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Liquid–liquid dispersion in a continuous oscillatory baffled reactor – Application to suspension polymerization

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Academic year: 2021

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Figure

Fig. 1. Steps and limitation for continuous suspension polymerization.
Fig. 2. Experimental set-up of the column (a) for the liquid–liquid dispersion study (b) for the polymerization tests with FI corresponding to flow controller and TI to the PT100 probe for temperature.
Table 5 covers the different parameters investigated in this sec- sec-tion: throughput, pulsation conditions (amplitude, frequency) and dispersed phase hold-up.
Fig. 3. Droplet size distribution all along the column for different operating conditions for different axial positions (a) Q tot = 10.1 L h ÿ1 , x 0 = 20 mm, f = 0.75 Hz, U = 25%, (b) Q tot = 10.3 L h ÿ1 , x 0 = 35 mm, f = 1 Hz, U = 25% and (c) Q tot = 10
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