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Performance evaluation of thermoplastic polyolefin (TPO) roof membranes weathering on full-scale test roofs in four different climatic areas of North America

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Performance evaluation of thermoplastic polyolefin (TPO) roof

membranes weathering on full-scale test roofs in four different climatic areas of North America

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http://www.nrc-cnrc.gc.ca/irc

Pe rform a nc e e va lua t ion of t he rm opla st ic polyole fin (T PO) roof m e m bra ne s w e a t he ring on full-sc a le t e st roofs in four diffe re nt c lim a t ic a re a s of N ort h Am e ric a

I R C - O R A L - 9 9 1

C a r l s o n , J . D . ; E l l i o t , S . ; D e l g a d o , A . H . ; P a r o l i , R . M . u t h o r

O c t o b e r 2 0 0 9

A version of this document is published in / Une version de ce document se trouve dans:

Waterproof Membranes 2009 Conference, Dusseldorf, Germany, October 19-21, 2009, pp. 2,

The material in this document is covered by the provisions of the Copyright Act, by Canadian laws, policies, regulations and international agreements. Such provisions serve to identify the information source and, in specific instances, to prohibit reproduction of materials without written permission. For more information visit http://laws.justice.gc.ca/en/showtdm/cs/C-42

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WESTERN STATES ROOFING CONTRACTORS

ASSOCIATION (WSRCA)

Project with field work by WSRCA and laboratory work by

NATIONAL RESEARCH COUNCIL OF CANADA (NRC)

TPO ROOF MEMBRANE

IN-SITU TESTING &

RESEARCH PROGRAM

Analysis of First Five-Years of

Field Observations and Laboratory Test Findings, but first a bit of background info….

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Built-up Roof BUR SBS Styrene-Butadiene-Styrene (Elastomer) APP Atactic Polypropylene (Plastomer) Modified Bitumen (Mod. Bit.) Asphalt-based CR (Polychloroprene) EPDM (Ethylene-Propylene-Diene Monomer or Ethylene-Propylene-Diene Terpolymer) Thermosets (TS) CSPE (chlorosulphonated Polyethelene) CPE (Chlorinated Polyethylene) TPO (Thermoplastic Polyolefin or Flexible Polyolefin) KEE

(Ketone Ethylene Ester)

PVC

Poly(Vinyl Chloride)

Theromplastics (TP) Polymer-based

Low Slope Roof Membranes

Genre of Low-Slope Roof Membranes Used In the Western United States

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How Do TPO Roof Membranes Stack Up?

General U.S. Experience:

Mostly Successes to Date

History has shown that almost no membrane roof system has been immune to issues or some sort of problem:

- BUR (blistering of organic felts, slippage, etc.) - Mod Bit (earlier APP cracking and weathering) - PVC (aged, unreinforced membrane shrinkage,

cracking, shattering)

- EPDM (shrinkage and bridging)

- Etc. (including TPO has been no different than others)

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Earlier Generation TPO Roof Membrane

Issues Included:

Some Problems with 1st Generation Sheets: - Welding issues and seam problems

- Complications with fire retardants and UV stabilizers

Other Issues Have Developed with Early Generation Sheets:

- Surface crazing and top coating cracking, particularly with darker-colored sheets

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Example of surface crazing and cracking

with earlier generation sheets

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Microscopic view of

initial crazing

Crazing more

pronounced over scrim

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Early TPO Issues, Such as

1st Generation Membrane Cracking What do we tell our clients, and

what do we do about it?

With most membranes, problematic seams can be treated as a repair and maintenance

measure

Sheet seams can be stripped in to repair cracking along seams. If membrane warranty expired, and field of

membrane in serviceable condition – candidate for repair and maintenance or service contract.

1stGeneration Membrane Cracking along

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WSRCA’s Low-Slope Technical & Research Committee Chose Proactive Research with Full-Scale Testing:

WSRCA TPO WEATHERING FARM

Inception January, 2000

Participating Manufacturers (in alphabetical order)

Carlisle

Firestone

Genflex (Now owned by Firestone)

Stevens Roofing Systems (Now Dow)

Participating Roofing Contractors (listed in chronological order that roofs were installed)

Snyder Roofing, Snohomish, Washington

Industrial Roofing, Anchorage, Alaska

Commercial Roofers, Las Vegas, Nevada

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Program Purpose

To examine weathering characteristics of

Thermoplastic Polyolefin (TPO) roof membranes by exposing them to various weather conditions of four distinctly different climatic regions in the Western United States.

