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Freezing of water in capillary tubes

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HAL Id: hal-01268781

https://hal.archives-ouvertes.fr/hal-01268781

Submitted on 5 Jun 2020

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Freezing of water in capillary tubes

Alexandre Ponomarenko, Thierry Ameglio

To cite this version:

Alexandre Ponomarenko, Thierry Ameglio. Freezing of water in capillary tubes. 3èmes Journées du

GDR Bois, Groupement de Recherche (GDR). FRA., Nov 2014, Nancy, France. 1 p. �hal-01268781�

(2)

> Perspectives

FREEZING: TWO DIFFERENT TIME SCALES

SUCROSE CONCENTRATION EFFECT

> A variation

> During the first 100 ms, an ice sheet propagates quickly at the interface between the liquid and the tube.

Quick propagation of an ice sheet

Trees are able to undergo several months of cold temperatures every year. This is very surprising since the temperature may go down to -30°C, far below the freezing temperature of water.

A direct consequence is the tree line, the limit in altitude where trees can survive.

How do trees survive the negative tempera-tures, until which critical temperature ? What sets the critical temperature ? What are the freezing dynamics of water in a tree ?

Since trees are not transparent, recording acoustic events is a promising technique to resolve those questions.

> Here we present some aspects of freezing of water in capillary tubes, monitored both with optics and acoustics.

> Context - Motivation

Tree in cold condition

Charrier (2014)

Tree line

Macias-Fauria (2013)

Slow propagation of the ice front

time (ms) x (mm) 100 0 0 10 20

V = 130 mm/s

20 40 60 80 120

> On a time scale of the order of 1 minute, the entire volume of the drop freezes. The freezing front first closes the drop at both ends (1-10s) and then propagates to the center (10-40s). Acoustic events are emitted only in the second step.

time (s) 20 40 10 0

V ~ 0.055 mm/s

x (mm) 30 x (mm) emission of ac oustic e ven ts 0 2 4 6

> Here we quantify the influence of sucrose concentration on the quantity of acoustic events.

The experiment shows a critical sucrose concentration above which there is no more acoustic emissions during freezing. In a tree, acoustic emission would only reflect freezing in the cells below this concentration.

Explore different kind of tubes : open and closed geometries , rigid and flexible tubes, hydrophil hydrophobe surfaces. As in a tree undergoing

freezing, we want to observe the freezing dynamics of a system where water with sugar and pure water are connected by a porous medium.

Work with porous media to understand propagation of freeze between cells and tissues in a tree. 0 5 0,3 1 4 2

T = 25°C

T = -20°C

sucr ose c onc en tr ation (g/L) 1 mm 1 mm porous medium

water with sugar pure water

number of ac oustic ev en ts sucrose concentration (g/L) 0 2 4 6 8 10 0 100 200

FREEZING OF WATER IN CAPILLARY TUBES

Alexandre Ponomarenko

1,2

, Thierry Améglio

1,2 1INRA UMR 547 PIAF, F-63100 Clermont-Ferrand, France 2Clermont Université, Université Blaise Pascal, UMR 547 PIAF, 63177, Aubière, France

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