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Conductivity and rupture in crack-deteriorated systems
A. Gilabert, M. Benayad, A. Sornette, D. Sornette, C. Vanneste
To cite this version:
Conductivity
and
rupture
in
crack-deteriorated
systems
A.
Gilabert,
M.Benayad,
A.Sornette,
D. Sornette and C. VannesteLaboratoire de
Physique
de la Matière Condensée(*),
Faculté des Sciences, Parc Valrose, 06034 Nice cedex, France(Reçu
le 22février
1989, révisé le 2 octobre 1989,accepté
le 5 octobre1989)
Résumé. 2014 La conductivité
électrique
et la force de rupture desystèmes
modèles fissurés à deux dimensions sont étudiéesexpérimentalement.
Deux cas sont considérés. Dans le cas 1, les fissuressont
disposées
aléatoirement sur les liens d’un réseau carré dessiné sur le continuum. La taillefinie de nos
systèmes
permet àpeine
d’atteindre lerégime critique
de lapercolation
et on mesureplutôt
un comportement décrit par des théories de milieux effectifs. Dans le cas 2, lespositions
etles orientations des fissures sont choisies aléatoirement sur le continuum
(fromage
« bleud’Auvergne
»).
Dans ce cas, de forts effetsd’écrantage
permettent d’atteindre lerégime
critique
et de mesurer les exposantscritiques
correspondants.
Nous avonscomparé
ces mesures avec des résultatsthéoriques
récentsqui
prennent en compte les différents modes de déformation à l’extrémité des fissures. Enparticulier,
le flambement de feuilles mincesjoue
un rôleimportant
etpeut
changer
les exposantscritiques.
Abstract. 2014Experimental
results on theconductivity
and ruptureproperties
of two-dimensional continuum crack deteriorated model systems arepresented.
Two different systems are considered. In case 1, cracks arerandomly positioned
on the bonds of aregular
square lattice drawn on the continuous system. Our finite size systemsbarely
reach the criticalpercolation regime.
The results rathercorrespond
to a mean fieldregime
which may be describedby
effective medium theories. In case 2, crackpositions
and orientations arerandomly
chosen in the 2D continuum(«
bluecheese »).
In this case, strongscreening
effects allow us to obtain the criticalregime
and to measure thecorresponding
critical exponents. The measurements arecompared
with recenttheoretical results which take account of the different modes of deformations
occurring locally
atthe crack level. In
particular, buckling
in thin foils is found to be animportant
deformation mode which screensefficiently
the stress enhancement at thetips
of the cracks,thereby changing
the critical exponents. ClassificationPhysics
Abstracts 05.70J - 72.60 - 62.20M 1. Introduction.Understanding
thetransport
properties
ofheteregeneous
or random media constitutes amajor challenge
ofpresent
research activities and also receivesstrong
incentive in the field ofapplied
andengineering
science due to the many real andpotential applications. Among
theheterogeneous
media, systems
containing
crackplay
a fundamental role : cracks are the(*)
CNRS URA 190.JOURNAL DE PHYSIQUE. - T. 51, N’ 3, 1cr FÉVRIER 1990
primary
enemy tofight
in order toprevent
fatigue
andeventually
failure of mechanicalsystems.
Damage
occurs in asystem
by
theapparition
of micro-cracks whicheventually
coalesce and create a macro-crack which may destabilize and lead toglobal
rupture.
At anotherlevel,
it isthrough
arrays of cracks that water or oilpermeate
in soil and can be recovered. On the otherhand,
cracks or ratherfaults,
asthey
are called in this context,control the brittleness of the earth crust and thus the occurrence of
earthquakes.
One could think of many other relevantexamples
where cracksplay
animportant
role.Experimental
and theoretical studies of crack deterioratedsystems
haveessentially
beendeveloped
in the field of theoretical andapplied
mechanics. Thecontinuing
refinement of theseapproaches
is thesubject
of a very intense research effort in this field.However,
focus has beenput
onsingle
or few crackproblems
likeperiodic
lattices of cracksby using
exactanalytical
methods. For dilute crackconcentration,
homogeneization
approaches
have been used such as, forinstance,
effective medium theories[1-3]
or continuousdamage theory
[4].
