Synthèse d'engrenages moléculaires
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After cooling down to room temperature, the mixture was diluted with DCM, filtered over celite and evaporated under reduced pressure.. The solution was
The reaction mixture was filtered through a short pad of celite and the solvent was concentrated under reduced pressure to give the crude product which was purified
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Experimentally, a continuous supersonic flow reactor was used to study this reaction over the 50-296 K temperature range employing pulsed laser photolysis and vacuum
After cooling to room temperature, the reaction mixture was diluted with EtOAc (50 mL), filtered through celite with copious washings, and then concentrated. The
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