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Compositional and morphological changes for ordered PtxFey/C oxygen electroreduction catalysts

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Academic year: 2021

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Figure 1a XRD patterns of Pt x Fe y /C series catalysts. Figure 1b Stick XRD  patterns of cubic Pt [Fm-3m], ordered cubic Pt 3 Fe [Pm-3m], ordered tetragonal  PtFe [P4/mmm] and cubic Fe [Fm-3m]
Figure 2 Representative HAADF-STEM images of general area for: (a) as- as-prepared Pt 3 Fe/C(800), (b) 10’000 E-cycled Pt 3 Fe/C(800), (c) as-prepared  Pt 3 Fe 2 /C(800), and (d) 10’000 E-cycled Pt 3 Fe 2 /C(800) catalysts.
Figure  5  Atomic  resolution  aberration-corrected  HAADF-STEM  images  of  selected  particles  from  as-prepared  Pt 3 Fe/C(800)  (a,b,c),  and  as-prepared  Pt 3 Fe 2 /C(800) (d,e)
Table 3. Activities (orr) for Pt series catalysts before and after 3000 E-cycles
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