Theseapproaches apply
when certainsymmetries
exist or when the concentration of cracks isnot too
large.
However the weak crack concentration limit does notalways apply
in manysystems
ofphysical
and industrial interest. This is our main motivation forstudying
the other limit ofstrong
heterogeneity
within the frame of thepercolation
model. A second motivation is found from the field of statisticalphysics
where it was realized that the critical behaviour ofelectrical
conductivity,
fluidpermeability, elasticity
modulus and failure threshold wasdifferent in discrete-lattice
percolation
and in a class of continuouspercolation
models(«
Swiss cheese » model[5])
pointing
out the existence of at least twouniversality
classes oftransport
phenomena
inpercolation.
Percolation of cracks(termed
« blue cheese » model in[6]
has been shown toyield
still another critical behaviour worthstudying
for its own sake.Many
studies have been devoted to the theoreticalprediction
of theconductivity
in disorderedsystems,
but less work has been devoted to consideration of thesepredictions
onthe
experimental
side[7].
Benguigui
[8]
has measured the electricalconductivity
G of Cu and Al foilspunched
with holesrandomly
distributed on a square lattice and on a continuum nearthe
percolation
threshold. He finds that G oc(1 -
N INc)’
with t = 1.1 ± 0.2 where N is thenumber of holes. Sofo et al.
[9]
have measured the conductance ofrandomly punched
metallizedmylar
sheets and find the criticalconductivity
exponent t
= 1.4 ± 0.2. Lobb andForester
[10]
find the criticalexponent t
= 1.24 ± 0.13 for holes distributed on a continuum.All these results confirm the
prediction
ofHalperin et
al.[5]
that t has the same value fordiscrete lattice
percolation
network or for disordered continuumsystem
in two dimensions. In thefollowing,
wereport
experimental
results on theconductivity
andrupture
properties
of two-dimensional continuum crack deteriorated model
systems.
In section2,
we define moreprecisely
the twotypes
ofsystems
which have been studied : in case1,
cracks arerandomly
positioned
on the bonds of aregular
square lattice drawn on the continuoussystem.
In case
2,
crackpositions
and orientations have random values on the continuoussystem.
Thisis the « blue cheese » model introduced in reference
[6].
Thegeometrical
properties
of thesesystems
which arereported
in aseparate
paper[11]
and the theoreticaltransport
properties
which have beenpreviously analysed
[6]
arebriefly
summarized in section 2. In section3,
the measured electricalconductivity
and mechanicalrupture
properties
of the two models aredescribed and
compared
topredictions.
In the first case, the finite size of oursystem
barely
allows us to reach the critical
percolation regime.
Both electrical andrupture
properties
could beexplained
from effective mediumapproaches.
In the second case,strong
screening
effects allow us to obtain the criticalregime
forsystem
sizes of the same order as in the first case andto measure the
corresponding
criticalexponents.
The results of therupture
arecompared
with the theoreticalpredictions
of the « blue cheese » model which takes account of the differentis found to be an
important
deformation mode which screensefficiently
the stressenhancement at the
tips
of thecracks,
thereby renormalizing
the criticalexponents
to their value for discrete lattices.2. Theoretical
properties
of crack-deterioratedsystems.
2.1 GEOMETRICAL PROPERTIES OF THE PERCOLATION MODELS. - We restrict ourselves to
the two-dimensional space
displayed
infigure
1. In model1, empty
rectangular
holes oflength
« a » withnegligible
width are distributedalong
the bonds of a square lattice drawn on a uniform electric or elastic medium. Inmodel 2,
the cracks arerandomly
distributed inposition
and orientation in a surface of size L x L. As the number n =N /L 2
of cracks perunit surface
increases,
apercolation threshold ne
is reachedcorresponding
to thegeometrical
deconnection of thesample
inmultiple fragments.
We denotenc(1)
andnc(2)
for models 1 and 2respectively.
