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SUPPORTING INFORMATION

Impact of the binder nature on the morphological change of sulfur electrodes upon cycling investigated by in-situ characterization methods

Quentin Lemariéa,b, Hassane Idrissib, Eric Maireb, Pierre-Xavier Thivelc, Fannie Alloinc, Lionel Rouéa,*

a INRS- Énergie, Matériaux, Télécommunications, Varennes, Québec, J3X 1S2, Canada

b Université de Lyon, INSA-Lyon, MATEIS, CNRS UMR5510, F-69621 Villeurbanne, France

c Univ. Grenoble Alpes, Univ. Savoie Mont Blanc, CNRS, Grenoble INP, LEPMI, 38000

Grenoble, France

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Figure S1. Schematics of (a) the dilatometry setup, (b) the acoustic emission setup and (c) the XRCT electrochemical cell

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Figure S2. Voltage profiles at C/50, C/20, C/10, C/5 and 1C of (a) PVdF, (b) CMC and (c) PDDA electrodes.

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0 100 200 300 400 500 600 700 1,6

1,8 2,0 2,2 2,4

Potential (V vs Li/Li+ )

Discharge capacity (mAh g-1) CMC PDDA

Figure S3. Voltage profiles of CMC and PDDA electrodes during their 1st discharge at C/20 in synchrotron XRCT cell. The potential jumps correspond to the XRCT acquisition steps during which the cell was let in open circuit. These OCP periods are here deleted for clarity.

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