring of environmental or health-related chemical

compounds

Prince Bahoumina, Hamida Hallil, Jean-Luc Lachaud, Dominique Rebière, Corinne Dejous

To cite this version:

Prince Bahoumina, Hamida Hallil, Jean-Luc Lachaud, Dominique Rebière, Corinne Dejous.

Microwave-based microsensor printed on film for the monitoring of environmental or health-related chemical compounds. Concours Posters GPU, Jan 2017, Talence, France. 2017. �hal-01831510�

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Laboratoire de l’Intégration du Matériau au Système

>

www.ims-bordeaux.fr

-18 -16 -14 -12 -10 -8 -6 -4 -2 0

1 2 3 4 5 6

S Parameters (dB)

Frequency (GHz)

S21 REF (dB) S11 REF (dB)

S11 2SENS21 (dB) S21 2SENS21 (dB)

Port 1

Port 2

Port 1

Port 2 1st mode: 2 large active zones

2nd mode: 3 large active zones

GPU – Environnements / SIS

Motivations and general purposes

MDA Team

Prince Bahoumina, Hamida Hallil, Jean-Luc Lachaud, Dominique Rebière, Corinne Dejous

prince.bahoumina@ims-bordeaux.fr ; hamida.hallil@ims-bordeaux.fr

Microwave-based microsensor printed on film for the monitoring of environmental or health-related chemical compounds

Proposed chemical gas sensor based on capacitive microwave resonators flexible paper device

Odors:

VOCs (Formol, Toluene) NH3, H2S

Microbiology:

Bacteria, Viruses, Allergen, Parasites, microorganisms

Atmospheric particulate matter:

PM10, PM2.5

Major primary pollutants: Nox-VOCs, CO, NH3, Sox, Toxic metal

-5,49 -5,485 -5,48 -5,475 -5,47 -5,465 -5,46 -5,455 -5,45 -5,445

0 10 20 30 40 50 60 70 80 90 100

S 21 (dB)

Time (min)

SEQUENCE 1 DEVICE 2 S21 SENS (dB) SEQUENCE 2 DEVICE 2 S21 SENS (dB) 0

ppm

500 ppm

0 ppm

500 ppm

0 ppm

1000 ppm

0 ppm

1000 ppm

0 ppm

2000 ppm

Proposed solution : CArbon and Microwave based Ultrasensitive gas Sensors (CAMUS)

The need for miniature sensors, integrated in all environments, highly selective and sensitive, with low cost and low power consumption, is growing more each year, due to the modernization and increasing global industrialization, which increase environmental and health pollution. This pollution concerns 7 million deaths in 2012, according to World Health Organization (WHO). It is known as a source of irritation, decreased lung capacity and odors. Some of these pollutants are considered carcinogenic, among them volatile organic compounds (VOCs) represent an issue as target compounds. In this context and to respond to this problem, we propose the real-time monitoring and quantification sensor for toxic gas, by combining an electromagnetic transduction resonator with a chemical sensitive layer of carbonaceous material in the frequency band from 0.5 GHz to 6 GHz. This platform is suitable for the Internet of Things and embedded systems, which open revolutionary perspectives to the proliferation of sensing and control sites with communicating wireless sensor networks.

2nd resonant mode (4.8 GHz)

Preliminary results of ethanol detection based on stub microwave resonators flexible kapton device

-16 -14 -12 -10 -8 -6 -4 -2 0

0 1000 2000 3000 4000 5000 6000

S 21 (dB)

Frequency (MHz)

DEVICE 2 REF_S21(dB) DEVICE 2 SENS_S21(dB) 1st resonant

mode (0.6 GHz)

Sensitive resonator

Reference resonator

Experimental results

Design & Simulation

Room temperature detection at first resonant mode (0.6 GHz)

Reference resonator

Sensitive resonator

Microwave resonator device

Differential detection

Wireless Communication

Autonomy (Passive )

Network of sensors & Easy integration for IoT applications Carbon materials

sensitive layer

High sensitivity

Totally integrated

Room temperature detection

Ink jet Printing Technologies

Low cost

planar circuits

Flexible substrate

dB

f

f dB

Gas molecules Modification of

microwave resonator response

Variation of the electrical properties of carbon materials

Modification of physico chemical properties

Perturbation of electromagnetic wave Sensitive

resonator

Reference resonator

Reference resonator

response Sensitive resonator

response

∆F

∆|GdB|

Advantages

IoT Gateway Cloud &

Big data base

Sensor node 1

Sensor node 2

EMT Gas & humidity

& Temperature &

pressure Sensor

Wired instrumentation sensor system

Wireless instrumentation sensor system

resonant mode (2.4 GHz) Sensitive

Resonator

Lsub

Wsub W

W = 14 mm ; Wsub = 34 mm L = 17.2 mm ; Lsub = 26 mm

Reference Resonator

Sensitive Layer

Conclusions

Insertion losses increase of -5, -10, -20 mdB for 500, 1000 and 2000 ppm of ethanol vapors respectively

Sensitivity is estimated at -10 μdB/ppm

Absorption and desorption time is about 6 min

Prospects

Make in-depth studies on new samples

Analyze results to better explain the behavior of the sensor physically and chemically

Integration in communicating systems for wireless sensor network and Internet of Things (IoT) applications

Références

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