The relevance of these blue-cheese models issuggested
from the crackstructure of many mechanical
[12] (damaged
crystals,
solids,
ceramics,
rocks...)
and naturalsystems
[13] (arrays
of faults ingeology
in relation to oil recovery,geothermics
andearthquakes
[14] ... )
which often consist in random arrays of micro-cracks ofvanishing
width. Thegeometrical properties
of model 1 are those of the discrete bondpercolation
model. Inparticular,
it is knownexactly
thatnc ( 1 )
= 1/2. Formodel 2,
previous
numerical studies haveshown that
nc (2 )
decreases as the cracklength a
increase i. e.ne(2) =
Ca - 2
[15-17],
resulting
in the existence of a
quasi-invariant
C =nc a 2
independent
of a. The intuitive idea is that eachcrack defines an excluded surface of the order of
a 2
around it.Hence,
the criticalpercolation
thresholdnc (2 )
corresponds
to the presence of a constant average number of cracks in eachtypical
surfacea2.
The value of the invariant C has been estimatedby
a number of authors. Arecent estimate
[11]
obtained from a carefulanalysis
of finite size effectsgives
C = 5.640 ± 0.005 for the
asymptotic
limit a - 0.Thus,
nearthreshold,
the number of cracks in a surfacea2
is of the order of the invariant C -- 5.6 in contrast to the value « 1 » in the samesurface for model 1. In other
words,
almost six times as many cracks are needed in model 2compared
to model 1 to reach thepercolation
threshold,
all other valuesbeing equal.
Fig.
1. - Differenttypes of chosen crack distribution.
a)
case 1 : cracks arerandomly
positioned
on the bonds of aregular
square lattice.b)
case 2 : crackpositions
and orientations arerandomly
chosen in the 2D continuum.2.2 TRANSPORT PROPERTIES. - In the so called « Swiss cheese »
model,
Halperin et
al.[5]
used ascaling
analysis
to estimate various criticalexponents
of thetransport
properties
(conductivity,
permeability, Young
modulus...)
ofsystems
punched
with holes. In the « bluemedium is the space between
randomly placed
clefts. In both cases it was found that the critical behavior of the electricalconductivity
is the same for model 1(discrete lattice)
and model 2(continuum).
The electricalconductivity obeys
the power lawM/M0 oc (p - pc)t
nearthe
percolation
threshold with the universal value t = 1.300 foundnumerically
for twodimensional
systems
[18].
2.3 RUPTURE PROPERTIES. - In
a
system
containing
cracks,
brittlerupture
following
theGriffith mechanism will occur under tensile stress
(mode
1[19]).
Thisrupture
scenario isexpected
to beprominent
for cracks withvanishing
width. In this failuremechanism,
thestress concentration at the apex of a crack tends to open the two
edges
and tolengthen
thecrack,
thusleading
to failure. This mechanism must be considered when thetips
of the cracksare
sharp,
i.e. withoutscreening
due forexample
to the presence ofrounding
or of acavity
atthe
tips
of the cracks. The Griffith criterion states that a crackgrowth
isgoverned by
thebalance between the mechanical energy released and the fracture surface energy
spent
as the crackpropagates.
In the blue cheesemodel,
each crack is surroundedby
many other cracks which interact withit,
locally
enhance or screen the stress concentration at the cracktip.
It has beenargued
in reference[6]
that the Griffith criterion could be extended in the presence of these interactions and theanalysis
could be reduced to thestudy
of thegeneric configuration
involving
one crack in closeproximity
(to
within a distance5)
to a border createdby
anothercrack
(Fig. 2).
Theanalysis
of the stress enhancement in thisconfiguration
leads to theprediction
of the critical behaviour of therupture
threshold. Ingeneral
the criticalexponent
of the
rupture
is distinct from its discretecounterparts
andcrucially depends
upon the deformation mode. However if the sheet isthin,
buckling
(out
ofplane
deformation)
occurs inorder to relax more
efficiently
thein-plane
elastic stresses[6].
In this case, it has been shownthat
buckling
suppresses thepredicted
additive correction(equal
to1/2)
to the failure criticalexponent
f
= dv due to stress fluctuations at the cracktips
in this continuous crackpercolation
model(d
is thedimensionality
of thesystem
and v is the criticalexponent
of the correlationlength).
Hence,
one recovers the discrete latticeexponent
for the criticalbehaviour.
This value of the failure
exponent
f
= d v in the discrete case stemsdirectly
from the node-link-blob structure of thepercolation
latice near threshold. The force feltby
a bond in aFig.
