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Characterization of 13 and 30 μm thick hydrogenated amorphous silicon diodes deposited over CMOS integrated circuits for particle detection application

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Characterization of 13 and 30 mm thick hydrogenated amorphous silicon diodes deposited over CMOS integrated

circuits for particle detection application

M. Despeisse

a,

*, G. Anelli

a

, S. Commichau

b

, G. Dissertori

b

, A. Garrigos

a

, P. Jarron

a

, C. Miazza

c

, D. Moraes

a

, A. Shah

c

, N. Wyrsch

c

, G. Viertel

b

aCERN, CH-1211 Geneva, Switzerland

bInstitute for Particle Physics, ETH, CH-8093 Zurich, Switzerland

cInstitute of Microtechnology, University of Neuchatel, CH-2000 Neuch# atel, Switzerland#

Abstract

We present the experimental results obtained with a novel monolithic silicon pixel detector which consists in depositing a n–i–p hydrogenated amorphous silicon (a-Si:H) diode straight above the readout ASIC (this technology is called Thin Film on ASIC, TFA). The characterization has been performed on 13 and 30mm thick a-Si:H films deposited on top of an ASIC containing a linear array of high-speed low-noise transimpedance amplifiers designed in a 0.25mm CMOS technology. Experimental results presented have been obtained with a 600 nm pulsed laser. The results of charge collection efficiency and charge collection speed of these structures are discussed.

1. Introduction

A radiation sensor for charged particles based on the deposition of hydrogenated amorphous silicon (a-Si:H) n–i–p films on ASIC [1,2] has been recently proposed. The charge collection of the a- Si:H films has been studied with an ASIC contain- ing 32 channels of Active Feedback Preamplifiers (AFP) designed in a 0.25mm CMOS technology [3]

(Fig. 1).

The AFP is a transimpedance amplifier which uses a PMOS transistor as feedback element, making the circuit fast and low-noise, two characteristics which are crucial to measure a-

Si:H films charge collections. The feedback current controls the noise, the gain and the speed of the amplifier. A 13mm thick and a 30mm thick n–i–p a-Si:H diodes have been deposited on two ASIC samples.

2. Leakage current

A negative voltage is applied to the ITO electrode (Fig. 2) connected to the p-layer which reverse biases the n–i–p diode and depletes it. The intrinsic i-layer is in fact slightly n-doped, thus the depleted layer extends increasing the voltage from the p–i interface down to the i–n interface. The dark current of thick a-Si:H n–i–p structures has been measured at low bias voltage elsewhere [2],

*Corresponding author.

E-mail address:[email protected] (M. Despeisse).

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and values of 6 pA/cm2for an applied voltage of 1 V/mm have been obtained. Above 130 V for the 30mm thick a-Si:H sample and 50 V for the 13mm thick a-Si:H sample, the dark current increases very rapidly (Figs. 3 and 4). A previous work [4]

has shown that this effect at room temperature can be attributed to a leakage through the p-layer, by a mechanism of field-enhanced generation at the p/i interface.

Above the reverse bias voltages of 280 V for the 30mm sample and 80 V for the 13mm sample, large leakage currents prevent precise measure- ments and full depletion operation of the a-Si:H diode. Leakage currents of individual pixels have been measured by monitoring the leak- age current flowing in the electronic channel (Fig. 4).

The leakage current flows through the AFP in puts and induces variations of the feedback current that are readout at the output of the AFP amplifier as DC variations. This current varies up to 50 nA/pixel for 260 V of bias that is sufficiently small compared to the AFP feedback current of 1.2mA, and does not induce variations in the amplifier transfer function.

3. Charge collection

Charge collection of the 13 and 30mm structures have been characterized using a 660 nm pulsed

Fig. 1. Photography of a 30mm n–i–p a-Si:H film deposited on the 32-channels AFP amplifier integrated circuit, the size is 2 mm4 mm.

ASIC AFP

Channel Pixel 94 µm* 68 µm

n+layer p+layer

a-Si:H i-layer 13µm or 30 µm ITO 65nm

660nm laser Top electrode

Negative voltage Vbias

Non depleted region, no field

Depleted region with field

Wd

- +

Fig. 2. Schematic of the n.i.p layers deposited on top of the ASIC.

0 50 100 150 200 250 300

10-2 10-1 100 101 102 103 104

Total leakage current (nA)

Vbias (V)

0 50 100 150 200 250 300

10-2 10-1 100 101 102 103 104

Vbias (V)

Fig. 3. I–V characteristic of the entire 30mm chip.

0 50 100 150 200 250 300

0 10 20 30 40 50 60

Channel leakage current (nA)

Vbias (V)

Fig. 4. I–V characteristic per pixel (AFP channel).

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laser (2 ns pulse width) [1,2], having a 1mm mean free path in a-Si:H.

The peaks (Figs. 5 and 6) correspond to the electron drift in the depleted region. We observe the peaks showing a rising time of 6 ns for both samples, and a falling time of 16 ns (30mm sample) to 20 ns (13mm sample) are constant while varying the detector bias voltage (the electron collection time is independent of the detector bias such that the i-layer is not fully depleted). By considering a linear variation of the electric field with the depth of the i-layer depleted zone, we can extract the electrons collection time constanttcoll;n [1]

tcoll;n¼ ðe0eSiÞ=ðmeq NdÞ ð1Þ

tcoll;n varies from 10 to 1 ns for an electron mobility of 10 to 1 cm2/V s. After 3 tcoll;n;95% of the collection is achieved. This model can be applied to the non-dispersive electron transport occurring at room temperature in a-Si:H (standard transport model, by conduction in extended states).