Program Goal

To provide pertinent technical and performance information to the Western States Roofing

Contractors Association membership, and the U.S. roofing industry at large, regarding TPO roof

membranes’ attributes, their performance properties and resistance to degradation due to the effects of weathering.

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The TPO roof membranes are applied in-situ on full-scale test roofs located in the following climatic areas:

Hot and Dry

Hot and Humid

Cold and Dry

Moderate and Wet

Anchorage, Alaska San Antonio, Texas

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Anchorage, Alaska TPO installation

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WSRCA’s Low-slope Committee and the Manufacturer Participants Agreed to Yearly Field Inspections, Examining Numerous Items, Including:

Seam Integrity

Physical Condition of Surface

Coefficient of Expansion

(Visible changes in tightness vs. looseness)

General surface hue and appearance differing from the time of installation

WSRCA’s Low-slope Committee and the Manufacturer Participants Agreed to Testing of Samples According to Standard Test Methods

Membrane Total Mil Thickness from random field locations

Coating Thickness over scrim

Dimensional Stability

Water Absorption

Tensile Strength

Low Temperature Properties, and added

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4,860 Sq.Ft. 4,600 Sq.Ft. Area 1 Area 2 4,700 Sq.Ft. 4,860 Sq.Ft. Area 3 Area 4 Area Dividers

Commercial Facility, Near Seattle, Washington

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1,200 Sq.Ft. 1,200 Sq.Ft. 1,200 Sq.Ft. 1,200 Sq.Ft. Area 4 Area 3 Area 2 Area 1

Medical Building, Anchorage, Alaska

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Commercial Facility, Las Vegas, Nevada

3,600 Sq.Ft. 3,330 Sq.Ft. 3,510 Sq.Ft. 3,870 Sq.Ft.

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Shopping Center, San Antonio, Texas

2,176 Sq.Ft. 2,135 Sq.Ft. 2,178 Sq.Ft. 2,192 Sq.Ft.

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Seattle, WA

Year 3 – Year 5 Comparison

Observed Changes - 1. Dimensional Stability

Membrane tightening observed, but it still continues to change a bit with temperature and sun conditions as is characteristic with

TPO compounds.

Seattle Area 1, Year 3

Note: Wrinkles Across Sheets (cross-machine direction)

Seattle Area 1, Year 5

Note: Membrane Tighter During Site Visit Two Years Later

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Seattle Area 2, Year 3

Note: Wrinkles Along Length of Sheets (in machine direction)

Seattle Area 2, Year 5

Note: Membrane Tighter Two Years Later -- Though Creases

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Seattle Area 3, Year 3

Note: Numerous Wrinkles in Various Directions

Seattle Area 3, Year 5

Though Some Wrinkles Remain, Membrane More

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Seattle Area 4, Year 3

Note: Some Wrinkles with Length of Sheet

Seattle Area 4, Year 5

Membrane Taut, Though Crease Remains Along Seam

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Observed Performance Changes

2. Some Slight Bridging at Angle Change

Las Vegas Site – 3 Years

Some bridging at angle changes

Example of more pronounced bridging

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Seattle, WA

Roof Area 1 Roof Area 2

Roof Area 1 Las Vegas, NV Roof Area 2 Surface Characteristics, Color/Hue

Observed Changes

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Requirement for Energy Star Label

Initial Solar Reflectance

Greater than or equal to 0.65

Maintenance of Solar Reflectance

Greater than or equal to 0.50 three years after initial installation under normal weathering conditions

Solar Reflectivity Testing

Solar Reflectometer – Thanks Firestone!

Seattle, Reflectivity Testing

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Reflectivity Testing at Cleaned Area

--Decided to compare two different methods

Pressure Wash to Clean Surface

Rinse, Scrub, Rinse, and Squeegee

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AGE OF

ROOF 1 2 3 4 1 2 3 4 1 2 3 4 1 2 3 4 AVERAGE

New - - -

-Average: 0.826 Average: 0.826 Average: 0.826 Average: 0.826 0.826 7-Month - - - 0.670 0.657 0.676 0.668

Average: - Average: - Average: - Average:* 0.668 0.668 3-4 Year 0.720 0.595 0.603 0.626 0.693 0.721 0.654 0.701 0.000 0.000 0.000 0.000 0.683 0.605 0.618 0.656

Average: 0.636 Average: 0.692 Average: 0.000 Average: 0.641 0.656 Elapsed Change: - 0.190 Elapsed Change: - 0.125 Elapsed Change: - - Elapsed Change: - 0.186 0.170

