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A Trapped Magnetic Field Over 5 T in Doped Bulk MgB2 Obtained by ex-situ Spark Plasma Sintering

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HAL Id: hal-01281127

https://hal.archives-ouvertes.fr/hal-01281127

Submitted on 7 Mar 2016

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A Trapped Magnetic Field Over 5 T in Doped Bulk

MgB2 Obtained by ex-situ Spark Plasma Sintering

Kévin Berger, Dan Batalu, Gheorghe Aldica, Petre Badica, Thomas Karwoth,

Xian Lin Zeng, Michael Koblischka, Bruno Douine, Jean Lévêque

To cite this version:

Kévin Berger, Dan Batalu, Gheorghe Aldica, Petre Badica, Thomas Karwoth, et al.. A Trapped Magnetic Field Over 5 T in Doped Bulk MgB2 Obtained by ex-situ Spark Plasma Sintering . 5th In-ternational Conference on Superconductivity and Magnetism - ICSM2016, Apr 2016, Fethiye, Turkey. p. 602, ID 556. �hal-01281127�

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A Trapped Magnetic Field Over 5 T in Doped Bulk MgB2

Obtained by ex-situ Spark Plasma Sintering

K. Berger1, D. Batalu2, G. Aldica3, P. Badica3,

T. Karwoth4, X. L. Zeng4, M. R. Koblischka4, B. Douine1, and J. Lévêque1.

1 University of Lorraine, GREEN, 54506 Vandoeuvre-lès-Nancy, France

2 University Politehnica of Bucharest, 060042, Bucharest, Romania

3 National Institute of Materials Physics, Atomistilor, 077125 Magurele, Romania

4Saarland University, Institute of Experimental Physics, 66123 Saarbrücken, Germany

Contact e-mail: kevin.berger@univ-lorraine.fr

The advantage of the very low density of MgB2 bulk samples must be taken into

consideration and, the generation of strong magnetic flux densities using MgB2 should be

investigated. It was shown in [1] that the organometallic addition to MgB2 of Ge2C6H10O7

greatly enhances the pinning forces, leading to higher critical current density Jc and

irreversibility field Hirr in the added sample compared to pristine MgB2, Fig. 1(a). All the

samples were produced by ex-situ Spark Plasma Sintering. In this contribution, we have studied the trapped magnetic field in samples of 20 mm in diameter and 4 mm high, but also in a stack of 6 of these samples leading to a total height of 24 mm. Field Cooling experiments were carried out at temperatures from 12 K to 30 K. The trapped magnetic field inside the stack of 6 samples and at the center of the surface are reported, Fig. 1(b).

5 10 15 20 25 30 35 0 2 4 6 8 10 MgB2 MgB2(Ge2C6H10O7)0.0014 Hir r (T ) T (K) -5 -4 -3 -2 -1 0 1 2 3 4 5 0 1 2 3 4 5 6 7 Trapped magnet ic f iel d, B tr ap (T)

Applied magnetic field, Bapp (T)

12 K 0.01 T/min 12 K 0.02T/min 20 K 0.01 T/min 20 K 0.1 T/min 30 K 0.1T/min 30 K 0.5 T/min

Fig. 1: Irreversibility field Hirr of a pristine MgB2 and of a doped MgB2 (a), and the measured trapped

magnetic field at the center of the surface of a stack of 6 samples of 20 mm diameter & 4 mm high (b). According to the obtained values of trapped magnetic field greater than 5 T at 12 K, and 4 T at 20 K,to their very low density and to their ease of manufacturing, doped bulk MgB2 with

Ge2C6H10O7 are really interesting for the intended applications.

References

1.D. Batalu, G. Aldica, S. Popa, L. Miu, M. Enculescu, R. F. Negrea, I. Pasuk, and P. Badica,

High magnetic field enhancement of the critical current density by Ge, GeO2 and

Ge2C6H10O7 additions to MgB2, Scripta Mater. 82 61 (2014).

Figure

Fig. 1: Irreversibility field H irr  of a pristine MgB 2  and of a doped MgB 2  (a), and the measured trapped  magnetic field at the center of the surface of a stack of 6 samples of 20 mm diameter & 4 mm high (b)

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