When electron collection is achieved, a long decay tail (Fig. 7) represents the hole collection (holes mobility is about 0.01 cm2/V s in a-Si:H).

Increasing the bias, we observe an increase of the collection speed (1.6ms for 70 V to 1ms for 220 V).

Holes are created in the vicinity of the p/i interface and drift up to the top electrode, on a short length.

0 20 40 60 80

0 2 4 6 8 10 12 14 16

time (ns)

Pulse height (mV)

40V 70V 100V 130V 160V 190V 210V 240V 270V

5 10 15 20

0 5 10 15 20

Bias voltage (sqrt(V))

Signal amplitude (mV)

(a)

(b)

Fig. 6. (a) 30mm sample, AFP output pulses for different detector bias voltages. (b) The signal amplitude versus the square root of the detector bias is displayed in the corner.

0 20 40 60 80 100

0 1 2 3 4 5 6 7 8

time (ns)

Vout (mV)

29V 39V 49V 58V 66V

72V 80V

4 5 6 7 8 9

4 6 8 10 12 14 16

sqrt (Vbias)

Signal Amplitude (mV)

(a)

(b)

Fig. 5. (a) 13mm sample, AFP output pulses for different detector bias voltages. (b) The signal amplitude versus the square root of the detector bias is displayed in the corner.

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Increasing the bias voltage, one increases the electric field so the holes speed. The drift length is not changing for holes, resulting in a global decrease of the collection time.

Due to the high speed of the current transient, the AFP pre-amplifier is shaping the signal. A deconvolution of the signals for biases of 70, 160 and 220 V have been carried out using the HSPICE model of the pre-amplifier AFP. We used a sum of two exponentials for the current transientiðtÞof the photodiode layer.

A fast exponential (Fig. 8) corresponds to the electrons transport (considering the standard transport model, the collection time constant is t1). A slow exponential (Fig. 8) corresponds to an approximation of the holes transport, the collec- tion time constant ist2:Actually holes have a non- dispersive transport, and are subjected to trapping in deep states, making hole mobility a time dependent parameter. Though simplifying the complex electronic transport in a-Si:H, we per- formed good fits between simulated and observed signals (Fig. 9).

We extracted an electron collection time con- stant oft1¼4:5 ns (not varying with bias) for the 30mm sample, corresponding to a mNd of 1.45 cm1V1s1; and a t2¼4 ns (not varying with bias) for the 13mm sample, corresponding to a mNdof 1.64 cm1V1s1. The holes collection

time constant t2 is varying with bias, from 600 ns at 70 V to 300 ns at 220 V. The charge collection speed of the 30mm sample has been characterized (Fig. 10) for 3 different biases.

It shows a collection of 50% of the total charge in 15 ns (electrons collection in 3t1), and a long tail corresponding to the holes collection.

0 100 200 300 400 500 600 700 800 900

0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1

time (ns)

Pulse height (mV)

70V 160V

220V

Fig. 7. AFP output pulses long tail for the 30mm sample for 3 different biases.

-20 0 20 40 60 80 100

0 2 4 6 8 10 12 14

x 10-3

time (ns)

Pulse height (V)

Simulated signal Measured signal Vbias = 70V

Vbias = 160V Vbias = 220V

Fig. 8. Fits obtained between signals measured on 30mm sample and signals simulated using a sum of 2 exponential as diode current transient.

101 102

time (ns)

Current transient (A)

70V

160V 220V

Fig. 9. Extracted current transient for the 30mm sample.

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4. Conclusion

We have characterized the charge collection speed of 13 and 30mm thick a-Si:H diodes directly deposited on the ASIC containing the readout electronics. We have used a 660 nm pulsed laser.

Our measurements have shown that there are two components in the response of the detector: a fast one attributed to the electrons transport and a much slower one attributed to the holes transport.

For both the 13 and the 30mm thick detectors the

fast component varies from 16 to 20 ns, whereas the slow component varies from 0.9 to 1.5ms. The fast component does not depend on the bias voltage, the slow one decreases increasing the bias voltage. The high leakage current observed in- creasing the bias voltage prevents full depletion of the detectors: the expected bias voltage for a full depletion of 30mm of a-Si:H is 415 V, and the maximum voltage we can apply to the 30mm thick, a-Si:H film is 280 V.

References

[1] P. Jarron, G. Anelli, S. Commichau, M. Despeisse, G.

Dissertori, C. Miazza, A. Shah, N. Wyrsch, G. Viertel, New concept of monolithic silicon pixel detectors: hydrogenated amorphous silicon on ASIC, presented at the 9th Pisa Meeting on Advanced Detectors, La Biodola, Isola d’Elba, Italy, May 25–31, 2003.

[2] N. Wyrsch, C. Miazza, S. Dunand, A. Shah, N. Blanc, R.

Kaufmann, L. Cavalier, G. Anelli, M. Despeisse, P. Jarron, D. Moraes, A.G. Sirvent, G. Dissertori, G. Viertel, Development of vertically integrated imaging and particle sensors, Presented to the Mathematics Research Society, Spring Symposium 2003, San Francisco, MRS Proceedings, to be published.

[3] G. Anelli, K. Borer, L. Casagrande, M. Despeisse, P.

Jarron, N. Pelloux, S. Saramad, Nucl. Instr. and Meth. A 512 (2003) 117.

[4] J.B. Chevrier, B. Equer, J. Appl. Phys. 76 (11) (1994).

0 1 2 3 4

x 10-7 0

0.5 1 1.5 2

x 10-14

time (s)

charge collected (C)

15ns

Vb = 70V Vb = 160V Vb = 220V

Fig. 10. Charge collection for the 30mm sample for 3 different biases.

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