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TEM characterization of turbostratic and rhombohedral BN interphases synthesized by chemical vapour infiltration in SiC/SiC-Si composites

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Academic year: 2021

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Table 1. Name and corresponding CVI temperature, CVI diluent gas and interphase thickness for each  sample
Fig. 1. OA and L c  microstructural parameters calculated from SAED patterns for 9/H/T, 9/N/T, 12/H/T and 12/N/T  BN samples and SAED patterns for 9/H/T (green frame) and 12/H/T BN samples (red frame)
Fig. 3. Filtered HRTEM images of (a) the fibre-interphase interface in 12/H/t sample, (b) lenticular cracks and (c)  edge of a crystallite in 12/H/T sample
Fig.  5.  TEM  observations  of  9/N/t  sample:  (a)  DF  image,  (b-d)  HRTEM  images  of  the  interphase,  the  fibre- fibre-interphase interface area and a BN crystallite, respectively
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