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Characterization of the Polylactic acid stretcheduniaxial and annealed by Raman spectrometryand Differential scanning calorimetry

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Academic year: 2021

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International Conference on Advanced Functional Materials and Composites 2018

Characterization of the Polylactic acid stretched uniaxial and annealed by Raman spectrometry

and Differential scanning calorimetry

A. Bouamer, A. Younes, M. Zergoug, A. HAMOUDA

Abstract : in this work, we have been interested in the characterization of the effect of heat treatment and mechanical treatment on the crystallinity of a polylactic acid (PLA) film by two techniques, DSC and Raman spectroscopy. the results obtained by the DSC for the stretched film shows the appearance of a broad peak of crystallization around 120 ° C, a rise in melting peak in a significant way, which shows that the uniaxial stretching has increased the crystallinity of the PLA, whereas for the annealed film appearance of a double melting peak. The results obtained by Raman spectroscopy show new peak appears at 922 cm?1 after stretching process, indicating crystallization process occurs.

Keywords : Raman, DSC, PLA, crystallinity

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