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Strain localization and fracture of cylindrical ice specimens under confining pressure

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STRAIN LOCALIZATION AND FRACTURE OF CYLINDRICAL

ICE SPECIMENS UNDER CONFINING PRESSURE

Chuanke Li 1, Ian Jordaan 1 and Paul Barrette 1

1

Memorial University of Newfoundland, St. John’s, Canada

ABSTRACT

A group of laboratory tests were conducted at Memorial University of Newfoundland with cylindrical ice specimens. The specimens were made with both laboratory ice and iceberg ice. In each test, the cylindrical specimen was triaxially confined at different pressure levels and an external constant deviatoric stress was exerted in the longitudinal direction. During the tests, some specimens showed a band of strain location in some cases leading to shear fracture. All those specimen showing strain localization or shear fracture made of laboratory ice were confined at relative low pressure levels (≤ 10 MPa) or high pressure levels ( ≥ 50 MPa). There was no strain localization or shear fracture observed at medium confinement levels. Strain localization or shear fracture observed in specimens made of iceberg ice was less pressure-dependent but initial flaws were observed in each specimen before the tests. Analysis shows that nonhomogeneity in the specimen is the likely cause of the localization. This has been confirmed by finite element simulations.

INTRODUCTION

It is well accepted that the load acting on structures during an ice impact event is transmitted through localized, short-lived zones of intense high pressure along the contact surface. Ice near the contact interface is highly confined and compressed with large deformations. Peak pressures reaching as high as 70 MPa were reported during the medium scale indentation tests on Hobson’s Choice Ice Island (Frederking et al. 1990).

In order to understand the mechanical behaviour of ice under confinement with large deformation, a group of triaxial tests was conducted with cylindrical specimens at

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Memorial University of Newfoundland. Both laboratory ice and iceberg ice were used to prepare the specimens. In the tests, the cylindrical specimens were confined at different pressure levels. A constant external load equivalent to 15 MPa of deviatoric stress was exerted in the axial direction of the specimen in each test. Mainly two types of behaviour were observed from the tests. One is that the specimen showed axial shortening and lateral expansion uniformly along the length of the specimen. Another is that the deformed specimen showed a band of shear strain localization in the direction of maximum shear which led some specimens to a complete fracture. Fine-grained materials were commonly observed within the band of the strain localization or within a certain distance along the faulted plane for the fractured specimens. In this paper, the main effort is made to study the mechanisms of shear fracture and its precursor strain localization. Studies on other engineering or geotechnical materials are briefly reviewed and a mathematical derivation for conditions of triggering the shear fracture of ice is given. Finite element analysis using a viscoelastic material and the continuum damage mechanics is conducted to assist the investigation.

TEST SETUP

The tests were conducted using laboratory prepared granular ice and a few specimens retrieved from the field. A cylindrical geometry was used for all specimens. The cylinders were 155 mm high and 70 mm in diameter. Samples were allowed to equilibrate for at least 12 hours at the temperature of interest prior to being tested. Testing was performed using a MTS test frame (Figure 1) fitted with a Structural Behaviour Engineering Laboratories Model 10 Triaxial Cell. The MTS system consisted of two servo-controlled hydraulic rams that applied axial load and confining pressure independently.

Figure 1 View of the triaxial cell with a specimen prepared for testing

A prepared sample was mounted on hardened steel end platens of the same diameter and the assembly was then enclosed in a latex jacket to keep the confining medium

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(silicone oil) from penetrating the ice. The specimen assembly was placed inside the triaxial cell and, in the tests at low strain levels, two linear variable differential transformers (LVDTs) were clamped to the sides of the jacketed specimen. In these tests, the LVDTs were used to monitor axial displacement and to control the advance rate of the ram. For tests at high strain levels, large sample distortions prevented the use of LVDTs. In these tests, the displacement of the ram was used to control the ram advance rate directly. The confining cell was closed and filled with silicone oil, and a small axial load was applied at ambient pressure to ensure contact between the specimen and piston. The confining pressure was then increased at 0.5 MPa per second to the target confinement, and then the specified axial deformation or creep load was applied to the sample after an interval of time. The parameters recorded during the tests included platen displacement, axial load, confining pressure and temperature. At the end of each test the axial load was quickly removed and the confining pressure was released gradually. The sample was removed from the cell immediately after testing and inspected for jacket leaks and large scale fractures.

