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Triphenylphosphine‐functionalized core‐cross‐linked micelles and nanogels with a polycationic outer shell: synthesis and application in rhodium‐catalyzed biphasic hydrogenations

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Academic year: 2021

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Figure 1. Architecture and composition of the core-crosslinked micelles (CCM) and nanogel (NG) particles
Figure 2. Synthesis of the triphenylphosphine-functionalized CCM and NG particles with an outer P4VPMe + I - hydrophilic shell
Figure 4. 31 P NMR spectrum for the toluene-swollen CCM 10% latex, before (a) and after (b) equilibration with a [RhCl(COD)] 2 toluene solution at a P:Rh ratio of 1:1
Figure 5. 31 P NMR spectra recorded at different times after mixing equivalent amounts of CCM 20% latexes with 0 and 100% Rh loadings, and stirring at room temperature: (a) 1.5 h; (b) 7 h; (c) 1 week
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