Synthèse de machines moléculaires pour le contrôle de mouvements de rotation et de translation
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(67) &,*' -,!'& G: %', -*-&! !* ,!'&& $ *!& . ,1 *# "-+ ',# "# * !&'+'# "#1 + !&',#1 +-*>!3* '0#1Q *Z>/3'.# "# #0',% . $-02#+#,2 . 02'!'.> 3 ">4#*-..#+#,2 "#1 +-2#301 +-*>!3* '0#1 3,'"'0#!2'-,,#*1 *'+#,2>1 . 0 3, 12'+3*31 *3+',#36T .0=1 *# ">4#*-..#+#,2 "# "#36 +-2#301 3,'"'0#!2'-,,#*1 "# .0#+'=0#wv #2 "#36'=+# %>,>0 2'-,wwQ #0',% #2 !-**T 0#,"#,2 !-+.2# #, wuvv "# * 17,2&=1# #2 "3 $-,!2'-,,#+#,2 "Z3, ,-34# 3 +-2#30 1> *3' 311' 130 *# $0 %+#,2 2&'-6 ,2&=,#wx `'%30# ~aT # +-2#30 3,'"'0#!2'-,,#* * . 02'!3* 0'2>"#.-34-'0!& ,%#0"#1#,1"#0-2 2'-,13'4 ,23,.0-!#1131!-,20D*>T S. Me2NOC. S. Me. S. . ! -* Z> (*6+ &,,!'& ++,*-,-* +. . . S. . . !%!)- + +%', -*+ *!& R5* <S5% ,T5% 6&6*,!'&+?. #+-2#30"#.0#+'=0#%>,>0 2'-,`Da#12 1>1303, *!=,#&>*'!-B" *!&'0 *T. 0-2 2'-, 3,'"'0#!2'-,,#**# 32-30 "# * *' '1-, !#,20 *# #12 ',"3'2# . 0 /3 20# >2 .#1 2�+'/3#+#,2 -3 .&-2-!&'+'/3#+#,2 !2'4>#1T ,1 !# ! 1 "# $'%30#Q *# +-34#+#,2 3,'"'0#!2'-,,#* #12 .-11' *# %0:!# 9 * !&'0 *'2> "3 1712=+# ',1' /3Z9 *Z ..-02"Z>,#0%'#*3+',#31#T 0 '**#301Q 3!3,#"'$$>0#,!' 2'-,#,20#* . 02'#0-2-0#2 * . 02'# 12 2-0 ,# .#32 ?20# $ '2#Q .3'1/3# *#1 "#36 . 02'#1 "# * +-*>!3*# 1-,2 '"#,2'/3#1T . # ">4#*-..#+#,2 "Z3, +-2#30 "# 1#!-,"# %>,>0 2'-, `Ea ..-02# /3#*/3#1. +>*'-0 2'-,1 9 1-, $-,!2'-,,#+#,2T 0-2 2'-, "3 +-2#30 E #12 .*31 0 .'"# /3# .0>!>"#++#,2Q * . 02'# 12 2-0 .#32 ?20# + ',2#, ,2 "'$$>0#,!'># "# * . 02'# 0-2-0 #2 *Z',20-"3!2'-,"#1%0-3.#+#,211-3$0>1"-,,#* .-11' '*'2>"#*'#0*#+-2#309"Z 320#1 +-*>!3*#1 -3 >4#,23#**#+#,2 9 3,# 130$ !# +>2 **'/3#T Z3,'"'0#!2'-,, *'2> "3 +-2#30 #12 + ',2#, ,2 1130># *-01 "# *Z>2 .# "Z',4#01'-, "# *Z&>*'!'2> `. 11 %# "Z3, !7!*# .&>,7*# "30-2-0 3V"#*9"312 2-09* + ,'=0#"Z3,#0-3#90-!#2!*'/3#2aT #1#,1 "# * 0-2 2'-, #12 /3 ,2 9 *3' !-,20D*> . 0 *# !#,20# 12>0>-%>,'/3# .-02 ,2 '!' 3, %0-3.#+#,2+>2&7*#T . *-01/3#*#1"#36.0#+'#01+-2#301!-,"3'1#,293,#0-2 2'-,3,'"'0#!2'-,,#**#Q. *#+-2#30"#20-'1'=+#%>,>0 2'-,`Fa >2>">4#*-..>" ,1*# 32"#.-34-'0',4#01#0 . RX.
