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Scanning Electron Microscopy mapping of VHF Surface Acoustic Wave devices

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Mapping acoustic field distributions of VHF to SHF SAW transducers using a Scanning Electron Microscope

A. Godet, J.M. Friedt, S. Demb´el´e, N. Piat, A. Khelif, P. Vairac, J. Agnus, P.Y. Bourgeois, G. Goavec-M´erou

jmfriedt@femto-st.fr,http://jmfriedt.free.fr FEMTO-ST Institute UMR 6174, Besan¸con, France

Scanning Electron Microscopy mapping of VHF Surface Acoustic Wave devices

• Scanning Electron Microscopy (SEM): recording backscattered & secondary electrons of the target illuminated by electrons (charged particle path bent by electric field associated with acoustic wave propagating on piezoelectric substrate)

• Low incoming electron energy (≤1 keV) to reduce charging on insulating piezo- electric substrates

• In-linesecondary electron detector most sensitive to the deflection induced by the acoustic field associated electric field

• SEM detectorbandwidth (2 MHz) insufficientfor time resolved SAW device acoustic field mapping (100-3000 MHz) [1]→

• ⇒ standing wave pattern (resonator) or interference between electromagnetic and acoustic related fields [2]

• Compatible with shear wave and sub-micrometer resolution acoustic field mapping

• Fastmeasurement (1 s) butqualitativemapping (not quantitative as optical interferometric methods)

0 2 4 6 8 10 12 14

-55 -50 -45 -40 -35 -30

frequency (MHz)

power spectrum (dBm)

SE2 photodetector bandwidth measurement

Rayleigh wave (LNO) and STW wave (quartz) acoustic field mapping

• Demonstration on SHF Rayleigh wave delay line (lithium niobate) and VHF STW wave (quartz).

• Optical interferometric analysis of STW device shows <10 pm out-of-plane displacement over IDTs ⇒SEM sees shear waves→

• Rayleigh wave on LNO at 2.4 GHz : 1.5 µm wavelength, hardly ac- cessible with optics

• Well resolved collimated beam despite propagating wave −→

• Failure to observe electric field associated with Love mode propagation due to the 1.5 µm thick insulating (SiO2) guiding layer.

• Advantages over optical measurements: fast (<1 s acquisition), com- patible with shear wave, high spatial resolution

• Drawbacks over optical measurements: qualitative mapping, not quantitative

• BUT ability to interact with the sample through Focused Ion Beam (FIB) milling of the piezoelectric substrate↓

acoustic wave

interdigitated transducer

mirror

acoustic

wave quartz

PCB electrodes

Top: 2.45 GHz Rayleigh wave. Bot.: 126 MHz STW wave

Interfering with wave propagation: FIB milled obstacles

acoustic wave

• Acoustic wave penetration of the order of the wavelength.

• High frequency operation to be compatible with FIB-milled structures,

• reflected Rayleigh wave propagationin directions in which no cou- pling might be expected

• Point source from slit between trenches.

• Etch rate in ST-cut quartz: 0.14±0.03µm3/nC (consistent with LNO)

acoustic wave

trench

slit

path acoustic

acoustic

wave trenches

IDT

Left: with acoustic field. Right: no acoustic field.

Top: point source from slit experiment. Bottom: half coral.

Conclusion & perspectives: stroboscopy

acoustic wave

• Possibility to implement stroboscopic[3] measure- ment if incoming electron beam is focused away from sample unless a reproducible wave pattern is met.

• Interaction mechanism of electrons with surface elec- tric fields remains to be understood forquantitative analysis.

Bibliography:

[1] G. Eberharter & al., Applied Physics Letters,37, p. 698, 1980.

[2] D. V. Roshchupkin, & al., Applied Physics Letters,60, p. 2330, 1992.

[3] H. P. Feuerbaum, & al., J. Phys. E:

Sci. Instrum.,11, p. 529, 1978.

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