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Solute-dislocation interactions in Al-Mg alloys at elevated temperatures

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HAL Id: jpa-00245869

https://hal.archives-ouvertes.fr/jpa-00245869

Submitted on 1 Jan 1988

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Solute-dislocation interactions in Al-Mg alloys at elevated temperatures

D. Stone, H. Wilson, R.-C. Kuo, Che-Yu Li

To cite this version:

D. Stone, H. Wilson, R.-C. Kuo, Che-Yu Li. Solute-dislocation interactions in Al-Mg alloys at elevated temperatures. Revue de Physique Appliquée, Société française de physique / EDP, 1988, 23 (4), pp.714-714. �10.1051/rphysap:01988002304071400�. �jpa-00245869�

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714

SOLUTE-DISLOCATION INTERACTIONS IN Al-Mg ALLOYS AT ELEVATED TEMPERATURES D. Stone, H. Wilson, R.-C. Kuo, and Che-Yu Li

Department of Materials Science and Engineering,

Cornell University, Ithaca, New York 14853

Revue Phys. Appl. 23

(1988)

714 AVRIL 1988,

Current theories for the creep of solid solu- tion alloys are concerned with three regimes of creep behavior, depending upon the level of stress, including conditions of alloy class creep behavior [1]. At low stresses the stress expon- ent, n, of the steady state-like (SSL) strain rate

has a value of about 4-5, similar to that of a pure metal. Within a range of intermediate stresses n = 3. At high stresses n increases.

Like the creep test, load relaxation and ten- sile tests can be used to examine the effects of solute-dislocation interactions. These interac- tions are manifested by the presence of a yield drop and serrated flow in a tensile test and a de- viation away from pure metal-like behavior in a load relaxation test [2]. In the present work a comparison has been made between results of the three types of tests performed on Al-Mg alloys at 350°C and 360°C. A load relaxation study of high purity aluminum at 360°C was also performed. The

results of this work lead to new insights on the

creep of solid solution alloys at elevated temper- atures.

Constant displacement rate tensile test data of

an Al-4.6% Mg alloy are shown in Figure 1 in the form of true stress-true strain curves. The data demonstrate the presence of yield drops and ser-

rated flow. The possibility that the serrated flow might be caused by jerky motion of the cross-

head, especially at low strain rates, has been ruled out.

Load relaxation data, constant displacement

rate tensile data and creep data are compared in Figure 2 in the form of log stress-log strain rate

curves. The tensile test data are taken from

Figure 1 at a strain level of 1%. The load relax- ation data correspond to an initial strain level of 6%. The SSL creep data are from a 5.5% Mg alloy tested by Pahutova and Cadek at 350°C and have been shifted slightly to take into account the 10°C difference in temperature [3]. The three types of data show excellent agreement in terms of the stress dependence of the strain rate.

The different power law regimes of the creep data are labelled in Figure 2. We find that the

serrations during the tensile tests peak at strain

rates for which the power law exponent for creep is 3. This result is consistent with the solute- dislocation interactions having their strongest effects in this regime [1]. At high strain rates

the serrations disappear, as would also be ex-

pected. At low strain rates, the amplitude of the

serrations decreases slightly, but compared to the

average stress, the amplitude of the serrations remains large at the low strain rates implying

that the effects of the solute-dislocation inter- actions persist at low strain rates.

At low strain rates the load relaxation data of the Al-4.6% Mg alloy, viewed in form of Figure 2,

are concave up. Load relaxation data of the pure aluminum, however, are concave down. Although having an average stress exponent near 5, the pure aluminum data demonstrate a power law exponent of about 3 at the lowest strain rates. The concave

up instead of concave down behavior of the Al-4.6%

Mg load relaxation data represents a deviation from the pure metal-like behavior at lower strain rates. In general, additional information to the

stress exponent is necessary to delineate the mechanisms involved.

In summary, serrations occur in constant dis-

placement rate tensile tests of a 4.6% Mg alloy in

the regime where the solute dislocation interac- tion is supposed to peak according to current con- cepts of creep in alloys. These serrations die out at high strain rates as would be expected based on the same concept. The serrations appear

to persist to low strain rates, in contrast to the pure metal-like behavior observed for creep. Both the tensile and load relaxation data demonstrate effects of the solute-dislocation interactions at low strain rates.

Acknowledgment

This work was supported by the Materials Science Division of the Department of Energy.

References

1. F.A. Mohamed and T.G. Langdon, Acta Metall.,

22, June (1984), p. 779.

2. S.-P. Hannula, R.-C. Kuo, D.W. Henderson, and C.-Y. Li, in Solute-Defect Interaction, Theory and Experiment, S. Saimoto, G.R. Purdy, and

G.V. Kidson, Pergamon Press, Toronto (1986),

p. 366.

3. M. Pahutova and J. Cadek, Phys. Stat. Sol. A, 56 (1979).

Figure 1

Figure 2

Article published online by EDP Sciences and available at http://dx.doi.org/10.1051/rphysap:01988002304071400

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