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7 | 3 6 2 Table of content

T

ABLE OF CONTENT

ACKNOWLEDGEMENT ... 3

ABSTRACT ... 5

TABLE OF CONTENT ... 7

LIST OF SYMBOLS ... 11

CHAPTER 1: GENERAL INTRODUCTION ... 15

SECTION 1.1 – Background ... 16

SECTION 1.2 – Objectives and scope of the thesis ... 21

SECTION 1.3 – Organization of the thesis ... 22

REFERENCES ... 23

CHAPTER 2: PROPERTIES OF EARLY AGE CONCRETE ... 25

SECTION 2.1 – Hardening process... 26

SECTION 2.2 – Early age volume changes ... 28

REFERENCES ... 45

CHAPTER 3: MATERIALS AND METHODS ... 53

SECTION 3.1 – Compositions and mixing procedure ... 54

SECTION 3.2 – Test methods ... 59

SECTION 3.3 – Experimental program ... 65

REFERENCES ... 66

CHAPTER 4: DEVELOPMENT OF AN EXPERIMENTAL STRATEGY FOR THE

MONITORING AND THE MODELING OF CEMENT BASED MATERIALS... 69

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SECTION 4.2 – Design of a revisited tstm system for testing concrete since setting time under

free and restraint conditions. ... 82

SECTION 4.3 – Development of tensile creep rigs ... 94

SECTION 4.4 – How to monitor the modulus of elasticity of concrete, automatically since the earliest age? ... 109

SECTION 4.5 – Testing concrete E-modulus at very early ages through several techniques: an inter-laboratory comparison ... 123

SECTION 4.6 – Creep testing of concrete since setting time by means of permanent and repeated-minute long loadings ... 146

SECTION 4.7 – Modeling basic creep of concrete since setting time... 163

CONCLUSIONS ... 179

REFERENCES ... 184

CHAPTER 5: APPLICABILITY OF ULTRASONIC MEASUREMENT ON THE

MONITORING OF THE SETTING OF CEMENT PASTES: EFFECT OF WATER

CONTENT AND MINERAL ADDITIONS ... 197

SECTION 5.1 – Materials and methods ... 200

SECTION 5.2 – Results and discussions ... 203

CONCLUSIONS ... 211

REFERENCES ... 212

CHAPTER 6: INFLUENCE OF THE WATER/CEMENT RATIO ON THE EARLY

AGE PROPERTIES OF CEMENT BASED MATERIALS ... 215

SECTION 6.1 – Influence Of The Water/Cement Ratio On The Early Age Free Deformation Of Cement Based Materials ... 216

SECTION 6.2 – Effect of water-cement ratio on the viscoelastic behavior of cement based material since setting time ... 225

CONCLUSIONS ... 252

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CHAPTER 7: INFLUENCE OF THE WATER-CEMENT RATIO AND THE

NATURE OF THE BINDER ON THE EARLY AGE PROPERTIES OF CEMENT

BASED MATERIALS BY MEANS OF MULTI-SCALE MONITORING ... 259

SECTION 7.1 – Multiscale monitoring and modeling of the Mechanical properties and the short term creep ... 261

SECTION 7.2 – Multiscale monitoring and modeling of Autogenous deformation and coefficient of thermal expansion ... 287

CONCLUSIONS ... 302

REFERENCES ... 304

CHAPTER 8: MONITORING AND MODELING OF THE VISCOELASTIC

PROPERTIES OF UHPSCC AND CONCRETES WITH HIGH SUBSTITUTION OF

PORTLAND CEMENT... 307

SECTION 8.1 – Experimental program ... 308

SECTION 8.2 – Repeated minute-long loading tests ... 311

SECTION 8.3 – Long duration creep tests ... 317

CONCLUSIONS ... 329

REFERENCES ... 331

CHAPTER 9: COMPARISON BETWEEN VISCOELASTIC PROPERTIES IN

TENSION AND IN COMPRESSION ... 333

SECTION 9.1 – Materials and methods ... 335

SECTION 9.2 – Experimental program ... 336

SECTION 9.3 – Experimental results ... 338

SECTION 9.4 – Modeling of tensile creep ... 346

CONCLUSIONS ... 349

REFERENCES ... 350

CHAPTER 10: GENERAL CONCLUSIONS AND SUGGESTIONS FOR FURTHER

WORKS ... 351

SUMMARY AND CONCLUSIONS ... 351

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ANNEXE ... 357

ANNEXE I – HOMOGENIZATION OF THE E-MODULUS THROUGH SEVERAL

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