TEST RESULTS

During the triaxial tests, mainly three types of deformed shapes of the ice specimens were observed. Schematic representations of the macroscopic shapes of typical deformed samples are shown in Figure 2. Samples that deformed without fracture showed axial shortening and lateral expansion which was relatively uniform along the length of the sample (Figure 2a). Samples that deformed with a band of shear strain localization with fine-grained materials within the band are illustrated in Figure 2b. Samples that were completely fractured after strain localization along the maximum shear direction are illustrated in Figure 2c.

The situation in Figure 2c is strongly related to the second case and strain location is the precursor the shear fracture. Thin sections taken after the test shown in Figure 3 provides solid evidence of this process. Figure 3a is the overall profile of an ice specimen after test showing strain localization and the trend to fracture in the direction of maximum shear. Fine-grained materials are observed within the band of stain localization, which make ice softener within the localized band than the surrounding areas (see Figure 3b). At a certain moment of the deformation history, the softening process within the band becomes instable and the specimen becomes completely fractured with failure oriented in the maximum shear direction (Figure 3c). In Figure 3c, fine-grained materials also exist in a certain distance from the faulted plane which indicates that the creation of the softening ice and strain localization occurred before the complete fracture. Meglis et al. (1999) suggested that the mechanisms of the formation of the fine-grained materials within the localization band are pressure-dependent. Microcracking and recrystallization are dominant at low confining levels (≤15 MPa). Recrystallization and pressure melting are responsible for the formation of fine-grained materials at high confinement levels (≥50 MPa).

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Figure 4 shows the pressure-temperature relationship of all the tests that have shown strain localization or its consequence – shear fracture. Both laboratory ice and iceberg ice specimens were studied. Occurrence of strain localization in specimens made in laboratory ice is pressure and temperature dependent. From Figure 4 it can be simply obtained that strain localization tends to occur at low (≤ 10 MPa) and high ( ≥ 50 MPa) confining pressures for laboratory ice and no evidence of strain localization was found at medium pressure levels among the tests with laboratory ice. Most of the events with strain localization in tests of laboratory ice occurred at relatively high temperature (higher than –10 °C) and only one test was found to have a failure at temperature equal to –21 °C and Pc = 10 MPa with a clearly observable initial flaw.

The tests with presence of strain localization with iceberg ice were relatively less dependent on the confining pressure and temperature. However, the tests did show that most of the events of strain localization using iceberg ice specimens occurred at low and high pressures except two failure events observed at confining pressure equal to 30 MPa. Initial flaws such as cracks, veins and brine pockets, etc., were clearly observed in all the iceberg ice specimens before the tests.

Figure 2 Schematic represents of macroscopic shape of deformed samples after tests. (a) most samples deformed relatively uniformly; (b) strain localization; (c) shear strain localization followed by shear fracture

In summary, for laboratory ice, the strain localization tends to occurr at low and high pressures and relatively high temperatures. This is in accordance with pressure-dependence of the microstructural changes in ice presented by Meglis et al. (1999). For iceberg ice specimens, occurrence of strain localization is relatively less dependent on confining pressure and temperature. The failure of iceberg ice specimens is suspected to be induced by the initial flaws. Analytical and numerical studies of mechanisms of strain localization are given in detail in the following sections.

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Figure 3 Photographs of samples show strain localization (a) profile for test IT 000501 showing localized bands at deviatoric stress = 15 MPa and confining pressure = 50 MPa (b) Thin section for IT 000501 showing fine grains concentrated along the localized bands (c) Thin section of a fractured specimen (IT000505) with fine grains along the faulted plane at deviatoric stress = 15 MPa and confining pressure = 65 MPa. -30 -25 -20 -15 -10 -5 0 0 20 40 60 80 Pressure (MPa) T e mp er at u re ( d e g C ) lab ice iceberg ice

Figure 4 Pressure against temperature for specimens showing strain localization or shear fracture.

