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DIC process for treatment of organic materials

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HAL Id: hal-02754479

https://hal.inrae.fr/hal-02754479

Submitted on 3 Jun 2020

HAL is a multi-disciplinary open access archive for the deposit and dissemination of sci- entific research documents, whether they are pub- lished or not. The documents may come from teaching and research institutions in France or abroad, or from public or private research centers.

L’archive ouverte pluridisciplinaire HAL, est destinée au dépôt et à la diffusion de documents scientifiques de niveau recherche, publiés ou non, émanant des établissements d’enseignement et de recherche français ou étrangers, des laboratoires publics ou privés.

DIC process for treatment of organic materials

Magdalena Kristiawan, Vaclav Sobolik, Mazen Al Haddad, Karim Allaf

To cite this version:

Magdalena Kristiawan, Vaclav Sobolik, Mazen Al Haddad, Karim Allaf. DIC process for treatment

of organic materials. International Workshop on Process Intensification in Fluid and Particle Engi-

neering, Oct 2006, Kobe, Japan. Chemical Engineering of Japan, Journal of Chemical Engineering

of Japan, 40, pp.1021-1029, 2006, Isolation of Indonesian Cananga Oil by Instantaneous Controlled

Pressure Drop: Influence of Processing Parameters on Compound Yields. �hal-02754479�

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Full text article was published in Journal of Chemical Engineering of Japan:

KRISTIAWAN M., SOBOLIK V., ALLAF K.: Isolation of Indonesian Cananga Oil by Instantaneous Controlled Pressure Drop: Influence of Processing Parameters on Compound Yields. Journal of Chemical Engineering of Japan. 40(11), 1021-1029 (2007).

DIC process for treatment of organic materials

V. Sobolik, Magdalena Kristiawan, M. Al Haddad, K. Allaf

University of La Rochelle, Pole Sciences,

Laboratory Mastering of Agro-Industrial Technologies Avenue Michel Crépeau, 17042 La Rochelle, France

Abstract

A new process for material texturing, instantaneous controlled pressure drop (DIC), consists in heating wet materials in an autoclave, followed by a fast expansion (∆P/∆t > 2.10

5

Pa/s) into a pressure lower than the atmospheric one (5 kPa). The vapour, which evolves due to the rapid pressure drop, mechanically strains the material. This stress creates porous structures, breaks the cells and destroys micro-organisms. The temperature of the material before the expansion is usually higher than 100°C and the pressure in the autoclave corresponds to the saturated steam pressure. Manifold applications of this process are presented on the example of the extraction of essential oil from dried ylang-ylang flowers. The essential oil is separated from the condensate. The treated flowers are also analysed. The results are compared with the classical steam distillation.

Keywords: Ylang-ylang, extraction, essential oil, steam distillation, Instantaneous Controlled Pressure Drop

IWPI 2006 (http://www2.kobe-u.ac.jp/~iwpi/).

C5. Int. Workshop on Process Intensification in Fluid and Particle Engng., Kobe

University, Japan, Oct.15-18 2006, Abstract

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