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Ultrasound assisted crystallization of a new cardioactive prototype using ionic liquid as solvent

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Table 1 summarizes all experimental conditions of crystallization by quick addition tests performed without (experiments 1, 3 and 5) and with ultrasound (experiments 2, 4 and 6)
Fig. 3. SEM images of recrystallized LASSBio-294 obtained by quick addition. (a) 159 mg·g −1 solution and 13.9 W/IL ratio (experiment 1); (b) 159 mg·g −1 solution and 14.9 W/IL ratio with US (experiment 2); (c) 159 mg·g −1 solution and 3.7 W/IL ratio (expe
Fig. 6. Particles size distribution (a) in volume and (b) in number of re- re-crystallized LASSBio-294 with different drug solution concentrations by  drop-wise addition.
Fig. 8. Particles size distribution and SEM images of recrystallized LASSBio-294 with low concentration (57 mg·g −1 solution) by dropwise addition of the  so-lution into reactor.
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