* Unofficial test results taken only at Seattle TPO Test Roof

AGE OF

ROOF 1 2 3 4 1 2 3 4 1 2 3 4 1 2 3 4 AVERAGE

New - - -

-Average: 0.826 Average: 0.826 Average: 0.826 Average: 0.826 0.826 3-4 Year 0.774 0.680 0.681 0.723 0.746 0.761 0.742 0.783 0.000 0.000 0.000 0.000 0.713 0.628 0.669 0.732

Average: 0.715 Average: 0.758 Average: 0.000 Average: 0.686 0.719 Elapsed Change: - 0.112 Elapsed Change: - 0.068 Elapsed Change: - Elapsed Change: - 0.141 0.107

ROOF AREA ROOF AREA ROOF AREA ROOF REA

CLEANED ROOF AREA TEST COMPARISONS FROM REGIONAL LOCATIONS

Anchorage, Alaska Las Vegas, Nevada San Antonio, Texas Seattle, Washington

WSRCA TPO WEATHERING FARM

Anchorage, Alaska

TEST COMPARISONS FROM REGIONAL LOCATIONS

Las Vegas, Nevada San Antonio, Texas Seattle, Washington

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Seattle Fifth Year Inspection and Data Collection

Mechanical Properties Mechanical Properties

• Thickness, Sheet Overall

• Thickness of Coating Over Scrim • Linear Dimensional Change

• Water Absorption • Tensile Properties Chemical Properties Chemical Properties

• Dynamic mechanical analysis (DMA) • Thermogravimetry (TG/DTG)

• Fourier transform infrared spectroscopy (FTIR)

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0.000 0.500 1.000 1.500 2.000

SEA1 SEA2 SEA3 SEA4

T h ick n ess ( m m ) 0 0.02 0.04 0.06 0.08 T h ickn ess ( in .) Seattle Seattle Unex p o sed E x p o sed 1-yr E x p o sed 3-yrs E x p o sed 5-yrs 60 mils requested ASTM spec.=1.0mm (0.039in)

60 mils requested ASTM spec.=1.0mm (0.039in)

0.000 0.500 1.000 1.500 2.000

TEX1 TEX2 TEX3 TEX4

T h ic kn ess ( m m ) 0 0.02 0.04 0.06 0.08 T h ickn ess ( in .) Texas Texas Unex p o sed E x p o sed 1-yr E x p o sed 3-yrs 0.000 0.500 1.000 1.500 2.000 LV1 LV2 LV3 LV4 T h ick n ess ( m m ) 0 0.02 0.04 0.06 0.08 Thi c k ne s s ( in. ) Las Vegas Las Vegas Unex p o sed E x p o sed 1-yr E x p o sed 3-yrs

ASTM spec.=1.0mm (0.039in) ASTM spec.=1.0mm (0.039in)

0.000 0.500 1.000 1.500 2.000

AK1 AK2 Ak3 AK4

T h ic k n es s ( m m ) 0 0.02 0.04 0.06 0.08 Thi c k ne s s ( in. ) Alaska Alaska Unex p o sed E x p o sed 1-yr E x p o sed 3-yrs E x p o sed 5-yrs Overall Thickness

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Seattle Seattle 0 0.2 0.4 0.6 0.8

SEA1 SEA2 SEA3 SEA4

T h ickn e ss (m m ) 0 0.01 0.02 0.03 T h ickn ess ( in .) Unex p o sed E x p o sed 1-yr E x p o sed 3-yrs E x p o sed 5-yrs 0 0.2 0.4 0.6 0.8

AK1 AK2 Ak3 AK4

Thi c k n e s s ( m m ) 0 0.01 0.02 0.03 Thi c k ne s s ( in. ) Alaska Alaska

ASTM spec.=0.305 mm (0.012in)

0 0.2 0.4 0.6 0.8

TEX1 TEX2 TEX3 TEX4

T h ickn e ss (m m ) 0 0.01 0.02 0.03 T h ickn ess ( in .) Texas Texas Unex p o sed E x p o sed 1-yr E x p o sed 3-yrs 0 0.2 0.4 0.6 0.8 LV1 LV2 LV3 LV4 T h ickn e ss (m m ) 0 0.01 0.02 0.03 T h ickn ess ( in .) Las Vegas Las Vegas Unex p o sed Exposed 1y r Exposed 3y rs

ASTM spec.=0.305 mm (0.012in)

ASTM spec.=0.305 mm (0.012in) ASTM spec.=0.305 mm (0.012in)

Unex p o sed Exposed 1y r Exposed 3y rs Exposed 5y rs

Over Scrim

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Thank you!

• Project progressing well.

Membrane’s seventh year

weathering data will be reviewed

2010.

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