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MECHANISMS OF STRAIN LOCALIZATION

Besides having been observed in ice, shear instabilities in the form of shear strain localization bands are commonly observed in metals and polymers subjected to large deformation. The formation of a shear band is often an immediate precursor to fracture of the materials as observed by Molinari and Clifton (1987) and Anand et al. (1987) for viscoplastic solids, and Armero (1999) for rate-dependent inelastic solids and Borja et al. (2000) for soft rock. The physical mechanisms responsible for triggering localization vary widely. For example, thermal softening plays a key role in initiating localization at high rates of loading in structural metals (Costin, 1979) and in viscoplastic materials (Molinari and Clifton, 1987). In brittle materials such as rocks, faulting appears to be caused by microcrack nucleation, growth and coalescence under uniaxial compressive stress conditions (Needleman, 1988). Needleman (1988) used incremental constitutive equations to discuss the formation of localization for both rate-independent materials and rate-dependent materials. For rate-independent elastic-plastic materials under homogenous conditions, the strain localization is induced by the strain softening. This is beyond the scope of this paper because ice is treated as a viscoelastic material under the testing conditions discussed above. Therefore, this paper focuses on the mechanisms of strain localization of rate-dependent materials. Needleman’s derivation is reviewed and applied to ice for this purpose.

Under compressive loading conditions, the total strain of ice under constant stress conditions can be expressed as:

(1) γ =γedc,

whereγeis the instantaneous elastic component; γdis the delayed elastic component and γcis the viscous component.

Thus, we get under homogenous conditions, the incremental constitutive equation can be written as

(2) )τ&=G(γ&−γ&v ,

where τ is shear stress; G is elastic shear modulus; γvis used to represent the viscous strain including the delayed elastic strain of ice.

Considering quasi-static loading conditions, assume that a bifurcation from a state of homogeneous shear into a deformation pattern with a shear band appears at some stage of the deformation history as sketched in Figure 5. Stress equilibrium requires

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(3) τ&b = , τ&o

where the subscripts b and o represent the region inside the band and outside the band, respectively, corresponding to Figure 5.

Figure 5 Simple shearing of a planar strip.

Then, under quasi-static loading conditions, at the moment of the deformation history when a bifurcation appears, equilibrium requires that the stress state remains homogenous as described in Eq.(3). Combining Eq.(2) and (3) gives

(4) 0G(γ&b −γ&0)= .

Since the elastic shear modulus, G, is positive, the unique solution to Eq.(4) is o

b γ

γ& = & . In fact, Eq.(4) excludes bifurcation. Needleman (1988) also used a minimum potential method to confirm this point. Accordingly, for rate-dependent materials, to get a nontrivial solution to Eq.(4), a band with some kind of nonhomogeneity such as material properties or stress levels different from those in the surrounding materials has to be introduced. Therefore, a solution can be constructed in which there is uniform straining inside the band and uniform straining outside the band with a jump in strain rate across the band. The crucial role of nonhomogeneity at quasi-static conditions for rate-dependent materials was studied by Anand et al. (1987), Molinari and Clifton (1987), Belytschko et al. (1991) and Bayliss et al. (1994).

It is worth noting that strain localization does not necessarily lead to immediate failure, even though a band with different material properties exists. The governing equation for strain localization instability is γ& /b γ&o →∞ (Hutchinson and Neale, 1977). By this criterion, a localization instability is associated with an increment of strain occurring in the band and no increase in strain outside the band. Under this condition, the strain localization will dominate the failure. Needleman (1991) used a linear Kelvin-Voigt model to study the localization instability in progressively softening solids by this governing equation. The term progressive softening is used to refer to circumstances where, at least for certain deformation histories, the constitutive relation permits the stress to decrease monotonically to zero after the attainment of a maximum stress. As summarized by Needleman (1991), localization dominates the Localization band b

o o

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failure when the material inside the band softens while material outside the band becomes relatively harder.

COMPUTER SIMULATIONS AND DISCUSSION

In this section, computer simulations aimed at exploring the effect of nonhomogeneities are presented. Ice is a progressive softening material which requires a framework that can characterize the actual softening process to model properly the progressive softening and study the localization problem. The constitutive model of the creep of ice under compressive loading conditions with large deformations applied in this paper can be expressed as

(5) ( ) exp( ) 0 S s s c n = ε& ,

where ε& is strain rate, c and n are constants, s0 is a reference stress; s is the von Mises

stress and S is the damage parameter. The damage parameter S of ice under triaxial loading conditions is highly pressure-dependent (Li et al. 2003). Under low confinement levels, microcracking and recrystallization are dominant. Under high confinement levels, recrystallization and possible pressure melting are the main mechanisms and microcracking is negligible. Therefore, the damage parameter is expressed as a function of confinement pressure and von Mises stress as shown below

(6) =

+ t q dt s s p f s s p f S 0 0 2 0 1( )( ) ( )exp( )] [ .

