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Mechanical behaviour of adhesively bonded ASTERM ablative TPS after Plasma-jet testing

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CONCEPT OF A SAMPLE-RETURN VEHICLE FOR BALLISTIC EARTH RE-ENTRY

IF Carrier

Filling Foam

FS Structure

FS TPS Lid TPS

Front Energy absorbing material

Rear Energy absorbing material Lid structure

Internal insulation

Internal structure

Sample Canister AFT TPS

FP7/SPACE: Activity 9.2.1 Strengthening of Space foundations / Research to support space science and exploration - SPA.2009.2.1.01

The research leading to these results has received funding from the European Union Seventh Framework Programme (FP7/2007-2013) under grant agreement n 241992 EADS/ASTRIUM, Fr supplied the ASTERM material and the plasma-jet test was carried at the Sirocco facility of CIRA, Italy

Main characteristics of a ballistic Earth re-entry. Effective max. total heat flux is about 11.6MW/m

2

, max. velocity 12.3km/sec (47.5Mach), total heat energy about 250MJ/m

2

.

T im e [s]

HeatFlux[kW/m2] Mach Velocity[m/s]

Altitude[km]

0 10 20 30 40 50 60

0 2000 4000 6000 8000 10000 12000 14000 16000

10 20 30 40 50

0 1000 2000 3000 4000 5000 6000 7000 8000 9000 10000 11000 12000 13000

0 20 40 60 80 100 120 C onvective R adiative total M ach V e locity Z

1 2 3 0 0 m /s

3 2 .3 1 4 5 .7

V = 1 2 3 0 0 m /s Z = 9 0 .0 8 km

1 1 6 0 0 kW /m2

V = 1 0 8 9 1 m/s Z = 5 7 .4 8 km M = 3 3 .6 4 8 8 3 2 kW /m2

2 9 3 2 kW /m2

http://www.rastas-spear.eu/

FP7/SPACE/241992 1/9/2011 – 30/10/2012

“Radiation-Shapes-Thermal

Protection Investigations for High

Speed Earth Re-entry”

Mechanical behaviour of adhesively bonded ASTERM ablative TPS after Plasma-jet testing

G. Vekinis and A. Marinou

Institute of Materials Science, NCSR Demokritos, Greece gvekinis@ims.demokritos.gr

Bending strength of ASTERM before and after plasma tests at 5MW/m2

0.00 0.50 1.00 1.50 2.00 2.50 3.00

Virgin ASTERM, loading vertical

to fibres Top char, loading vertical

to fibres Virgin ASTERM, side,

spec. cut horizontally

Side char, spec. cut horizontally

Virgin ASTERM, side,

spec. cut vertically

Side char, spec. cut vertically

Transverse Rupture Strength, MPa

Bending strength of charred ASTERM from the top and the side surface (specimens cut both horizontally and vertically) in comparison with the strength

values measured on similar size specimens on virgin ASTERM Cross section of an adhesively joined ASTERM (supplied by EADS/ASTRIUM) specimen after

Plasma jet testing at 5MW/m2 for 12 seconds at the Sirocco facility at CIRA. Total recession at top is about 2mm, it is fairly uniform and <0.5mm on the sides. Charred region varies from 6 to 12mm.

Recession of the adhesive is slightly larger (photo on top left). The adhesive used was an RTV Silicone elastomeric rubber mixed with small amount of ASTERM powder

ASTERM-adhesive interface in charred region

Virgin ASTERM-adhesive interface ASTERM-

loaded adhesive in charred region The ASTERM-

loaded adhesive remained well bonded after testing with minimal additional recession

ASTERM in charred region

Virgin ASTERM Bending tests of some

adhesive joints tested.

Transverse rupture strength decreases by adding ASTERM powder but increases with curing time.

No decohesion was noted at the interfaces so the results reflect the actual maximum extension during bending of the adhesives tested and range from about 150% in the case of adhesive A + ASTERM after 24 hrs to 450% in the case of one of the adhesives as supplied.

Maximum tensile elongation in Bending

0 50 100 150 200 250 300 350 400 450

0 5 10 15 20 25 30

Curing time, hrs

Max Tensile elongation, %

Adhesive A Adhesive A +7.5%AST Adhesive A +15%AST

Transverse Rupture Strength - Adhesive A

0 0.5 1 1.5 2 2.5 3 3.5

0 5 10 15 20 25 30

Curing time, hrs

TRS, MPa

Adhesive A Adhesive A +7.5%AST Adhesive A +15%AST

Sequence of photos showing the gradual deformation of adhesive-joined ASTERM under direct shear loading and its correspondence on the load-displacement curve. Original joint thickness was 1mm. The very good adhesion and very large extension at final failure is clearly visible.

Bending strength at liquid Nitrogen temp (-196oC) of various adhesives

Bending tests in liq. Nitrogen

58.5 76.7

63.8 54.3

122.6

0.0 20.0 40.0 60.0 80.0 100.0 120.0 140.0

1

TRS (MPa)

Adhesive B+15%AST Adhesive B Adhesive A +15%As"

Adhesive A CV1142

Schematic of the directly shear test and typical load-displacement curves (below)

Interim Conclusions:

• Commercially available RTV silicone elastomeric rubber adhesives perform satisfactorily for joining and bonding ASTERM ablative TPS

• Room temperature and cryogenic mechanical behaviour are sufficient for use for joining and bonding ASTERM tyiles to various substrates including aluminium, CFRP etc

• Post Plasma-jet analyses show that recession of ASTERM and of

ASTERM-containing adhesives is minimal and the remanent

strength of the ASTERM (and the joints) is satisfactory

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