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Basis of near-infrared spectroscopy

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Academic year: 2022

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Advantages Inconvenient - Nondestructive

- Quick measurement

- Reduces environmental pollution - Fewer errors due to low sample treatment

- Allows analysis anywhere - Low maintenance cost

- High initial investment - Needs calibration

Introduction

 1800: Frederick William Herschel discovered near infrared.

 Initial rejection of near-infrared spectroscopy.

 Finals 1960: Karl Norris initiates the measurement of diffuse reflectance.

Basis of near-infrared spectroscopy

 Electromagnetic radiation :

 Infrared: NIR (750-2500nm) / MIR (2500- 25000nm)/ Far (25000- 100000nm)

 Molecular vibrations: C – H, N – H, C – O, O – H (links functional groups)

 Measurement of radiation absorbed:

- Reflection: specular reflection and diffuse reflection - Transmittance

Absorption Spectra: View the absorption of the links.

Structure and operation of the devices NIRS Types of measures

Calibration

 The NIRS device requires a pre calibrated using conventional methods

.

Application of NIRS in food quality

 Quality of food: a set of measurable parameters, which provide a level of satisfaction of consumer needs.

 The NIRS to measure various chemical parameters that define the quality of a food.

 Measuring qualitative and quantitative moisture, proteins, lipids, carbohydrates ...

Examples:

- Fraud Detection: Adulteration of meat - Maturation

Advantages and inconvenient Conclusions

 The introduction of NIRS in food industry led to a breakthrough between the methods.

 The investigation of a continuous calibration that can be used in various analytes and food shows how this method is of great interest to industry.

Références

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