The first component on the right of Eq. (6) represents damage under low confinements and the second component represents damage under high confiments. The parameters in Eq. (6) were calibrated through the results of the triaxial tests and the calibrated results at a temperature of -10 ºC were detailed addressed in the work by Li et al. (2003). Based on Eq. (5) and (6), a UMAT subroutine was written to simulate the time-dependent material properties of ice in the finite element analysis software, ABAQUS, which was used to analyze cylindrical ice specimens deformed to high strain levels. A constant temperature of –10 °C was assumed in the analysis.

As discussed in the preceeding section, for rate-dependent material under homogenous conditions, strain localization is excluded. Therefore, a nonhomogeneity has to be introduced in order to trigger the strain localization. Two types of analyses are made in this research. The first was to introduce a material imperfection inside the specimen with a low elastic modulus as compared to the surrounding ice. The second was to model the friction effect at the both ends of the specimen. The friction can limit the

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lateral movement of the surfaces of the both ends of the specimen, which is believed to be able to cause nonhomogeneities.

For the analysis including a material imperfection, the local nonhomogeneity was placed at two different positions of the specimen to study its effect. The results of the finite element analysis are shown in Figure 6. This shows that the enhanced strains occur within a band triggered by the imperfection along with the direction of maximum shear approximately. It also shows that the strain localization band is sensitive to the position of the imperfection. For the case without imperfections but with friction at the both ends damage contour plots for the specimen under different pressures are showed in Figure 7. It demonstrates that damage at pressure = 15 MPa and 60 MPa grows very fast at the center of the specimen in comparison to the surrounding areas and forms a band oriented along maximum shear direction. This nonhomogeneity is caused by end effects which lead to the non-uniformity of the damage distribution. In Figure 7b damage at pressure of 35 MPa is small and almost uniform throughout the whole specimen because in this case the growth of damage is restricted.

The ice inside the band is damaged faster and more severely, which make the properties of ice change much quicker, than that in the surrounding areas, at pressure of 15 MPa and 60 MPa. At some stage of the damage evolution, this process will cause the ice inside the band to soften while the ice in the surrounding areas is still in a hardened state. Strain localization instability will occur along the band and cause the ice to fail. Recently, studies of ductile fracture were conducted by Bandstra and Koss (2001) by introducing two voids inside the materials; Orsini and Zikry (2001) did a similar analsysis with four voids. Both the studies showed strong tendency for strain localization between the voids which was attributed to the void growth and interaction. Both the constitutive model and the numerical model show that strain localization can be induced by nonhomogeneities of mechanical properties such as initial flaws or by the end effect. From the analyses for intact laboratory ice, it seems that the confining pressure plays a significant role in the initiation of the strain localization. It shows that when the temperature is equal to -10 °C, at the low pressure and high pressure levels strain localization occurs readily, but at the medium pressure level, strain localization is less prone to occur. This is in accordance with the observation from the experiments.

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Figure 6 (a) Deformed mesh for the imperfection near the center (b) Deformed mesh for the imperfection near the top end

Figure 7 (a)Damage contour plot for pressure = 15 MPa (b) Damage Contour plot for pressure = 35 MPa (c) Damage contour plot for pressure = 60 MPa

Other possible mechanisms of the strain localization and fracture should be considered. As proposed by Molinari and Clifton (1987) and Bayliss et al. (1994), for viscoplastic materials at high strain rate deformation, the thermal effect may be significant for the onset of strain localization (Jordaan, et al. 2005). This effect has been observed in ice because the temperature through the specimen is not uniform in the tests. The higher the temperature is, the softener is the ice and the nonhomogeneity is caused by the thermal effect. The current numerical model can only predict the possibility of the strain localization. For post-localization behaviour (onset of fracture and its growth), a special numerical technique has to be established to solve the strong discontinuity of the mechanical behaviour on the fracture plane and outside the fracture plane.

(a) (b)

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Concluding Remarks

Through the observation from triaxial tests with laboratory ice, shear fracture of ice specimens is prone to occur at low and high confinement pressure levels. Strain localization is the precursor of the shear fracture. For the tests with iceberg ice, initial flaws are responsible for the formation of shear fracture. For a rate-dependant material such as ice, strain localization instability is excluded under homogenous conditions. Non-homogenous conditions have to be introduced to trigger the strain localization instability. Computer simulations show that initial flaws in ice and friction at the two ends of a specimen are effective to trigger the bands of shear strain localization. Temperature effect is not studied in this research, but it is certainly an important factor during the process of shear fracture (see Figure 3). This remains an important subject for the future study. A constitutive model with continuum damage mechanics including the temperature effect for ice is being established by the present research group to study this topic.