2. -macro-link is
proportional
to 03BEd-1
due
to enhancementcoming
from the bottleneck effect that the force is transmittedonly by
the macro-linksseparated
from each otherby
thetypical
distance §.
An additionalfactor e
appears which stems from the lever arm effect which increases the local forceacting
on a microbond to a valueproportional
to 03BEd~
(Nc -
N)d"
The failure is thusproportional
to 03BE - d
thereby yielding
therupture exponent
d v[20].
3.
Expérimental
results.We have
performed
electricalconductivity
andrupture
stressexperiments
[21]
on aluminium sheets of thickness - 14 )JLm to 25 um andtypical
size 30 x 30 cm. Each sheet is deterioratedby
N identical craks of samelength
in the range a = 1.5 to 3 cm and distributedfollowing
tothe rules of model 1 or 2. The cracks are cut with a thin blade and the width w of the cracks are
negligible
ascompared
to theirlength
a(w a/100).
3.1 ELECTRICAL CONDUCTIVITY OF THE CRACK PERCOLATION MODELS. - To the best of
our
knowledge,
no suchexperimental
results have beenreported previously
in crack deterioratedsystems.
Cracks canrepresent
forexample
the lines of fractures in rocks thatmust be avoided for an electrical current to pass
through
thesystem.
Figure
3a(resp. 4a)
shows the variation of the normalized conductanceM1 (N)/M1 (0)
(resp.
M2(N)/M2(0))
as a function of the reduced crack numberN/Nc
for model 1(resp.
formodel 2)
where cracks are distributed on a lattice(resp.
on acontinuum).
In case 1(resp. 2),
Ne
isapproximately equal
to 340(resp. 490).
It is clear thatN c2 >- N cI
since there is no« excluded surface » effects in model 2 in contrast to model 1 in which cracks are allowed to
be in contact to others
only
by
oneextremity.
This hasalready
been discussed in section 2.1. Note that the twofigures
are notdirectly comparable
since the sizes of the aluminium sheetswere different for each
system.
Note that the
slopes
at theorigin
of the two curvesM1 (N ) /M1 (0 )
andM2(N)/M2(0)
are notequal,
contrary
to what one couldexpect
naively
on the basisthat,
in this « isolated crack »regime,
the crackdensity
is so small that interactions between different cracks can beneglected.
The difference can be traced back to the fact that the decrease of theconductance,
inducedby
the addition of asingle
crack oriented with anangle 40
withrespect
to the averagehorizontal
equipotentials,
is a non-linear function of0.
Weexpect
the conductance todepend
on the first moments
of 0
which are different in the two models. Forexample,
in model1,
thesecond moment is
~2) =
(’TT/4)2=0.617
whereas inmodel 2,
one must take the averagevalue
(~ 2)
over allpossible
crack orientations between 0 and7r/2
whichgives
~> 2) = (ir /2 )2 /3 ~
0.822. Note that thisproblem
is related to the Einstein correction for theviscosity
in asuspension
of rods as a function of the concentration of rods.As the number of slits
increases,
the behaviour ofM1 (N )
becomes even more different from that ofM2 (N ).
One can seeclearly
theupward
curvature ofM2 (N ) in
figure
4a whereas thisphenomenon
canonly
be seen infigure
3a forM1 (N )
in thevicinity
ofNc.
We propose toexplain
this difference from the fact thattransport
properties
of model 2 are controlledby
strong
screening
effects between cracks[6,
21,
22]
coming
from the existence ofoverlapping.
Indeed,
nearthreshold,
the number of cracks in a surfacea 2
is of the order of the invariant C .=: 5.6 inmodel 2,
in contrast to the value « 1 » in the same surface for model 1. We thusexpect that,
for a same value ofa/L,
ratio of the cracklength
over thesystem size,
model 2will sooner enter the critical
region,
as observedexperimentally.
This
explains
why
we have been able to reach thescaling regime
forM’1 (N )
in our finitesamples only
in thevicinity of N c :
anupward
curvature can be observed nearNc
infigure
3a,
and
increasing
fluctuations are observed in thisregion. Trying
to extract a criticalexponent
Fig.