(68) !& +%'$6-$!* + &+'$-,!'&'- ,'$$ ,! *# 1#,1 "# * 0-2 2'-, #2 ',1' . 11#0 "Z3,# 0-2 2'-, &-0 '0# 9 3,# 0-2 2'-, ,2'&-0 '0#T #22# -.>0 2'-, >2> 0>311'# %0:!# 9 * + A20'1# "# * !-,$'%30 2'-, "3 !#,20# 12>0>-%>,'/3#Q.3'1/3Z'*1Z %'2"#*Z>*>+#,2/3'0>%'2*#1#,1"#* 0-2 2'-,"3+-2#30T 0> !2'-, "Z>.'+>0'1 2'-, "3 !#,20# 12>0>-%>,'/3# "-,! >2> 32'*'1># .-30 !-,4#02'0 *# +-2#30F#,1-,>.'+=0#/3' *-01.#322-30,#0" ,1*#1#,1-..-1>T . ',1'Q *# +-2#30 E >2> +-"'$'> #, 0#+.* < ,2 *# %0-3.#+#,2 +>2&7*# . 0 3,. %0-3.#+#,2>.'+>0'1 *#Q*#"'+>2&7*! 0 +'"#T-,.-1'2'-,,#+#,2#,.-1'2'-,xZ 3 *'#3"#wZ. 00 ..-029* "-3 *#*' '1-,#12,>!#11 '0# $',"Z>4'2#0* 12 '*'1 2'-,"#* .-1'2'-, **7*'/3# *-01 "# * ">.0-2-, 2'-,T #22# 12 '*'1 2'-, 0#,"0 '2 *Z>.'+>0'1 2'-, +-',1#$$'! !#.3'1/3#*#! 0 ,'-,1#0 '2+-',10> !2'$T Me2NOC. S. S. Me2NOC. hv. Base . hv.
(69) . S.
(70)
(71) (3'S)-(P)-1' Clockwise rotation. Step 4. Step 2. S. S. CONMe2. S. Epimerization changes the direction of rotation.
(72) . S.
(73)
(74) (3'S)-(M)-1.
(75)
(76) (3'R)-(M)-1' Anticlockwise rotation. Step 2'. Step 4'. S. Me2NOC. CONMe2. S. hv. Step 5' . Step 3 . S. S.
(77)
(78) (3'R)-(P)-1. Base. hv.
(79)
(80) (3'S)-(P)-1'. CONMe2. Step 1'. S. S. S. Step 5.
(81)
(82) (3'S)-(M)-1. Me2NOC. b. CONMe2. Step 1. Step 3' S.
(83)
(84) (3'R)-(M)-1'. S.
(85)
(86) (3'R)-(P)-1. . ! -* RQ> (*6+ &,,!'&+ 6%,!)- +1$ + *',,!'& '*!* ,&,! '*!* '&,*8$6+ -%', -*F?. . # $-,!2'-,,#+#,2 "3 +-2#30 F #12 0#.0>1#,2> '%30# vuT Z'00 "' 2'-,. .&-2-!&'+'/3# "# *Z'1-+=0# `xZaV`aVF ',"3'2 3,# 0-2 2'-, "3 0-2-0 " ,1 *# 1#,1 &-0 '0# "-,, ,2 *'#3 9 * $-0+ 2'-, "# *Z'1-+=0# `xZaV`aVF; +-',1 12 *#Q .3'1/3# *# %0-3.#+#,2 "'+>2&7*! 0 +'"# 1# 20-34# #, .-1'2'-, .1#3"- 6' *# . 0 0 ..-02 3 12 2-0Q .-1'2'-, 12>0'/3#+#,2 ">$ 4-0 *# `>2 .#vaT ,# ',4#01'-, "Z&>*'!'2> 2�+'/3#+#,2 !2'4># 20 ,1$-0+# *Z'1-+=0# `xZaV`aVF; #, `xZaV`aVF .*31 12 *#Q >2 ,2"-,,>/3#*#%0-3.#+#,2"'+>2&7*! 0 +'"#0#4'#,2#,.-1'2'-,>/3 2-0' *#. 0 0 ..-02 312 2-0T#22#>2 .#.#0+#2 30-2-0"#$0 ,!&'0*#!7!*# #,8>,'/3#"312 2-0 9 * + ,'=0# "Z3,# 0-3# 9 0-! #2 !*'/3#2 #2 $-0!# . 0 !-,1>/3#,2 *# 1712=+# 9 1# ">.* !#0" ,13,#1#3*##2+?+#"'0#!2'-,`>2 .#waT,#1#!-,"#'00 "' 2'-,',"3'23,# 0-2 2'-, " ,1 *# 1#,1 &-0 '0# #2 20 ,1$-0+# *Z'1-+=0# `xZaV`aVF #, '1-+=0#. RY .
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