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In situ powder x-ray diffraction, synthesis, and magnetic properties of the defect zircon structure ScVO4−x

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Academic year: 2021

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Figure 1. In situ powder X-ray diffraction contour plot of ScVO 3
Table 1. Structural Parameters, Bond Angles, and Average Bond Distances for ScVO 4 - x Zircon Defect Phase (space group: I4 1 /amd) As Obtained from Rietveld Refinements against Two Neutron and One X-ray Diffraction Pattern Measured at Room Temperature a
Figure 8 shows the TGA/DTA traces during the reduc- reduc-tion of ScVO 4 to ScVO 3 in CO/Ar with a single broad exotherm and a single step mass loss
Figure 7. In situ powder X-ray diffraction contour plot of ScVO 4

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