3. - a)
Normalized conductance(N)(N)/M1
(0 )
of an aluminium sheetpunched by
cracks as afunction of the number N of cracks for a distribution on a square lattice
(model 1).
Threeexperiments
are
reported corresponding
to three different realizations of crackconfigurations
all other parametersbeing
fixed. In theseexamples,
the system size is 30 x 30 cm, thelength
of the cracks isa = 1.5 cm and the
percolation
threshold is found nearNc _
330 for all three realizations. Thesuperposition
of the three curvesgives
an idea about theuncertainty
of the measurements. The continuous linecorresponds
to the average values of the three measurements.b)
Logarithm
of the normalized conductanceM1(N)/M1(O)
averaged
over three measurements(continuous
line inFig.
3a)
versus
Log
(Ne - N )
for a distribution of cracks on a square lattice. Thestraight
lines 1 and 2 have aslope respectively equal
to 1 and 2.averaged
over the threeexperiments presented
infigure
3a as a function ofLog
(Nc 2013 N )
Fig.
4. - Normalized conductanceM2 (N )/M2 (0 )
of an aluminium sheetpunched by
cracks as a function of the normalized number of cracks for a continuum distribution :a)
linear scale,b)
log-log
representation
near thepercolation
threshold of the average over twoexperiments.
In thisexample,
thesystem size is --, 30 x 30 cm, the
length
of the cracks is a = 3 cm and thepercolation
threshold isNc
= 490.with t = 1.3 ± 0.2. A similar fit carried over for each of the three
experiments gives
valuesranging
from 1.2 to 1.4confirming
this result. Note that we havepresented
these fits forcompleteness
but remain aware of their limited valuecoming
from the smallness of the rangeover which
they
have been obtained.In model
2,
thescaling regime
isclearly
observed and a measure of theexponent t
can bemade with better confidence than for model 1. In
figure
4b,
thelog-log
plot
version offigure
4a ispresented
from which we deduce the criticalexponent t
= 1.4 ± 0.1 near thepercolation
threshold,
also inagreement
with the theoretical value 1.3[5, 6].
Localspatial
fluctuations ofconductivity
inducedby
the continuum do not appear tochange
theconductivity
criticalexponent
from its discrete value in two dimensions.3.2 MECHANICAL RUPTURE PROPERTIES OF THE CRACK PERCOLATION MODELS. -
Scaling
laws in
rupture
ofpercolation
models haverecently
been much studiedtheoretically
[23].
Yetexperimental
results are scarse. Forexample, Benguigui et
al.[24]
have studied therupture
stress of Cu and Al foils
punched
with holes distributed at random on a square lattice.They
find that the
rupture
forceF,
follows the behaviourF, -
(1 -
N /Nc )f
withf
= 2.5 ± 0.2which compares well with
prediction f
= 2 v = 2.66.To our
knowledge,
noexperimental
results ofrupture
on crack deterioratedsystems
have beenreported
previously.
Theexperimental
set-up
isrepresented
infigure
5. One bar is fixed and an external force F isapplied
to the other mobile bar.Figure
6arepresents
the failure threshold stressFr
for model 2 as a function of the number of cracks. We see that a smallnumber
of
cracks decreasesmarkedly
F,.
This decrease isstronger
for therupture
stress than for theconductivity
and can be understood from the fact that therupture
stress is sensitive tohigh
order moments of the distribution of the stresses. At lowconcentrations,
the failurethreshold
could,
inprinciple,
be obtained from an effective mediumapproach
[2]
which translates into the mechanical context the ideasdeveloped,
forexample,
in the determinationFig.
5. -Experimental
set up which has been used for the measurement of the rupture force threshold.felt
by
agiven
crack is considered as the sum of the extemalapplied
stressplus
the stresscreated
by
the presence of all the other cracks. Due to the slow decrease(r-
2)
of thedipole
stress created
by
a crack as a function ofdistance r,
one must take into account thecontribution of many cracks
[2].