Acknowledgement

Funding from National Sciences and Engineering Research Council of Canada (NSERC) is greatly appreciated.

References

Armero, F., 1999. Large-scale modeling of localized dissipative mechanism in a local continuum: applications to the numerical simulation of strain localization in rate-dependent inelastic solids. Mechanics of Cohesive-Frictional Materials. Vol. 4, pp. 101-131.

Anand, L., Kim, H. and Shawki, T.G., 1987. Onset of shear localization in viscoplastic solids. J. Mech. Phys. Solids. Vol. 35, No.4, pp. 407-429.

Bandstra, J.P. and Kross, D.A., 2001. Modeling the ductile fracture process of void coalescence by void-sheet formation. Materials Science and Engineering. A319-321, pp. 490-495.

Bayliss, A., Belytschko, T., Kulkarni, M. and Lott-Vrumpler, D.A., 1994. On the dynamics and the role of imperfection for localization in thermo-viscoplastic materials. Modelling Simul. Mater. Sci. Eng. Vol. 2, pp. 941-964.

Belytschko, T., Moran, B. and Kulkarni, M., 1991. On the crucial role of imperfections in quasi-static viscoplastic solutions. Transactions of the ASME, Vol. 58, pp. 658-665.

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Borja, R.I., Regueiro, R.A. and Lai, T.Y., 2000. FE modeling of strain localization in soft rock. Journal of Geotechnical and Geoenvironmental Engineering. Vol. 126, pp. 335-343.

Costin, L.S., Christman, E.E., Hawley, R.H. and Duffy, J., 1979. On the localization of plastic flow in mild stell tubes under dynamic torsional loading. J. Hardening, ed., Proceedings 2nd Conference on Mechanical properties at High Rates of Strain, Conference series No. 17 (Bristol and London), pp.90-100.

Frederking, R.M.W., Jordaan, I.J. and McCallum, J.S., 1990. Field tests of ice indentation at medium scale, Hobson’s Choice Ice Island. Proc. 10th International IAHR Symposium on Ice, Espoo, Finland, Vol. 2, pp.931-944.

Jordaan, I., Li, C., Barrette, P., Duval, P. and Meyssonnier, J., 2005. Mechanisms of ice softening under high pressure and shear. Submitted to POAC’05, Potsdam, New York.

Li, C., Jordaan, I.J., and Barrette, P., 2003. Damage and microstructural changes in ice in compression during interaction with structures. Advances in Fracture and Damage Mechanics. Proceedings of the 3rd International Conference on Fracture and Damage Mechanics, Ed F.-G Buchholz, Richard, H. A., and Aliabadi, M.H., pp. 431-436,. Meglis, I.L., Melanson, P.M., Jordaan, I.J., 1999. Microstructural change in ice: II. Creep behavior under triaxial stress conditions. Journal of Glaciology. Vol. 45, No. 151, pp. 438-448.

Molinari, A. and Clifton, R.J., 1987. Analysis characterization of shear localization in thermoviscoplastic materials. Transactions of the ASME, Vol. 54, pp.806-812.

Needleman, A., 1988. Material rate dependence and mesh sensitivity in localization problems. Computer Methods in Applied Mechanics and Engineering. Vol. 67, pp. 69-85.

Needleman, A., 1991. On the competition between failure and instability in progressively softening solids. Transactions of the ASME. Vol. 58, pp. 294-298.

Hutchinson, J.W. and Neale, K.W., 1977, Influence of strain rate sensitivity on necking under uniaxial tension. Acta Metall., Vol. 25, pp. 839-846.

Orsini, V.C. and Zikry, M.A., 2001. Void growth and interaction in crystalline materials. International Journal of Plasticity. Vol. 17, pp. 1393-1417.

Figure

Figure 1 View of the triaxial cell with a specimen prepared for testing
Figure 4 shows the pressure-temperature relationship of all the tests that have shown  strain localization or its consequence – shear fracture
Figure 4 Pressure against temperature for specimens showing strain localization or  shear fracture
Figure 5 Simple shearing of a planar strip.
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