The method of reference[2]
is based on thesuperposition
technique
and the ideas ofself-consistency applied
to the average traction on individualcracks. In
principle,
ityields approximate analytical
solutions for the stressintensity
factoraccurate up to
quite
close distances between cracks.However,
itsimplementation
isquite
cumbersome. We do nottry
to compare our results with thisapproach
and rather focus on thecritical behaviour near the
percolation
thresholds where all effective medium theories areFig.
6. -Rupture
force thresholdFr
as a function of the number of cracksrandomly
distributed on acontinuum
(model 2) : a)
linear scale ;b)
log-log representation
near thepercolation
threshold for different cracklengths
ashowing
an averageslope
of 2.6. The broken linecorresponds
to theslope
3.16.The behaviour of the failure threshold in models 1 and 2 are different. This is due to the
sensitivity
of failure to the « weakest »part
of thesystem
or in other words to thelargest
and« more
dangerous »
defectoccurring
in thesystem
[22, 25].
Dangerous
defects are assembliesof
neighboring
cracks which interactconstructively
so as to create astrong
tip
enhancementfactor. Due to the different
topology
of the twomodels,
oneexpects
[and
weverify]
that thefailure threshold
decreases,
atfirst,
morerapidly
with N for model 1 than for model 2. This is due to the fact that all cracks weaken thesystem
efficiently
in model 1. Furthermore there is alarger probability
for the occurrence ofadjacent
cracks which reinforce each other in model 1 due to its on-lattice construction than in the off-lattice model 2.In the
vicinity
of thepercolation
threshold,
we measure, on thelog-log plot
offigure
6b,
arupture
exponent
Fm
= 2.5 ± 0.2 in agreement with theexpected
result 2 v = 2.66 formodel 2. It is remarkable that we are able to reach the critical
regime
in such smallsystems
(N
1000 ).
This can beexplained by
the very efficientscreening
(also
at work in theconductivity
of section3)
of the stress concentrationby
the numerous random crackssurrounding
each crack. The result is the same for a variant of model 2 in which thepositions
of the cracks are random but their orientation can be ±7r/4
withrespect
to the direction of theapplied
stress.Let us mention an
interesting
observation made on thesystem
during
itsrupture.
As weapply
anincreasing
tensile stress as the two ends of thesheet,
we observe acomplex buckling
and a marked
tearing
of the sheet. This is due to the fact that themacroscopic
2d-plate
is notrigidly clamped, and
because of its smallthickness,
its elastic curvature modulus is very small(proportional
to e3
where e is the thickness of thefoil).
It ispreferable
for the elasticplate
tobuckle out of the
plane
in order to relax thein-plane
elastic stresses. Thescreening
of the strainby buckling
is so efficient that one recovers the discrete-latticeexponents
f m
= du = 2.66[6].
Withoutbuckling,
thepredicted
exponent
should bef m
= 3.16[6]
andwould
correspond
to the dashed line infigure
6b,
which isclearly
not suitable forfitting
the data.The results of the failure threshold for model 1 are
presented
infigure
7. We measure anapparent
failureexponent
around 1.4 ± 0.2 which is very different from theexpected
value 2.66. We believe that thisapparent exponent
is thesignature
of the crossover from a meanfield behaviour to the critical
regime.
As for theconductivity problem,
stress concentrationscreening
is much less efficient in this model than in model 2 and finite size effects are morestringent.
We have not tried to uselarger
systems
because of theprohibitive
time needed toprepare them.
Indeed, contrary
to the case of theconductivity,
one needs a different foil foreach measurement
point
since each determination of the failure thresholddestroys
thesample.
Fig.
7.- Rupture
force thresholdFr
as a function of the number of cracksrandomly
distributed on the bonds of a square lattice. Thelength
of the cracks is a = 3 cm.4. Conclusion and
perspectives.
the on-lattice models 1 is more akin to that of an effective medium
clearly
outside the criticalregime
because of the finite size of oursystems, except
in the closevicinity
of thepercolation
threshold. The difference between the two models stems from different
screening
of the stressenhancement
by
neighboring
cracks whichchange
thesensitivity
to finite size effects. In asequel
work,
we intend toexplore
theregime
of failure in the absence ofbuckling
deformation and toverify
the existence of a directedpercolation
threshold for the mechanical behaviour.Acknowledgments.
We thank Dr. P. Sibillot for technical assistance.
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